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DESIGN AND PROPERTIES OF A FUNCTIONALLY GRADIENT CERAMIC TOOL MATERIAL

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Acta Metallurgica Sinica(English Letters) 1999年第5期12卷 1054-1058页

作者： j. zhao,x. Ai, j.H. Zhang, j.x. Deng and C.Z. Huang Department of Mechanical Engineering, Shandong University of Technology, jinan 250061,China

Based on the analyses of the severity of cutting process as well as the failure mechanisms of ceramic tools, a model for designing functionally gradient ceramic tool materials with symmetrical distribution is presented, by which a Al 2O 3/(W,Ti)C ceramic tool material FG 2 was developed. Multi objective optimization method was employed in designing the compositional distribution of this ceramic tool material. The results of both continuous and intermittent cutting tests are indicative of the much better cutting behavior of the functionally gradient ceramic tool FG 2 than that of the common ceramic tool SG 4.

关键词： functionally gradient materials materials design compositional distribution ceramic tool

ExPERIMENTAL INVESTIGATION AND THERMODYNAMIC CALCULATION ON PHASE PRECIPITATION OF INCONEL 740

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Acta Metallurgica Sinica(English Letters) 2006年第6期19卷 425-431页

作者： S.Q.zhao Y.jiang j.x.Dong x.S.xie Department of Physics Ningxia UniversityYinchuan 750021China Department of Materials Science The Northwest Second Nationalities InstituteYinchuan 750021China High Temperature Materials Research Laboratories University of Science and Technology BeijingBeijing 100083China

A novel nickel-based superalloy INCONEL 740 was under development for application in ultra-supercritical superheater tubers above 750℃. The precipitation behaviors of η phase and γ' particles of the alloy were investigated through experimental study and phase computation. Experimental results showed that η phase formed a Widmanst?tten pattern structure following long-term exposure at elevated temperatures and that the coarsening of γ' particle follows a cube rate law:r-3 ∝ t. Thermodynamic calculation results showed that Al and Ti had an important effect on the precipitation behavior of γ' andη phases. Two suggested novel modified alloys, wherein the Al and Ti contents were modified, were designed and melted for the experimental study. The preliminary results indicated that the modified alloys exhibited higher structural stability following long-term exposure at 750℃ till 5000h.

关键词： superalloy INCONEL 740 precipitate thermodynamic calculation

Photoluminescence from Silicon Nanocrystals in Encapsulating Materials

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journal of Materials Science & Technology 2013年第3期29卷 221-224页

作者： Z.Deng x.D.Pi j.j.zhao D.Yang State Key Laboratory of Silicon Materials and Department of Materials Science and Engineering Zhejiang University

Naturally oxidized freestanding silicon nanocrystals （Si NCs） are incorporated in commonly used encapsulating materials to explore the photoluminescent application of Si NCs in device structures such as solid-state lighting light-emitting diodes （LEDs） and solar cells. The quantum yield of Si NCs before the incorporation has reached about 45% at the excitation wavelength of 370 nm without any special surface modification. It is found that medium Ioadings, e.g., 5 wt% of Si NCs in encapsulating materials help to obtain high external quantum efficiency （EQE） of the mixtures of Si NCs and encapsulating materials. The curing of encapsulating materials significantly reduces EQE. Among all the encapsulating materials investigated in this work, silicone- OE6551 enables the highest EQE （21% at excitation wavelength λex = 370 nm） after curing. Based on current findings, we have discussed the continuous efforts to advance the photoluminescent application of Si NCs.

关键词： Photoluminescence Silicon nanocrystals Epoxy Silicone Quantum yield External quantum efficiency

EFFECT OF SILICON ADDITION ON RECRYSTALLIZATION AND PHASE TRANSFORMATION BEHAVIOR OF HIGH-STRENGTH HOT-ROLLED TRIP STEEL

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Acta Metallurgica Sinica(English Letters) 2008年第3期21卷 163-168页

作者： L.j. Zhu D. Wu x.M. zhao College of Materials Science and Engineering Jilin University Changchun 130025 China The State Key Laboratory of Rolling Technology and Automation Northeastern University Shenyang110004 China

Because Si is a noncarbide forming element, a multiphase microstructure consisting of ferrite, bainite, and retained austenite, at room temperature, can be formed by controlling the thermomechanical process strictly. The cooling schedules must be restricted by the formation of pearlite and cementite. In the present article, a new integrated mathematical model for prediction of microstructure evolution during controlled rolling and controlled cooling is developed for a typical kind of low carbon Si-Mn TRIP steel, which consists of temperature simulation, recrystallization, and transformation models. The influence of Si contents has been thoroughly investigated. The calculated results indicate that Si retards recrystallization, restrains austenite grain growth as well as accelerates polygonal ferrite transformation.

关键词： TRIP steel Recrystallization Ferrite transformation Bainite transformation Silicon

MODELING OF MICROSTRUCTURAL EVOLUTION IN MICROALLOYED STEEL DURING HOT FORGING PROCESS

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Acta Metallurgica Sinica(English Letters) 2006年第4期19卷 279-286页

作者： j. Wang j. Chen Z. zhao x.Y. Ruan National Die ＆. Mold CAD Engineering Research Center Shanghai Jiaotong University Shanghai 200030 China

The microstractural evolution of microalloyed steel during hot forging process was investigated using physical simulation experiments. The dynamic recrystallized fraction was described by modifying Avrami＇s equation, the parameters of which were determined by single hit compression tests. Double hit compression tests were performed to model the equation describing the static recrystallized fraction, and the obtained predicted values were in good agreement with the measured values. Austenitic grain growth was modeled as： Dinc^5 = D0^5 ＋ 1.6 × 10^32t·exp （ -716870/RT ） using isothermal tests. Furthermore, an equation describing the dynamic recrystallized grain size was given as Ddyn=3771·Z^-0.2. The models of microstructural evolution could be applied to the numerical simulation of hot forging.

关键词： microalloyed forging steel flow stress recrystallized fraction grain size

Unlocking the stable interface in aqueous zinc-ion battery with multifunctional xylose-based electrolyte additives

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journal of Energy Chemistry 2025年第1期100卷 770-778页

作者： xiaoqin Li jian xiang Lu Qiu xiaohan Chen Yinkun zhao Yujue Wang Qu Yue Taotao Gao Wenlong Liu Dan xiao zhaoyu jin Panpan Li Institute for Advanced Study Chengdu University School of Mechanical Engineering Chengdu University College of Food and Biological Engineering Chengdu University Institute of Fundamental and Frontier Sciences University of Electronic Science and Technology of China College of Materials Science and Engineering Sichuan University

The growth of dendrites and the side reactions occurring at the Zn anode pose significant challenges to the commercialization of aqueous Zn-ion batteries（AZIBs）. These challenges arise from the inherent conflict between mass transfer and electrochemical kinetics. In this study, we propose the use of a multifunctional electrolyte additive based on the xylose（xylo） molecule to address these issues by modulating the solvation structure and electrode/electrolyte interface, thereby stabilizing the Zn anode. The introduction of the additive alters the solvation structure, creating steric hindrance that impedes charge transfer and then reduces electrochemical kinetics. Furthermore, in-situ analyses demonstrate that the reconstructed electrode/electrolyte interface facilitates stable and rapid Zn2+ion migration and suppresses corrosion and hydrogen evolution reactions. As a result, symmetric cells incorporating the xylo additive exhibit significantly enhanced reversibility during the Zn plating/stripping process, with an impressively long lifespan of up to 1986 h, compared to cells using pure ZnSO4electrolyte. When combined with a polyaniline cathode, the full cells demonstrate improved capacity and long-term cyclic stability. This work offers an effective direction for improving the stability of Zn anode via electrolyte design, as well as highperformance AZIBs.

关键词： Solvation

Cadmium sulfide cage photocatalysis coupled electroactive biofilm for synergistic promotion of tetracycline degradation and electricity production

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journal of Materials Science & Technology 2023年第35期166卷 86-97页

作者： Z.S.Yuan j.x.Zou x.L.zhao j.Y.Shi C.S.Guo M.Yan School of Chemistry and Chemical Engineering Harbin Institute of TechnologyHarbin 150001China

Tetracycline(TC)as a common broad-spectrum antibiotic,has been frequently detected in soil and sur-face *** becomes a great threat to the ecological ***,a device of photocatalysis as-sisted microbial fuel cell(photo-MFC)was constructed for TC degradation and energy *** this photo-MFC,cadmium sulfide(CdS)cage photocatalysis can degrade most of TC in a short *** the Co_(3)O_(4)@C-CC(carbonization and calcination of the ZIF-67 precursor in-situ grown on the carbon cloth(CC))bioanode degrades the rest of TC as well as the photocatalytic products,thus improving the *** co-existence of photocatalysis with bioanode changes the microbial community structure of the *** dominant phylum is Geobacter(60.2%)in normal MFC while that in photo-MFC are Pro-teobacteria(43.5%)and Geobacter(33.2%).Therefore,the synergistic effect of photocatalytic degradation and biodegradation achieves a chemical oxygen demand(COD)removal of 98.6%,which is higher than that of normal MFC(77.6%)or single CdS cage photocatalysis(23.8%).In addition,the photogenerated electrons can be transferred to the cathode,which reduces their combination with holes and increases the electricity generation of MFC,achieving a maximum power density of 3.37 W/m^(2).After degradation,the effluent with 200 mg L^(−1) TC exhibits no visible ***,electrochemical test,finite-difference time-domain(FDTD),density functional theory(DFT)calculation and the free radical trapping experiments verify the possible mechanisms of photocatalytic degradation in this *** strat-egy paves a new way for low energy consumption removal and energy recovery of organic pollutants.

关键词： Photo-MFC CdS cage Tetracycline degradation Mineralization Electricity production

Multistage serrated flow behavior of a medium-manganese high-carbon steel

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journal of Iron and Steel Research International 2020年第9期27卷 1064-1072页

作者： j.Chen Y.Zhang j.j.Wang C.M.Liu S.x.zhao Key Laboratory for Anisotropy and Texture of Materials Ministry of EducationNortheastern UniversityShenyang 110819LiaoningChina Shenyang Industrial Transformation Upgrading Promotion Center Shenyang 110083LiaoningChina The State Key Laboratory of Rolling and Automation Northeastern UniversityShenyang 110819LiaoningChina School of Materials Science and Engineering Northeastern UniversityShenyang 110819LiaoningChina Central Research Institute Baoshan Iron&Steel Co.Ltd.Shanghai 201999China

The deformation mechanisms and the flow stress behavior of a medium-manganese high-carbon steel during cold deformation at a strain rate of 10×5 s^-1 were explored using a universal testing machine,an x-ray diffractometer,a field emission scanning electron microscope and a high-resolution transmission electron *** results show that continuous step-up serrated flow behavior appears after the yielding point,and the true stress-strain curve is roughly divided into five stages based on distinctive densities and amplitudes of *** strengthening mechanisms of the experimental steel involve Cottrell atmosphere,twinning-induced plasticity(TWIP)efect and transformation-induced plasticity(TRIP)*** effect is the dominant deformation mechanism,and deformation twins formed by TWIP effect comprise primary,secondary and ***,TRIP effect arises in the local high-strain *** element plays a key role in the transformation of the deformation mechanism.A small amount of carbide precipitates around twin boundaries lead to the formation of local carbon-poor regions,and Md temperature and stacking fault energy of medium-manganese high-carbon steel are propitious to the occurrence of TRIP *** addition,the contributions of various deformation mechanisms to plasticity are calculated,and that of TWIP effect is the greatest.

关键词： Serrated flow Deformation mechanism Deformation twin Twinning-induced plasticity Transformation-induced plasticity

RECRYSTALLIZATION IN A SPINODAL Cu Ni Fe ALLOY

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Acta Metallurgica Sinica(English Letters) 1999年第4期12卷 322-326页

作者： Hao, S.M. Hao, x.j. zhao, G. Li, H.x. Northeastern Univ Shenyang China

The interaction of spinodal decomposition and recrystallization process, and the characteristic of recrystallization in Cu-Ni-Fe alloy aged at different temperatures after solution-treatment and cold rolling have been studied by structural analysis and Vickers hardness test. It has shown that the recrystallization of spinodal Cu -Ni-Fe alloy might be divided into 2 types: spinodal decomposition, recovery and recrystallization of two-phase microstructure take place in the deformed alloy aged below the spinodal temperature; while recrystallization of single-phase microstructure and growth of fully-recrystallized grains take place in the deformed alloy aged above the spinodal temperature. The deformed alloy aged below the spinodal temperature recrystallizes in cellular morphology.

关键词： Aging of materials Decomposition Iron alloys Metal melting Microstructure Morphology Nanotechnology Nickel alloys Permanent magnets Recrystallization (metallurgy)