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Growth,Structural and Microhardness Studies on New Semiorganic Single Crystals of Calcium Para Nitrophenolate Dihydrate

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journal of Materials Science & Technology 2007年第6期23卷 855-859页

作者： C.Vesta R.Uthrakumar C.justin Raj A.jonie Varjula j.mary linet S.jerome Das Department of Physics Loyola CollegeChennai-34India

Good quality crystals of calcium p-nitrophenolate （NPCa） were grown from saturated solution by slow evaporation method. The crystal structure analysis and the molecular arrangement of these crystals were determined using X-ray diffraction （XRD）. From Single crystal XRD studies, NPCa is found to be crystallized in the mon- oclinic system with a space group P21/n. The functional groups of the material were confirmed qualitatively by F-FIR （Fourier transform infrared spectroscopy） spectral analysis. Optical absorption studies reveal the absorption region and microhardness studies were carried out to confirm the mechanical behaviour of the crystals.

关键词： Characterization Crystal growth Structural analysis FTIR spectral analysis Microhardness UV-Vis analysis

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Growth, Optical, Mechanical, Dielectric and Theoretical Studies on Potassium Pentaborate Tetrahydrate (KB_5O_8·4H_2O) Single Crystal by Modified Sankaranarayanan-Ramasamy Method

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journal of Materials Science & Technology 2009年第6期25卷 745-748页

作者： C. justin Raj S. Krishnan S. Dinakaran j. mary linet R. Uthrakumar R. Robert S. jerome Das Department of Physics FET Saveetha University Department of Physics RMK Engineering College Department of Physics Loyola College

A nonlinear optical single crystal of potassium pentaborate tetrahydrate （KB5O8·4H2O） has been grown from aqueous solution by using unidirectional crystal growth method of Sankaranarayanan-Ramasamy （SR） with a due modification in the growth assembly. Potassium pentaborate crystal of 60 mm length and 10 mm diameter has been grown along （100） plane with a growth rate of 3 mm per day within a period of 20 days. The grown crystal was subjected to single crystal X-ray diffraction analysis to confirm that the crystal belongs to the orthorhombic system. Some fundamental data such as valance electron plasma energy, Penn gap, Fermi energy and electronic polarizability of the grown crystal were calculated. The presence of borate in the grown crystal was confirmed by Fourier transform infrared （FTIR） spectroscopy. The optical transmission property of the grown crystal was analyzed using ultra violet （UV） visible spectral analysis. Surface morphology of the growth plane was observed using scanning electron microscopy （SEM）. The mechanical strength of the crystals was found out using Vickers microhardness test along the growth axis. Frequency dependent dielectric constant of the grown crystal was studied for various temperatures along （100） plane.

关键词： Crystal growth Characterization Nonlinear optic materials

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