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Growth,Structural and Microhardness Studies on New Semiorganic Single Crystals of Calcium Para Nitrophenolate Dihydrate

Growth,Structural and Microhardness Studies on New Semiorganic Single Crystals of Calcium Para Nitrophenolate Dihydrate

作     者:C.Vesta R.Uthrakumar C.Justin Raj A.Jonie Varjula J.Mary Linet S.Jerome Das 

作者机构:Department of PhysicsLoyola CollegeChennai-34India 

出 版 物:《Journal of Materials Science & Technology》 (材料科学技术(英文版))

年 卷 期:2007年第23卷第6期

页      面:855-859页

核心收录:

学科分类:07[理学] 0817[工学-化学工程与技术] 0806[工学-冶金工程] 070205[理学-凝聚态物理] 08[工学] 080501[工学-材料物理与化学] 0805[工学-材料科学与工程(可授工学、理学学位)] 0703[理学-化学] 0802[工学-机械工程] 0801[工学-力学(可授工学、理学学位)] 0702[理学-物理学] 

主  题:Characterization Crystal growth Structural analysis FTIR spectral analysis Microhardness UV-Vis analysis 

摘      要:Good quality crystals of calcium p-nitrophenolate (NPCa) were grown from saturated solution by slow evaporation method. The crystal structure analysis and the molecular arrangement of these crystals were determined using X-ray diffraction (XRD). From Single crystal XRD studies, NPCa is found to be crystallized in the mon- oclinic system with a space group P21/n. The functional groups of the material were confirmed qualitatively by F-FIR (Fourier transform infrared spectroscopy) spectral analysis. Optical absorption studies reveal the absorption region and microhardness studies were carried out to confirm the mechanical behaviour of the crystals.

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