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Comparison of Perovskite Systems Based on AFeo_(3)(A=Ce,La,Y)in Co_(2) Hydrogenation to Co

Transactions of Tianjin University 2024年第4期30卷 337-358页

作者： Anna n.Matveyeva Shamil o.omarov Laboratory of Materials and Processes for Hydrogen Energy Ioff e Institute194021 St.PetersburgRussia

Co_(2) is the most cost-eff ective and abundant carbon resource,while the reverse water-gas reaction(rWGS)is one of the most eff ective methods of Co_(2) *** work presents a comparative study of rWGS activity for perovskite systems based on AFeo_(3)(where A=Ce,La,Y).These systems were synthesized by solution combustion synthesis(SCS)with diff erent ratios of fuel(glycine)and oxidizer(φ),diff erent amounts of nH 4 no_(3),and the addition of alumina or silica as *** techniques,including X-ray diff raction analysis,thermogravimetric analysis,Fourier transform infrared spectroscopy(FTIR),scanning electron microscopy,energy-dispersive X-ray spectroscopy,n 2-physisorption,H_(2) temper-ature-programmed reduction,temperature-programmed desorption of H_(2) and Co_(2),Raman spectroscopy,and in situ FTIR,were used to relate the physicochemical properties with the catalytic performance of the obtained *** specifi c perovskite-containing system(either bulk or supported)has its own optimalφand nH_(4) no_(3) amount to achieve the highest yield and dispersion of the perovskite *** all synthesized systems,bulk SCS-derived La-Fe-o systems showed the highest resistance to reducing environments and the easiest hydrogen desorption,outperforming La-Fe-o produced by solgel combustion(SGC).Co_(2) conversion into Co at 600°C for bulk ferrite systems,depending on the A-cation type and preparation method,follows the order La(SGC)nces in properties between La-Fe-o obtained by the SCS and SGC methods can be attributed to diff erent ratios of oxygen and lanthanum vacancy contributions,hydroxyl coverage,morphology,and free iron oxide *** situ FTIR data revealed that Co_(2) hydrogenation occurs through formates generated under reaction conditions on the bulk system based on La-Fe-o,obtained by the SCS method.γ-Al_(2)o_(3) improves the dispersion of CeFeo_(3) and LaFeo_(3) phases,the specifi c surface area,and the quant

关键词： Perovskites LaFeo_(3) CeFeo_(3) YFeo_(3) Solution combustion synthesis Co_(2) hydrogenation Reverse water–gas reaction(rWGS)

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numerical Simulation of Thermocapillary Convection with Evaporation Induced by Boundary Heating

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Fluid Dynamics & Materials Processing 2024年第7期20卷 1667-1686页

作者： o.n.Goncharova V.B.Bekezhanova Altai State University Institute of Mathematics and Information TechnologiesBarnaul656049Russia Institute of Computational Modelling SB RAS Department of Differential Equations of MechanicsKrasnoyarsk660036Russia

The dynamics of a bilayer system filling a rectangular cuvette subjected to external heating is *** influence of two types of thermal exposure on the flow pattern and on the dynamic contact angle is *** particular,the cases of local heating from below and distributed thermal load from the lateral walls are *** simulation is carried out within the frame of a two-sided evaporative convection model based on the Boussinesq approximation.A benzine–air system is considered as reference *** variation in time of the contact angle is described for both heating *** lateral heating,near-wall boundary layers emerge together with strong convection,whereas the local thermal load from the lower wall results in the formation of multicellular motion in the entire volume of the fluids and the appearance of transition regimes followed by a steady-state *** results of the present study can aid the design of equipment for thermal coating or drying and the development of methods for the formation of patterns with required structure and morphology.

关键词： Thermocapillary convection two-phase system numerical modeling contact angle

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Polyelectrolyte Complexes between Hyperbranched and Linear Polysaccharides: Fucoidan/Chitosan

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Chinese Journal of Polymer Science 2024年第4期42卷 468-479页

作者： Ekaterina R.Gasilova Daria n.Poshina Aleksandra o.Sitnikova natalia n.Saprykina Yury A.Skorik Institute of Macromolecular Compounds of the Russian Academy of Sciences Bolshoi VO 31St.Petersburg199004Russian Federation

Polyelectrolyte complexes(PECs)of hyperbranched(HB)and linear polysaccharides are promising as more effective encapsulation agents compared to PECs formed by linear *** investigated the PECs between the HB anionic polysaccharide fucoidan(FUC)and the cationic linear polysaccharide chitosan(CS).The FUC had a molecular weight(MW)of 30×*** PECs were prepared in three solvents(water,0.01 and 0.1 mol/L acetic acid)with CS of MW of 15,110 and 170 kDa,and deacetylation degrees(DDA)of 70%and 97%.The structures of the PECs and the initial FUC were investigated by multi-angle static and dynamic light *** the FUC contained 18 wt%of—oSo3 groups and 5 wt%of uronic acid units,it was a“strong-weak”copolyanion,so the HB macromolecules of the FUC formed nanogel particles in 0.1 mol/L AcoH and open branched structures in water,as confirmed by the Kratky *** mixing the solutions of original components,the PEC structures underwent an equilibration period,the duration of which increased with the MW of *** the charge stoichiometry was approached,the PECs shrank;the fractal dimension approached unity,indicating the side-by-side packing of adjacent FUC branches with the help of *** aggregation in the vicinity of the charge compensation was hardly observed,as it occurred in a very narrow *** PEC content at theζ-potential inversion depended on solvents’pH and the DDA of *** the extreme case of core-shell PECs in 0.1 mol/L AcoH,obtained by mixing FUC nanogels with the solutions of high MW CS of 97%DDA,the protruding tails of CS formed a positively charged shell in the whole range of FUC content(10 wt%nning electron microscopy and atomic force microscopy images of dried samples were discussed in relation to the light scattering results.

关键词： Polyelectrolyte complexes Chitosan Hyperbranched fucoidan Light scattering

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HL-3装置欧姆等离子体中高频磁流体不稳定性的实验观测

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核聚变与等离子体物理 2024年第3期44卷 328-333页

作者：杨秋磊陈伟张洁程时葵梁绍勇张轶泼 HL-3实验团队核工业西南物理研究院成都610041

在HL-3装置1MA电流等离子体欧姆放电实验期间,米尔诺夫(Mirnov)探针测量到两种高频磁流体(MHD)不稳定性。在等离子体启动阶段,电流爬升受到抑制,碘化钠探测器测量到逃逸电子增加。同时Mirnov探针测量到多分支频率f为20~400k Hz的高频MH... 详细信息

在HL-3装置1MA电流等离子体欧姆放电实验期间,米尔诺夫(Mirnov)探针测量到两种高频磁流体(MHD)不稳定性。在等离子体启动阶段,电流爬升受到抑制,碘化钠探测器测量到逃逸电子增加。同时Mirnov探针测量到多分支频率f为20~400k Hz的高频MHD不稳定性。结果表明,这种不稳定性的出现与逃逸电子增加密切相关,并抑制了等离子体电流的爬升,损失了大约7%伏秒数。等离子体电流和密度爬升时,Mirnov探针测量到频率f为110~160k Hz的高频MHD不稳定性。这种不稳定性频率与芯部阿尔芬频率成正比,处于环向阿尔芬本征模频率范围。随着这种不稳定性的演化,等离子体发生了破裂。这些高频MHD不稳定性的研究对于HL-3后续放电及未来ITER的初始放电有重要的参考意义。

关键词：等离子体磁流体不稳定性逃逸电子破裂

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RBC aggregation,deformation and adhesion to endothelium:Role of nitric oxide derived from L-Arginine and sodium nitroprusside

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Journal of Innovative optical Health Sciences 2024年第5期17卷 53-65页

作者： M.K.Maksimov P.B.Ermolinskiy o.n.Scheglovitova n.n.Sklyankina A.V.Muravyov A.E.Lugovtsov A.V.Priezzhev Faculty of Physics M.V.Lomonosov Moscow State University bld.1subbuilding.2Leninskie goryMoscow 11991Russia n.F.Gamaleya national Research Center for Epidemiology and Microbiology 18 Gamaleya StreetMoscow 123098Russia K.D.Ushinsky Yaroslavl State Pedagogical University 108/1 Respublikanskaya StreetYaroslavl 150000Russia

Red blood cells(RBCs)are the most abundant human blood *** aggregation and deformation strongly determine blood viscosity which impacts hemorheology and *** turn,RBC properties depend on di®erent endogenous and exogenous *** such factor is nitric oxide(no),which is mainly produced by endothelial cells(EC)from L-arginine amino acid in the circulatory *** the mechanisms of the RBC-endothelium interplay are not clear up to date and considering its possible clinical importance,the aims of this study are to investigate in vitro:(1)The e®ect of L-arginine induced no on RBC aggregation and adhesion to endothelium;(2)the no e®ect on RBC aggregation and deformation induced by L-arginine and sodium nitroprusside without the presence of endothelium in the *** RBC aggregation and adhesion to a monolayer of EC were studied using optical tweezers(oT).The RBC deformability and aggregation without endothelium in the samples were studied using the°ow chamber method and Myrenne *** con¯rmed that no increases deformability and decreases aggregation of *** showed that the soluble guanylate cyclase pathway appears to be the only no signaling pathway *** the samples with the endothelium,the\bell-shaped"dependence of RBC aggregation force on L-arginine concentration was observed,which improves our knowledge about the process of no production by ***,data related to L-arginine accumulation by endothelium were obtained:necessity of the presence of extracellular L-arginine stated by other authors was put under *** our study,no decreased the RBC-endothelium adhesion,however,the tendency appeared to be weak and was not con¯rmed in another set of *** our knowledge,this is the¯rst attempt to measure the forces of RBC adhesion to endothelium monolayer with oT.

关键词： Red blood cells aggregation L-arginine endothelium optical tweezers Myrenne flow chamber

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一道闪电的传说巴塞罗那Relámpago住宅

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室内设计与装修 2024年第6期 99-103页

作者： h3o建筑事务所秋落 h3o建筑事务所

总部位于巴塞罗那的年轻建筑事务所h3o建筑事务所推出了Relámpago住宅,这是他们最为特别和不同寻常的住宅项目之一。在巴塞罗那郊区圣胡斯特德斯韦恩的传统加泰罗尼亚农舍内,对一座面积55m2的谦逊老谷仓进行翻新,打造出一个色彩丰富的... 详细信息

总部位于巴塞罗那的年轻建筑事务所h3o建筑事务所推出了Relámpago住宅,这是他们最为特别和不同寻常的住宅项目之一。在巴塞罗那郊区圣胡斯特德斯韦恩的传统加泰罗尼亚农舍内,对一座面积55m2的谦逊老谷仓进行翻新,打造出一个色彩丰富的独特空间,向访客诉说着自己难忘的故事。项目的灵感源自业主的愿望,这是一位热爱创意和艺术的历史学家。设计师以多年前一道闪电穿越古老农舍的传说为出发点,力图在功能性和大胆设计中展现这一灵感,以激发客户的艺术兴趣。

关键词：建筑事务所巴塞罗那住宅项目艺术兴趣加泰罗尼亚 Rel 闪电

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转角的邂逅巴塞罗那Tiberi酒吧

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室内设计与装修 2024年第6期 104-107页

作者： h3o建筑事务所西溪 h3o建筑事务所

h3o建筑事务所是巴塞罗那一家年轻的设计公司,而同样位于巴塞罗那的Ti&beri俱乐部则以客制化的餐饮服务为人们所熟知。为了重新定义本地传统酒吧的体验,Tiberi俱乐部联手h3o建筑事务所的3位创始人Adri,orriols、JoanGener和MiquelRuiz,... 详细信息

h3o建筑事务所是巴塞罗那一家年轻的设计公司,而同样位于巴塞罗那的Ti&beri俱乐部则以客制化的餐饮服务为人们所熟知。为了重新定义本地传统酒吧的体验,Tiberi俱乐部联手h3o建筑事务所的3位创始人Adri,orriols、JoanGener和MiquelRuiz,共同打造了Tiberi酒吧。这是该俱乐部的第一家实体店,并已于2023年初夏开业。Tiber酒吧位于充满活力的PobleSec街区的一个转角处,面积82m^(2)。这个地区以多元的文化特色为亮点,吸引着众多的年轻人。设计师将这个空间打造成一个“宾至如归的酒吧”,完美诠释了Tiberi俱乐部的本质:试图通过提供独特的餐饮体验,来促进陌生人之间的交流和联系。

关键词：建筑事务所巴塞罗那餐饮服务俱乐部实体店酒吧陌生人客制化

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Detailed seismic zoning of the East Kazakhstan region in the Republic of Kazakhstan

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Geodesy and Geodynamics 2024年第2期15卷 156-165页

作者： natalya V.Silacheva n.P.Stepanenko o.K.Kurilova A.D.Kudabayeva A.T.Danabayeva Institute of Seismology Ministry of Emergency SituationsAlmaty 050060Kazakhstan

Kazakhstan is currently drafting new construction regulations that comply with the major provisions of the *** regulations are created on the basis of seismic zoning maps of various degrees of detail,developed by our Institute of Seismology using a new methodological approach for *** article is about creating the first normative map of the Detailed Seismic Zoning on a probabilistic foundation for the Republic of Kazakhstan’s East Kazakhstan *** carried out the probabilistic assessment of seismic hazard using a methodology consistent with the main provisions of Eurocode 8and updated compared with that used in developing maps of Kazakhstan’s General Seismic Zoning and seismic microzoning of *** most thorough and current data accessible for the area under consideration were combined with contemporary analytical *** have been done to not only the databases being used but also the way seismic sources were shown,including active faults *** a scale of 1:1000000,precise seismic zoning maps of the East Kazakhstan region were created for two probabilities of exceedance:10%and 2%in 50 years in terms of peak ground accelerations and macroseismic *** obtained seismic hazard distribution is generally consistent with the General Seismic Zoning of Kazakhstan’s previous ***,because active faults were included and a thoroughly revised catalog was used,there are more pronounced zones of increased danger along the fault in the western part of the *** the west of the territory,acceleration values also increased due to a more accurate consideration of seismotectonic *** maps are the basis for developing new state building regulations of the Republic of Kazakhstan.

关键词： Probabilistic seismic hazard assessment Detailed seismic zoning Peak ground acceleration Microseismical intensity

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Machine learning in liver surgery:Benefits and pitfalls

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World Journal of Clinical Cases 2024年第12期12卷 2134-2137页

作者： Rafael Calleja Manuel Durán María Dolores Ayllón Ruben Ciria Javier Briceño Hepatobiliary Surgery and Liver Transplantation Unit Hospital Universitario Reina SofíaMaimonides Biomedical Research Institute of CordobaCórdoba 14004Spain

The application of machine learning(ML)algorithms in various fields of hepatology is an issue of ***,we must be cautious with the *** this letter,based on a published ML prediction model for acute kidney injury after liver surgery,we discuss some limitations of ML models and how they may be addressed in the *** the future faces significant challenges,it also holds a great potential.

关键词： Machine learning Liver surgery Artificial intelligence Random forest Prediction model

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Phase composition,conductivity,and sensor properties of cerium-doped indium oxide

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nano Materials Science 2024年第2期6卷 193-200页

作者： M.I.Ikim G.n.Gerasimov V.F.Gromov o.J.Ilegbusi L.I.Trakhtenberg n.n.Semenov Federal Research Center for Chemical Physics of RAS MoscowRussia University of Central Florida OrlandoFLUSA Moscow Institute of Physics and Technology(State University) DolgoprudnyMoscow RegionRussia Lomonosov Moscow State University MoscowRussia

The hydrothermal synthesis of In_(2)o_(3)and Ceo_(2)–In_(2)o_(3)is investigated as well as the properties of sensor layers based on these *** the synthesis of In_(2)o_(3),intermediate products In(oH)_(3)and InooH are formed,which are the precursors of stable cubic(c-In_(2)o_(3))and metastable rhombohedral(rh-In_(2)o_(3))phases,respectively.A transition from c-In_(2)o_(3)to rh-In_(2)o_(3)is observed with the addition of Ceo_(2).The introduction of cerium into rh-In_(2)o_(3)results in a decrease in the sensor response to hydrogen,while it increases in composites based on c-In_(2)o_(3).The data on the sensor activity of the composites correlate with XPS results in which Ceo_(2)causes a decrease in the concentrations of chemisorbed oxygen and oxygen vacancies in rh-In_(2)o_(3).The reverse situation is observed in composites based on c-In_(2)o_(3).Compared to In_(2)o_(3)and Ceo_(2)–In_(2)o_(3.o.tained by other methods,the synthesized composites demonstrate maximum response to H_(2)at low temperatures by 70–100℃,and have short response time(0.2–0.5 s),short recovery time(6–7 s),and long-term stability.A model is proposed for the dependence of sensitivity on the direction of electron transfer between In_(2)o_(3)and Ceo_(2).

关键词： Cerium oxide Indium oxide nanocomposite Hydrothermal method Cubic phase Rhombohedral phase Sensor response Conductivity Hydrogen Response/recovery time

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