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Direct synthesis of large-area Al-doped graphene by chemical vapor deposition:Advancing the substitutionally doped graphene family

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Nano Research 2022年第2期15卷 1310-1318页

作者： Sami Ullah Yu Liu Maria Hasan Wenwen Zeng q.tao Shi Xiaoqin Yang Lei Fu huy q.ta Xueyu Lian Jingyu Sun Ruizhi Yang Lijun Liu Mark H.Rummeli College of Energy Soochow Institute for Energy and Materials Innovations Soochow UniversitySuzhou 215006China Key Laboratory of Advanced Carbon Materials and Wearable Energy Technologies of Jiangsu Province Soochow UniversitySuzhou 215006China NUTECH School of Applied Sciences&Humanities and Computer Engineering Department National University of TechnologyIslamabad 42000Pakistan Centre of Polymer and Carbon Materials Polish Academy of SciencesM.Curie-Sklodowskiej 34Zabrze 41-819Poland School of Energy and Power Engineering Xian Jiaotong UniversityXian 710049China College of Chemistry and Molecular Science Wuhan UniversityWuhan 430072China Institute for Complex Materials IFW Dresden 20 Helmholtz Strasse Dresden 01069Germany Institute of Environmental Technology VSB-Technical University of Ostrava17.listopadu 15Ostrava 70833Czech Republic

Graphene doping continues to gather momentum because it enables graphene properties to be tuned,thereby affording new properties to,improve the performance of,and expand the application potential of *** can be chemically doped using various methods such as surface functionalization,hybrid composites(e.g.,nanoparticle decoration),and substitution doping,wherein C atoms are replaced by foreign ones in the graphene *** works have predicted that graphene could be substitutionally doped by aluminum(Al)atoms,which could hold promise for exciting applications,including hydrogen storage and evolution,and *** theoretical predictions suggest that Al substitutionally doped graphene(AIG)could serve as a material for gas sensors and the catalytic decomposition of undesirable ***,fabricating Al substitutionally doped graphene has proven challenging until ***,we demonstrate how controlled-flow chemical vapor deposition(CVD)implementing a simple solid precursor can yield high-quality and large-area monolayer AIG,and this synthesis is unequivocally confirmed using various characterization methods including local electron energy-loss spectroscopy(EELS).Detailed high-resolution transmission electron microscopy(HRTEM)shows numerous bonding configurations between the Al atoms and the graphene lattice,some of which are not theoretically ***,the produced AIG shows a CO_(2) capturability superior to those of other substitutionally doped graphenes.

关键词： aluminum-doped graphene single-solid precursor chemical vapor deposition carbon dioxide capture energy storage catalytic applications

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Graphene transfer methods: A review

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Nano Research 2021年第11期14卷 3756-3772页

作者： Sami Ullah Xiaoqin Yang huy q.ta Maria Hasan Alicja Bachmatiuk Klaudia Tokarska Barbara Trzebicka Lei Fu Mark H.Rummeli College of Energy Soochow Institute for Energy and Materials InnovationsKey Laboratory of Advanced Carbon Materials and Wearable Energy Technologies of Jiangsu ProvinceSoochow UniversitySuzhou215006China School of Energy and Power Engineering Xi’an Jiaotong UniversityXi’an710049China Institute for Complex Materials IFW Dresden20 Helmholtz StrasseDresden01069Germany NUTECH School of Applied Sciences&Humanities and Computer Engineering DepartmentNational University of TechnologyIslamabad42000Pakistan Centre of Polymer and Carbon Materials Polish Academy of SciencesM.Curie-Sklodowskiej 34Zabrze41-819Poland College of Chemistry and Molecular Science Wuhan UniversityWuhan430072China Institute of Environmental Technology VŠB-Technical University of Ostrava17.listopadu 15Ostrava70833Czech Republic

Graphene is a material with unique properties that can be exploited in electronics, catalysis, energy, and bio-related fields. Although, for maximal utilization of this material, high-quality graphene is required at both the growth process and after transfer of the graphene film to the application-compatible substrate. Chemical vapor deposition (CVD) is an important method for growing high-quality graphene on non-technological substrates (as, metal substrates, e.g., copper foil). Thus, there are also considerable efforts toward the efficient and non-damaging transfer of quality of graphene on to technologically relevant materials and systems. In this review article, a range of graphene current transfer techniques are reviewed from the standpoint of their impact on contamination control and structural integrity preservation of the as-produced graphene. In addition, their scalability, cost- and time-effectiveness are discussed. We summarize with a perspective on the transfer challenges, alternative options and future developments toward graphene technology.

关键词： high-quality transfer application-compatible substrate graphene technology

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In-situ observations of novel single-atom thick 2D tin membranes embedded in graphene

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Nano Research 2021年第3期14卷 747-753页

作者： Xiaoqin Yang huy q.ta Wei Li Rafael G.Mendes Yu Liu q.tao Shi Sami Ullah Alicja Bachmatiuk Jinping Luo Lijun Liu Jin-Ho Choi Mark H.Rummeli School of Energy and Power Engineering Xi’an Jiaotong UniversityNo.28Xianning West RoadXian710049China

There is ongoing research in freestanding single-atom thick elemental metal patches,including those suspended in a two-dimensional(2D)material,due to their utility in providing new structural and energetic insight into novel metallic 2D *** pores have shown promise as support systems for suspending such *** study explores the potential of Sn atoms to form freestanding stanene and/or Sn patches in graphene *** atoms were deposited on graphene,where they formed novel single-atom thick 2D planar clusters/patches(or membranes)ranging from 1 to 8 atoms within the graphene *** of three or more atoms adopted either a star-like or close-packed structural *** functional theory(DFT)calculations were conducted to look at the cluster configurations and energetics(without the graphene matrix)and were found to deviate from experimental observations for 2D patches larger than five *** was attributed to interfacial interactions between the graphene pore edges and Sn *** presented findings help advance the development of single-atom thick 2D elemental metal membranes.

关键词： in-situ transmission electron microscopy Sn atoms planar cluster graphene vacancy

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悬浮于石墨烯空位/孔洞中的独立纳米结构

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Science China Materials 2023年第1期66卷 35-50页

作者：刘玉 huy q.ta 杨晓琴张月周军华施启涛曾梦琪 Thomas Gemming Barbara Trzebicka 付磊 Mark H.Rümmeli Soochow Institute for Energy and Materials Innovations College of PhysicsOptoelectronics and EnergyCollaborative Innovation Center of Suzhou Nano Science and TechnologyKey Laboratory of Advanced Carbon Materials and Wearable Energy Technologies of Jiangsu ProvinceSoochow UniversitySuzhou 215006China IFW Dresden P.O.Box D-01171 DresdenGermany Gusu Laboratory of Materials Suzhou 215123China Leibniz Institute for Solid State and Materials Research Dresden P.O.Box 270116D-01171 DresdenGermany Centre of Polymer and Carbon Materials Polish Academy of SciencesM.Curie-Sklodowskiej 34Zabrze 41-819Poland Institute of Environmental Technology VSB-Technical University of Ostrava17.Listopadu 15Ostrava70833Czech Republic College of Chemistry and Molecular Sciences Wuhan UniversityWuhan 430072China

在电子束辐照下,石墨烯较易形成空位、孔洞等缺陷,从而捕获外来原子,形成新的结构.由于这些结构具有一些令人兴奋的性质,它们和石墨烯之间的相互作用引起了科研工作者相当大的研究兴趣.本文总结了利用透射电子显微镜在制备和表征悬浮在... 详细信息

在电子束辐照下,石墨烯较易形成空位、孔洞等缺陷,从而捕获外来原子,形成新的结构.由于这些结构具有一些令人兴奋的性质,它们和石墨烯之间的相互作用引起了科研工作者相当大的研究兴趣.本文总结了利用透射电子显微镜在制备和表征悬浮在石墨烯中的独立纳米结构的方法,以及原子分辨率下观察到的此类材料中原子/结构的动态行为过程,讨论了新型金属/非金属掺杂剂对具有不同键结构的石墨烯空位的影响,以及位于石墨烯边缘的单原子/团簇的催化活性.此外,还讨论了独立单原子厚二维团簇/金属/金属烯和二维团簇/金属/金属烯氧化物的动态形成过程.并指出这些纳米结构的形成、稳定性和宏观效应对于新的原子/分子尺度纳米技术的实际应用至关重要.以上数据证实了新型纳米结构的数量不断增加,并预示着相关研究的不断深入.

关键词：纳米结构透射电子显微镜纳米技术键结构石墨烯单原子电子束辐照分子尺度

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An Enhanced Ensemble-Based Long Short-Term Memory Approach for Traffic Volume Prediction

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Computers, Materials & Continua 2024年第3期78卷 3585-3602页

作者： Duy quang Tran huy q.Tran Minh Van Nguyen Faculty of Civil Engineering Nha Trang UniversityNha Trang650000Vietnam Robotics and Mechatronics Research Group Faculty of Engineering and TechnologyNguyen Tat Thanh UniversityHo Chi Minh City700000Vietnam Department of Civil Engineering Ho Chi Minh City University of Technology and EducationHo Chi Minh City700000Vietnam

With the advancement of artificial intelligence,traffic forecasting is gaining more and more interest in optimizing route planning and enhancing service *** volume is an influential parameter for planning and operating traffic *** study proposed an improved ensemble-based deep learning method to solve traffic volume prediction problems.A set of optimal hyperparameters is also applied for the suggested approach to improve the performance of the learning *** fusion of these methodologies aims to harness ensemble empirical mode decomposition’s capacity to discern complex traffic patterns and long short-term memory’s proficiency in learning temporal ***,a dataset for automatic vehicle identification is obtained and utilized in the preprocessing stage of the ensemble empirical mode decomposition *** second aspect involves predicting traffic volume using the long short-term memory ***,the study employs a trial-and-error approach to select a set of optimal hyperparameters,including the lookback window,the number of neurons in the hidden layers,and the gradient descent ***,the fusion of the obtained results leads to a final traffic volume *** experimental results show that the proposed method outperforms other benchmarks regarding various evaluation measures,including mean absolute error,root mean squared error,mean absolute percentage error,and *** achieved R-squared value reaches an impressive 98%,while the other evaluation indices surpass the *** findings highlight the accuracy of traffic pattern ***,this offers promising prospects for enhancing transportation management systems and urban infrastructure planning.

关键词： Ensemble empirical mode decomposition traffic volume prediction long short-term memory optimal hyperparameters deep learning

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Post-CMOS processing challenges and design developments of CMOS-MEMS microheaters for local CNT synthesis

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Microsystems & Nanoengineering 2023年第6期9卷 281-295页

作者： Avisek Roy Bao q.ta Mehdi Azadmehr Knut E.Aasmundtveit Department of Microsystems University of South-Eastern Norway3184 HortenNorway

Carbon nanotubes(CNTs)can be locally grown on custom-designed CMOS microheaters by a thermal chemical vapour deposition(CVD)process to utilize the sensing capabilities of CNTs in emerging micro-and nanotechnology *** such a direct CMOS-CNT integration,a key requirement is the development of necessary post-processing steps on CMOS chips for fabricating CMOS-MEMS polysilicon heaters that can locally generate the required CNT synthesis temperatures(~650-900℃).In our post-CMOS processing,a subtractive fabrication technique is used for micromachining the polysilicon heaters,where the passivation layers in CMOS are used as masks to protect the *** dielectric etching,it is necessary to achieve high selectivity,uniform etching and a good etch rate to fully expose the polysilicon layers without causing *** achieved successful post-CMOS processing by developing two-step reactive ion etching(RIE)of the SiO2 dielectric layer and making design improvements to a second-generation CMOS *** the dry etching process,CMOS-MEMS microheaters are partially suspended by SiO2 wet etching with minimum damage to the exposed aluminium layers,to obtain high thermal *** fabricated microheaters are then successfully utilized for synthesizing CNTs by a local thermal CVD *** CMOS post-processing challenges and design aspects to fabricate CMOS-MEMS polysilicon microheaters for such high-temperature applications are detailed in this *** developed process for heterogeneous monolithic integration of CMOS-CNT shows promise for wafer-level manufacturing of CNT-based sensors by incorporating additional steps in an already existing foundry CMOS process.

关键词： synthesis steps damage

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Fuzzy Feedback Control for Electro-Hydraulic Actuators

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Intelligent Automation & Soft Computing 2023年第5期36卷 2441-2456页

作者： tan Nguyen Van huy q.Tran Vinh Xuan Ha Cheolkeun Ha Phu huynh Minh School of Engineering-Technology Thu Dau Mot UniversityThu Dau Mot City590000Vietnam Faculty of Engineering-Technology Nguyen Tat Thanh UniversityHo Chi Minh City754000Vietnam Hue Industrial College Hue City530000Vietnam Robotics and Mechatronics Lab University of UlsanUlsan City44610Korea

Electro-hydraulic actuators(EHA)have recently played a signiﬁcant role in modern industrial applications,especially in systems requiring extremely high *** can be explained by EHA’s ability to precisely control the position and force through advanced sensors and innovative control *** of the promising approaches to improve control accuracy for EHA systems is applying classical to modern control algorithms,in which the proportional–inte-gral–derivative(PID)algorithm,fuzzy logic controller,and a hybrid of these methods are popular *** this paper,we developed a novel version of the fuzzy control algorithm and linear feedback control method,namely fuzzy lin-ear feedback control,to improve the control *** achieve the highest performance,weﬁrst designed a mathematical EHA model based on the Matlab/Simulink software packages thanks to the selected parameters,which are similar to a real EHA ***,we respectively applied PID,fuzzy PID(FPID),and fuzzy linear feedback control(FLFC)before comparing them to have a full view of the outstanding advantages of the proposed *** simulation results showed that the proposed FLFC algorithm is approximately 99%and 77%super-ior in performance to the PID and feedback control algorithms,respectively.

关键词： Electro-hydraulic actuator fuzzy PID feedback control

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EXISTENCE AND StaBILITY OF PERIODIC AND ALMOST PERIODIC SOLUTIONS TO THE BOUSSINESq SYSTEM IN UNBOUNDED DOMAINS

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Acta Mathematica Scientia 2022年第5期42卷 1875-1901页

作者： Thieu huy NGUYEN Truong Xuan PHAM Thi Ngoc Ha VU The Sac LE School of Applied Mathematics and Informatics Hanoi University of Science and Technology Vien Toan ung dung va Tin hocDai hoc Bach khoa Hanoi 1DaiCoVietHanoiVietnam Department of Mathematics Faculty of Information TechnologyThuyloi university Khoa Cong nghe Thong tinBo mon ToanDai hoc Thuy loi175 Tay SonDong DaHa NoiViet Nam Thuyloi University Dai hoc Thuy Loi175 Tay SonDong DaHanoiViet Nam

In this paper we investigate the existence and stability of periodic solutions(on a half-line R_(+))and almost periodic solutions on the whole line time-axis R to the Boussinesq system on several classes of unbounded domains of R^(n) in the framework of interpolation *** the linear Boussinesq system we combine the L^(p)—L^(q)-smoothing estimates and interpolation functors to prove the existence of bounded mild ***,we prove the existence of periodic solutions by invoking Massera’s *** also prove the existence of almost periodic *** we use the results of the linear Boussinesq system to establish the existence,uniqueness and stability of the small periodic and almost periodic solutions to the Boussinesq system using fixed point arguments and interpolation *** results cover and extend the previous ones obtained in[13,34,38].

关键词： Boussinesq systems periodic solutions almost periodic solutions unbounded domains smoothing estimates dual estimates interpolation spaces stability

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Synergistic protection of Si anode based on multi-dimensional graphitic carbon skeletons

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Nano Research 2022年第9期15卷 8146-8155页

作者： q.tao Shi Haiming Wang Junhua Zhou huyquang ta Jiaqi Wang Xueyu Lian Klaudia Kurtyka Barbara Trzebicka Thomas Gemming Mark H.Rümmeli Soochow Institute for Energy and Materials Innovation College of EnergyKey Laboratory of Advanced Carbon Materials and Wearable Energy Technologies of Jiangsu ProvinceSoochow UniversitySuzhou 215006China Institute for Complex Materials IFW Dresden20 Helmholtz StrasseDresden 01069Germany Centre of Polymer and Carbon Materials Polish Academy of SciencesM.Curie-Sklodowskiej 34Zabrze 41-819Poland Thomas Gemming-Institute of Environmental Technology VSB-Technical University of Ostrava17.Listopadu 15Ostrava 70833Czech Republic

Inspired by the natural corn structure,a Si@hollow graphene shell@graphene(Si@GS@G)anode material was prepared in which silicon nanoparticles were preliminarily anchored onto the surface of an elastic graphene shell and further constrained using graphene *** graphene oxide shells with abundant surficial hydrogen bonds,which were synthesized using a novel bottom-up method,were used as an intermediate material to anchor positively charged silicon nanoparticles via electrostatic attraction and achieve a rational spatial *** inner hollow graphene shell anchorage and outer graphene constraint synergistically constituted a porous and robust conductive corn-like *** as-fabricated Si@GS@G anode afforded efficient electron and ion transport pathways and improved structural stability,thereby enhancing Li+storage capability(505 mAh·g^(−1)at 10 A·g^(−1))and extending the lifespan compared to the single hollow graphene shell or graphene sheet-protected Si anode(72%capacity retention after 500 cycles).The improved kinetics of the Si@GS@G anode were investigated using electro impedance spectroscopy,galvanostatic intermittent titration,and pseudocapacitance contribution rate analysis,and the structural evolution was analyzed using ex situ electron *** study proposes a novel hollow graphene oxide shell as an activated intermediate material for designing a porous electrode structure that facilitates an enhanced electrochemical performance.

关键词： synergistic protection multi-dimensional graphitic carbons corn-like structure elastic skeleton Si/C anode

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The RdDM Pathway Is Required for Basal Heat Tolerance in Arabidopsis

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Molecular Plant 2013年第2期6卷 396-410页

作者： Olga V. Popova huy q. Dinh Werner Aufsatz Claudia Jonak GMI-Gregor Mendel Institute of Molecular Plant Biology Austrian Academy of Sciences Dr. Bohr-Gasse 3 1030 Vienna Austria

Heat stress affects epigenetic gene silencing in Arabidopsis. To test for a mechanistic involvement of epige-netic regulation in heat-stress responses, we analyzed the heat tolerance of mutants defective in DNA methylation, his-tone modifications, chromatin-remodeling, or siRNA-based silencing pathways. Plants deficient in NRPD2, the common second-largest subunit of RNA polymerases IV and V, and in the Rpd3-type histone deacetylase HDA6 were hypersensi- tive to heat exposure. Microarray analysis demonstrated that NRPD2 and HDA6 have independent roles in transcriptional reprogramming in response to temperature stress. The misexpression of protein-coding genes in nrpd2 mutants recover-ing from heat correlated with defective epigenetic regulation of adjacent transposon remnants which involved the loss of control of heat-stress-induced read-through transcription. We provide evidence that the transcriptional response to temperature stress, at least partially, relies on the integrity of the RNA-dependent DNA methylation pathway.

关键词： heat stress RNA-directed DNA methylation transposons read-through transcription.

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