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Recent development of chemically complex metallic glasses: from accelerated compositional design, additive manufacturing to novel applications

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Materials Futures 2022年第1期1卷 9-31页

作者： J Y Zhang Z q Zhou Z B Zhang M H Park q Yu Z Li J Ma A d Wang H G huang M Song B S Guo q Wang Y Yang department of Mechanical Engineering College of EngineeringCity University of Hong KongKowloon TongKowloonHong KongPeople’s Republic of China Shenzhen Key Laboratory of High Performance Nontraditional Manufacturing College of Mechatronics and Control EngineeringShenzhen UniversityShenzhenGuangdong 518060People’s Republic of China School of Materials Science and Engineering Dongguan University of TechnologyDongguanGuangdong 523808People’s Republic of China Institute of Materials China Academy of Engineering PhysicsJiangyouSichuan 621907People’s Republic of China State Key Laboratory of Powder Metallurgy Central South UniversityChangshaHunan 410083People’s Republic of China Institute of Advanced Wear&Corrosion Resistant and Functional Materials Jinan UniversityGuangzhouGuangdong 510632People’s Republic of China Institute of Materials Laboratory for MicrostructuresShanghai UniversityShanghai 200444People’s Republic of China department of Materials Science and Engineering College of EngineeringCity University of Hong KongKowloon TongKowloonHong KongPeople’s Republic of China department of Advanced design and System Engineering College of EngineeringCity University of Hong KongKowloon TongKowloonHong KongPeople’s Republic of China

Metallic glasses(MGs)or amorphous alloys are an important engineering material that has a history of research of about 80–90 *** different fast cooling methods were developed for multi-component MGs between 1960s and 1980s,1990s witnessed a surge of research interest in the development of bulk metallic glasses(BGMs).Since then,one central theme of research in the metallic-glass community has been compositional design that aims to search for MGs with a better glass forming ability,a larger size and/or more interesting properties,which can hence meet the demands from more important *** this review article,we focus on the recent development of chemically complex MGs,such as high entropy MGs,with new tools that were not available or mature yet until recently,such as the state-of-the-art additive manufacturing technologies,high throughput materials design techniques and the methods for big data analyses(*** learning and artificial intelligence).We also discuss the recent use of MGs in a variety of novel and important applications,from personal healthcare,electric energy transfer to nuclear energy that plays a pivotal role in the battle against global warming.

关键词： metallic glasses amorphous alloys alloy design additive manufacturing machine learning high throughput materials design

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Solid solution strengthening of high-entropy alloys from first-principles study

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Journal of Materials Science & Technology 2022年第26期121卷 105-116页

作者： H.L.Zhang d.d.Cai X.Sun H.huang S.Lu Y.Z.Wang q.M.Hu L.Vitos X.d.ding State Key Laboratory for Mechanical Behavior of Materials Frontier Institute of Science and TechnologyXi’an Jiaotong UniversityXi’an 710049China Key Laboratory of Shaanxi Province for Craniofacial Precision Medicine Research College of StomatologyXi’an Jiaotong UniversityXi’an 710049China department of Materials Science and Engineering The Ohio State University2041 College RoadColumbusOH 43210United States Institute of Metal Research Chinese Academy of SciencesShenyang 110016China Science and Technology on Surface Physics and Chemistry Laboratory Jiangyou 621908China Applied Materials Physics Department of Materials Science and EngineeringRoyal Institute of TechnologyStockholm SE-10044Sweden

Solid solution strengthening(SSS)is one kind of strengthening mechanisms and plays an important role in alloy design,in particular for single-phase alloys including high-entropy alloys(HEAs).The classical Labusch–Nabarro model and its expansions are most widely applicable to treating SSS of solid solution alloys including both conventional alloys(CAs)and *** this study,the SSS effects in a series of Febased CAs and HEAs are investigated by using the classical Labusch–Nabarro model and its *** size misfit and shear modulus misfit parameters are derived from first-principles *** on available experimental data in combination with empirical SSS model,we propose fitting constants(i.e.,the ratio between experimental hardness and predicted SSS effect)for these two families of *** predicted host/alloy family-dependent fitting constants can be used to estimate the hardness of these SSS *** agreement between predicted and measured hardness values is satisfactory for both CAs and HEAs,implying that the proposed approach is reliable and successful.

关键词： Alloys Solid solution strengthening Hardness Size misfit parameter Shear modulus misfit parameter First-principles calculations

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MOdIFICATION OF SURFACE MECHANICAL PROPERTIES OF POLYCARBONATE BY B^+ ANd O^+ IONS IMPLANTATION

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Acta Metallurgica Sinica(English Letters) 2002年第1期15卷 33-38页

作者： S.d. Yao C. Sun S.q. Zhou C.C. Sun Y.H. Lu L. huang A. Vantomme q. Zhao G. Langouche Sch. of Phys. Peking Univ. Beijing 100871 China

By implanting B+ and O+ ions respectively into polycarbonate (PC) plates, the surface mechanical properties of PC have been improved. Measurement by Nano Indenter II showed that the hardness of samples increased 7-25 times than that before implantation; and the modulus of elasticity raised 2-5 times. The wear-resistance was tested by ball crusher; the width and depth of the wear-streak decreased by 1/3-1/2 or even more. The structure, deformation and appearance were analyzed by using Micro-FTIR Spectra, ESCA method and the steps instrument. These analyses showed that the structure of PC had been modified: a series of new cross-linking yielded, it depends on the Linear Energy Transition (LET) of implanted ions in the high polymer compounds.

关键词： polycarbonate ion implantation surface modification

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On the friction effects on rigid-body penetration in concrete and aluminium-alloy targets

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defence Technology（防务技术） 2019年第4期15卷 576-581页

作者： C.G. Chai A.G. Pi q.M. Li F.L. huang Institute of Chemical Materials China Academy of Engineering Physics Mianyang Sichuan 621900 China State Key Laboratory of Explosion Science and Technology Beijing Institute of Technology Beijing 100081 China School of Mechanical Aerospace and Civil Engineering University of Manchester Manchester M13 9PL UK

The friction on the projectile shank is usually excluded in the penetration analysis due to the difficulties to measure the pressure and frictional *** this article,the frictional force on projectile shank is discussed indirectly through the comparison between experimental data and empirical/analytical formulas of the penetration depth for both concrete and aluminium-alloy *** is found that the effect of the frictional force along the projectile shank can be further discussed by the afore comparison and discussion and cannot be ignored because of the relatively large effecting area,especially for deep penetration of concrete and aluminium-alloy targets,where the friction will account for more proportion of penetration resistance.

关键词： Penetration Friction Concrete Aluminium

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Acta Mechanica Sinica 2020年第6期36卷 1294-1301,I0003页

作者： C.G.Chai A.G.Pi q.M.Li F.L.huang Institute of Chemical Materials China Academy of Engineering PhysicsMianyang621900China State Key Laboratory of Explosion Science and Technology Beijing Institute of TechnologyBeijing100081China School of Mechanical Aerospace and Civil EngineeringUniversity of ManchesterManchesterM139PLUK

Similarity can reflect common laws in the mechanism of rigid-body *** this paper,the similarities in rigid-body penetration depth are demonstrated by three non-dimensional but physically meaningful quantities,i.e.,ρkinetic,I∗ln and N′*** three quantities represent the non-dimensional areal density of projectile kinetic energy,the effect of nose geometry,and the friction at the interactive cross section between projectile and target *** is shown that experimental data of rigid projectile penetration,from shallow to deep penetration,can be uniquely unified by these three similarity quantities and their ***,for ogival nose projectiles,their penetration capacities are dominated byρkinetic,which is consisted by non-dimensional effective length Leff and non-dimensional quantity dpn=ρpv20AY which has the same form as Johnson’s damage *** the sacrifice of minor theoretical accuracy,the non-dimensional penetration depth P/d can be understood as directly controlled by dpn,enhanced by projectile effective length Leff under a multiplication relation,and optimized by projectile nose geometry in the formation of I∗ln.

关键词： Concrete target deep penetration Similarity-Johnson's damage number

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Experimental study of“Tong Xia”purgative method in ameliorating lung injury in acute necrotizing pancreatitis

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World Journal of Gastroenterology 2000年第1期6卷 115-118页

作者： Xia q Jiang JM Gong X Chen GY Li L huang ZW department of TCM The First University Hospital of West China University of Medical SciencesChengdu 610041Sichuan ProvinceChina.

AIM To investigate the role of tumor necrosisfactor(TNF)in lung injury during acutenecrotizing pancreatitis(ANP),and thetherapeutic effect of'Tong Xia'purgativemethod in minimizing the severity of lung *** Fourteen canines were randomlydivided into 3 groups:the'Tong Xia'treatmentgroup(n = 5)using dachengqitang;salinecontrol group(n = 5),and the sham operationgroup(n = 4).TNF activity in serum and inbronchoalveolar lavage fluid(BALF),the serumendotoxin levels were measured,and theseverity of lung injury *** Elevation of TNF activity was moreprominent in BALF than in *** activity inserum at 6 and 12 hours and in BALI:wassignificantly decreased in the'Tong Xia'treatment group than in the saline control one(q=21.11,q=12.07,q=9.03,respectively,Pd the lung injury was significantlyalleviated at 12 hours as compared with that inthe saline group,manifested as amelioration otthe lung wet/ dry weight ratio,decrease inprotein concentration and neutrophils count inBALF,and improvement of pulmonaryinflammatory changes.A positive correlationwas demonstrated between serum TNF activity and endotoxin *** Hypersecretion of TNF is shownto be one of the major causes of lung injuryduring ANP;'Tong Xia'purgative method couldalleviate the degree of lung injury mediated byTNF.

关键词： Subject headings pancreatitis/therapy lung disease tumor necrosis factor Tong Xia method

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Extension/Compression-Controlled Complete Band Gaps in 2d Chiral Square-Lattice-Like Structures

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Acta Mechanica Solida Sinica 2018年第1期31卷 51-65页

作者： Y. L. huang N. Gao W.q. Chen R.H. Bao department of Engineering Mechanics Zhejiang University Hangzhou 310027 China State Key Lab of CAd & CG Zhejiang University Hangzhou 310058 China Key Laboratory of Soft Machines and Smart devices of Zhejiang Province Zhejiang University Hangzhou 310027 China Soft Matter Research Center Zhejiang University Hangzhou 310027 China

Achieving tunable band gaps in a structure by external stimuli is of great importance in acoustic applications. This paper aims to investigate the tunability of band gaps in square-lattice-like elastic periodic structures that are usually not featured with notable band gaps. Endowed with chirality, the periodic structures here are able to undergo imperfection-insensitive large deformation under extension or compression. The influences of geometric parameters on band gaps are discussed via the nonlinear finite element method. It is shown that the band gaps in such structures with curved beams can be very rich and, more importantly, can be efficiently and robustly tuned by applying appropriate mechanical loadings without inducing buckling. As expected, geometry plays a more significant role than material nonlinearity does in the evolution of band gaps. The dynamic tunability of band gaps through mechanical loading is further studied. Results show that closing, opening, and shifting of band gaps can be realized by exerting real-time global extension or compression on the structure. The proposed periodic structure with well-designed chiral symmetry can be useful in the design of particular acoustic devices.

关键词： Band gap Tunability Square-lattice-like periodic structure Chiral symmetry,Large deformation

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WIdE-BANd LASER CLAddING: WEAR ANd CORROSION RESISTANCE OF A Ni-BASEd ALLOY

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Acta Metallurgica Sinica(English Letters) 1997年第5期10卷 445-452页

作者： Pan, q.Y. huang, W.d. Li, Y.M. Lin, X. Zhou, Y.H. Yang, X.C. Northwestern Polytechnical Univ Xi'an China

A novel wide-band laser cladding system, with high rate of cladding, has been developed in the present work. The system mainly consisted of a 5kW CO2 laser, an automatic powder feeder and a wide-band scanning rotative polygon mirror which can produce a linear or rectangular focused laser beam. Using this system, a Ni-Cr-Si-B alloy powder was cladded on the surface of type 321 austenitic stainless steel in order to improve its wear and corrosion resistance. The pitting corrosion, high temperature oxidation and wear tests were conducted in order to evaluate the properties of the laser cladded layer. The results demonstrated that the cladded layer can significantly improve the adhesive wear and pitting corrosion resistance of the substrate. Moreover, the cladded layer exhibited good oxidation resistance, which is almost the same as that of GMR-235d Ni-based superalloy.

关键词： Boron Chromium alloys Cladding (coating) Laser applications Nickel alloys Silicon alloys Wear resistance

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Electrochemical performance of thermally-grown SiO2 as diffusion barrier layer for integrated lithium-ion batteries

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Frontiers in Energy 2018年第2期12卷 225-232页

作者： X.d.huang X.F.GAN q.A.huang J.Z.YANG Key Laboratory of MEMS of the Ministry of Education School of Electronic Science and EngineeringSoutheast UniversityNanjing 210096China School of Chemistry and Chemical Engineering Nanjing University of Science and TechnologyNanjing 210094China

direct integration of lithium-ion battery （LIB） with electronic devices on the same Si substrate can significantly miniaturize autonomous micro systems. For achieving direct integration, a barrier layer is essential to be inserted between LIB and the substrate for blocking Li^＋ diffusion. In this paper, the feasibility of thermal SiOa film as the barrier layer is investigated by electrochemical characterization and X-ray photoelectron spectroscopy （XPS）. due to the negligible side reactions of thermal SiO2 with electrolyte, the solid electrolyte interphase （SEI） layer formed on the surface of the barrier layer is thin and the SEI content mainly consists of hydrocarbon together with slight polyethylene oxide （PEO）, LixPOyFz, and Li2CO3. Although 8-nm thermal SiO2 effectively prevents the substrate from alloying with Li^＋, the whole film changes to Li silicate after electrochemical cycling due to the irreversible chemical reactions of SiO2 with electrolyte. This degrades the performance of the barrier layer against the electrolyte penetration, thus leading to the existence of Li^＋（in the form of F-Si-Li） and solvent decompositions （with the products of hydrocarbon and PEO） near the barrier layer/substrate interface. Moreover, it is found that the reaction kinetics of thermal SiO2 with electrolyte decrease significantly with increasing the SiO2 thickness and no reactions are found in the bulk of the 30-nm SiO2 film. Therefore, thermal SiO2 with an appropriate thickness is a promising barrier layer for direct integration.

关键词： autonomous micro system direct integration barrier layer thermal SiO2 film X-ray photoelectron spectroscopy (XPS)

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Evolution of microstructure and texture in copper during repetitive extrusion-upsetting and subsequent annealing

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Journal of Materials Science & Technology 2017年第7期33卷 690-697页

作者： q.Chen d.Y.Shu J.Lin Y.Wu X.S.Xia S.H.huang Z.d.Zhao O.V.Mishin G.L.Wu State Key Laboratory of Mechanical Transmission Chongqing University Chongqing 400044 China

The evolution of the microstructure and texture in copper has been studied during repetitive extrusionupsetting（REU） to a total von Mises strain of 4.7 and during subsequent annealing at different temperatures. It is found that the texture is significantly altered by each deformation pass. A duplex 001 ＋ 111 fiber texture with an increased 111 component is observed after each extrusion pass,whereas the 110 fiber component dominates the texture after each upsetting pass. during REU, the microstructure is refined by deformation-induced boundaries. The average cell size after a total strain of 4.7 is measured to be ~0.3 μm. This refined microstructure is unstable at room temperature as is evident from the presence of a small number of recrystallized grains in the deformed matrix. Pronounced recrystallization took place during annealing at 200？C for 1 h with recrystallized grains developing predominantly in high misorientation regions. At 350？C the microstructure is fully recrystallized with an average grain size of only 2.3 μm and a very weak crystallographic texture. This REU-processed and subsequently annealed material is considered to be potentially suitable for using as a material for sputtering targets.

关键词： Severe plastic deformation Repetitive extrusion-upsetting Copper deformation microstructure Texture Annealing

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