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一种合成α-溴代芳酮的简便方法

中国医药工业杂志 2016年第11期47卷 1393-1393页

作者： Ghorpade ak 宋承恩

芳烷基酮类化合物在亚硝酸钠（0．5倍摩尔量）和碘化钾（5mol％）存在下，经33％溴氢酸（1.2倍摩尔量）作用，

关键词：溴代简便芳酮合成酮类化合物亚硝酸钠碘化钾摩尔

葡萄膜黑色素瘤的发病趋势、治疗及预后[英]

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国际眼科纵览 2011年第6期35卷 420-421页

作者： Singh AD Turell ME Topham ak 杜葵芳（摘）

葡萄膜黑色素瘤是成年人常见的眼内原发性恶性肿瘤。常见的治疗手段为眼球摘除术、放射治疗或其他方法。其5年生存率不等，在25％～66％之间。随着新治疗手段（如经瞳孔温热治疗）的出现，以及大量较小的黑色素瘤由新技术所诊断，保留... 详细信息

葡萄膜黑色素瘤是成年人常见的眼内原发性恶性肿瘤。常见的治疗手段为眼球摘除术、放射治疗或其他方法。其5年生存率不等，在25％～66％之间。随着新治疗手段（如经瞳孔温热治疗）的出现，以及大量较小的黑色素瘤由新技术所诊断，保留患眼的治疗方法重新受到重视，传统的患眼摘除术逐渐减少。

关键词：葡萄膜黑色素瘤放射治疗发病趋势原发性恶性肿瘤经瞳孔温热治疗眼球摘除术预后 5年生存率

Interest of SAAG in Etiological Diagnosis of Ascites in African Black

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Open Journal of Gastroenterology 2018年第10期8卷 337-347页

作者： Okon Anassi Jean Baptiste Soro Dramane Doffou Stanislass Diakite Mamadou Koné Amadou aké Fabrice Thot’o Amani Sroboua N’dri N’guessan Hepato-Gastroenterology Department University Hospital Center Bouaké Ivory Coast Hepato-Gastroenterology Department University Hospital Center Abidjan Ivory Coast

Purpose: To show the interest of the serum-ascites concentration gradient in albumin (SAAG) in the etiological diagnosis of ascites in African black. Materiel and Methods: This was a monocentric observational and analytical study performed on patients over 15 years old and hospitalized in the Hepato-Gastroenterology department of Cocody from January 1st, 2010 to March 31st, 2017 for ascites. The cytology and chemistry of the ascites fluid and the protidogram were performed. The main outcome measure was the prediction of portal hypertension (PHT) or non-portal hypertension related causes of ascites from SAAG. Results: The hospital prevalence of ascites was 11%. There were 82 women (46.9%) and 93 men (53.1%) with a sex ratio (M/F) of 1.1. SAAG was low in 68.6% of cases and high in 31.4% of cases. The most common etiologies were post-viral cirrhosis (74%), HCC (16.60%) and peritoneal tuberculosis (13.7%) respectively. In the case of high SAAG, 91% of ascites related to PHT were observed, but also 77.5% of a low SAAG corresponded to ascites related to PHT (p = 0.024) with Se = 35% Sp = 84% and accuracy = 44%. All patients with peritoneal tuberculosis had a SAAG low of less than 1.1 g/dl significantly (p = 0.002). SAAG had a diagnostic performance of 89% in peritoneal tuberculosis at the cutoff value of ?1.24 g/dl (AUROC = 0.91, Se = 96%, Sp = 86%) while in post viral hepatitis cirrhosis at a threshold of 0.58 g/dl the diagnostic performance was 60% (AUROC = 0.69, Se = 53%, Sp = 79%). Conclusion: The simple technical SAAG, allowing to distinguish the ascites linked to the PHT and the ascites not bound to the PHT, can be used like a method of diagnosis of the etiologies of the ascites especially in the peritoneal tuberculosis in the African countries low income.

关键词： SAAG Ascites Peritoneal Tuberculosis Cirrhosis PHT

经口喷洒高渗葡萄糖:一新生儿镇痛的可行性选择

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世界核心医学期刊文摘（儿科学分册） 2005年第2期1卷 6-7页

作者： akξam M. rmeci A.R. 高蕊 Celebiler Mh.137.CadHubanlar IspartaTurkey

目的:研究表明疼痛和压力会引起新生儿生理和行为的显著改变。至今尚无药物被推荐用于缓解新生儿的轻度疼痛。由于有报道将不同的甜溶液用注射器经口给予患儿可减轻新生儿疼痛,笔者根据行为急性疼痛评定标准对当刺痛足月新生儿的脚后跟时。

关键词：经口高渗葡萄糖急性疼痛镇痛效果安慰剂对照口给无菌水处理方法

Cardiovascular Disorders during HIV-AIDS in the Point G University, Hospital Internal Medical Service

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Open Journal of Internal Medicine 2020年第1期10卷 13-20页

作者： Camara BD Traore ak Soukho-Kaya A Traore D Dembele M Diall IB Sy D Doumbia AA Dao K Tolo N Kailou A Traore HA Department of Internal Medicine CHU Point G Bamako Mali Cardiology Department CHU of Point G Bamako Mali

The number of HIV-infected patients in the world is estimated at 34 million, including 30.1 million adults with 2.7 million new infections and 1.8 million deaths from HIV according to the 2011 UN AIDS report [1]. The prevalence of HIV infection in the general population of Mali is estimated at 1.1% according to DHSM-V [2]. Cardiovascular manifestations are increasingly encountered during our consultations with patients living with HIV. Thus we initiated this work with the aim of studying the cardiovascular lesions during the HIV-AIDS in the department of internal medicine of the point G. Methods: This retrospective descriptive study was conducted in the Internal Medicine department of the University Hospital Center (CHU) of the Point G from January 2008 to December 2012. Having included all HIV + patients hospitalized in the service with cardiovascular manifestations and who had performed a chest X-ray, cardiac and vascular ultrasound, electrocardiogram and/or cerebral computed tomography. Results: At the end of this work, 20 patients with cardiovascular lesions were identified in 273 hospitalized patients during the study period, i.e. a frequency of 7.3%. The 40 to 50 age group accounted for 45.0% with an average age of 42.4 ± 8.73 years. The most common cardiovascular risk factors were hypertension and active smoking with 31.58% each. Pericarditis accounted for 32% of cases, followed by cardiomyopathies with 23%. Conclusion: In our study, cardiovascular lesions are common in PHAs and etiologies are dominated by pericarditis.

关键词： Cardiovascular Disorders HIV-AIDS ARVs

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醛-锅法转变为硫代伯酰胺

中国医药工业杂志 2014年第2期45卷 160-160页

作者： Yadav ak 温颖玲

醛在氨水作用下与碘（1．06eq）室温反应30min后，直接与二硫代磷酸A乙酯（1eq）于90℃反应2h，得相应的硫代伯酰胺，18例收率76％～93％。苯甲醛或苯乙醛芳环上带供电子基收率高于吸电子取代。操作简单，无需金属参与，实用性强。

关键词：二硫代磷酸苯乙醛酰胺一锅法室温反应水作用苯甲醛电子

Fanconi anemia manifesting as a squamous cell carcinoma of the mandible: a case report

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Open Journal of Stomatology 2011年第2期1卷 45-49页

作者： A. Pinar Erdem G. Ikikarakayali N. Yalman G ak M. A Erdem M. B. Bilgic E. Sepet 不详

Progressive bone marrow failure and development of malignancies, particularly acute myeloid leukemia and solid tumors the most important features of Fan- coni’s Anemia (FA). This paper reports the case of a 16-year-old patient with FA who developped squa- mous cell carcinoma of the mandible, ten years after the bone marrow transplantation (BMT).

关键词： Squamous Cell Carcinoma Fanconi’s Anemia Mandible Bone Marrow Transplantation

Simultaneous Determination by HPLC-UV Vis of Tartrazine and Sunset Yellow in Soft Drinks Sold in Benin

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American Journal of Analytical Chemistry 2022年第8期13卷 277-288页

作者： Janvier Engelbert Agbokponto André Philippe S. Kpaibe Loconon Achille Yemoa Assogba Gabin Assanhou Habib Ganfon Gildas Komenan Gbassi Michèle aké N’cho Christoph Amin Laboratoire de Chimie Analytique et d’Analyse des Médicaments UFR Pharmacie Faculté des Sciences de la Santé Université d’Abomey-Calavi Cotonou Bénin UFR Pharmacie Faculté des Sciences de la Santé Université d’Abomey-Calavi Cotonou Bénin Département de Chimie Analytique Bromatologie Chimie Générale et Minérale UFR des Sciences Pharmaceutiques et Biologiques Université Félix Houphou&euml t-Boigny Abidjan C&ocirc te d’Ivoire

The use of dyes such as tartrazine (E102) and sunset yellow (E102) in food, beverages and health products for technological and commercial purposes is common. The adverse effects caused by these dyes, such as allergies and hyperactivity disorder have been reported, especially in children. In the present study, a chromatographic method was developed and validated for simultaneous determination of tartrazine and sunset yellow. The chromatographic separation was performed on a Lichrocart® C18 column (125 × 4.6 mm;5 μm) with a security Guard-C18 column (4 × 2.0 mm, 5 μm;Phenomenex, Torrance, CA, USA) maintained at 30°C. The mobile phase consisted of a mixture of acetonitrile/ammonium acetate buffer pH 6.8 in gradient mode with a flow rate of 1 mL/min. The injection volume was 10 μL. The detection wavelength was set at 455 nm. The parameters of specificity, linearity, precision, repeatability, accuracy and sensitivity were examined for validation. The developed method is linear in the range of 1 μg/mL to 100 μg/mL with a R2> 0.998. The intra-day and inter-day precisions (RSD) were less than 0.6% and 3.1% respectively. The detection limit was 0.03 μg/mL and the quantification limit was 0.1 μg/mL. The retention time of tartrazine was 2.86 min, while sunset yellow was detected at 5.67 min. A simple, rapid, accurate and robust HPLC/UV-Visible method was developed and validated for simultaneous identification and quantification of tartrazine and sunset yellow. This developed method was successfully applied for the simultaneous determination of tartrazine and sunset yellow in soft drinks sold in Benin.

关键词： Tartrazine Sunset Yellow HPLC-UV Food Dyes

Structural Integrity of Welded Structures:Process-Property-Performance (3P) Relationship

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机械制造文摘（焊接分册） 2011年第1期 37-37页

作者： Mustafa Koak Gedik Holding Ankara Cad. No. 306 Seyhli-34913 PendikIstanbulTurkey Formerly at the GKSS Research Center

In most engineering metallic structures,welded joints are often the locations for the crack initiation due to inherent metallurgical,geometrical defects as well as heterogeneity in mechanical properties and presence of residual stresses. In order to maintain structural integrity of welded structures for whole service life of the structure,relationship between welding process,properties(of base metal & weld joint) and performance of the structure(requirements & controlling factors of the service conditions) should be well-understood and established. The quality of the relationship between this 3P is crucial to obtain economic and safe design,fabrication and service life. Specific features of each welding and joining process should ideally be well understood by the designer for a selected material at the early stage of the design. Resulting micro-structural & mechanical and geometrical properties should be obtained to have defined or intended structural performance under either specific environment or stresses. Nowadays,use of advanced welding processes with high performance steels and aluminum alloys together with well established and high quality welding consumables ensures safe and economic design,fabrication,inspection and service of the welded components and structures. Additionally,new developments in the fitness-for-service(FFS) procedures(e. g. BS 7910,R6 and FITNET FFS) and codes have significantly increased the accuracy of the structural integrity assessment of weld flaws. More and more engineering structures are built using multi-material design approach where numbers of materials with significantly different mechanical properties are joined to create weight and cost-efficient structures. Structural safety evaluation of such material-mix structures require sound understanding and description of the welding process,interfacial & weld joint properties in conjunction with global behavior of the component under external loadings. The existing knowledge on the w

关键词：焊接机械制造技术信息工艺