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Physico-chemical parameters for the assembly of moxifloxacin hydrochloride and cetyltrimethylammonium chloride mixture in aqueous and alcoholic media

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Chinese Journal of Chemical Engineering 2023年第5期57卷 280-289页

作者： Arnop Dutta Md.Tuhinur R.Joy Sk.Md.Ali Ahsan Mansour K.Gatasheh Dileep Kumar Malik Abdul Rub Md.anamul hoque Mohammad Majibur Rahman Nasrul Hoda D.M.Shafiqul Islam Department of Chemistry Jahangirnagar UniversitySavarDhaka 1342Bangladesh Department of Chemistry Jashore University of Science and TechnologyJashore 7408Bangladesh Department of Biochemistry College of ScienceKing Saud UniversityP.O.Box 2455Riyadh 11451Saudi Arabia Laboratory for Chemical Computation and Modeling Institute for Computational Science and Artificial IntelligenceVan Lang UniversityHo Chi Minh CityViet Nam Faculty of Applied Technology Van Lang UniversityHo Chi Minh CityViet Nam Center of Excellence for Advanced Materials Research King Abdulaziz UniversityJeddah 21589Saudi Arabia Chemistry Department Faculty of ScienceKing Abdulaziz UniversityJeddah 21589Saudi Arabia Department of Environmental Sciences Jahangirnagar UniversitySavarDhaka 1342Bangladesh Department of Neurology Henry Ford Health SystemDetroitMI 48292USA

The aggregation behavior of the mixture of cetyltrimethylammonium chloride(CTAC), a cationic surfactant, and moxifloxacin hydrochloride(MFH), a fourth-generation fluoroquinolone antibiotic drug, has been studied using the conductivity technique in aqueous and alcoholic(EtOH, 1-PrOH, and 2-BuOH)media. The study was performed at several temperatures between 298.15 and 323.15 K at 5 K *** assembly has been characterized by evaluating the micellar parameters, such as the critical micelle concentration(CMC) and the counter ion binding(β), of the CTAC + MFH mixture. The values of the CMC for the assembly of the CTAC + MFH mixture were reliant on the composition of alcohols in the mixed solvents and the temperature. The CMC values of the CTAC + MFH mixture increased with increasing temperature;that is, assembly was delayed by increased temperature. The micellization of the CTAC + MFH mixed system was delayed in alcoholic media. The observed-ΔG0mvalues for the association of the CTAC + MFH mixed system demonstrated a spontaneous aggregation process under all study *** on the-ΔH^(0)_(m) and +ΔS^(0)_(m) values, the association of the CTAC + MFH mixture is exothermic and the interaction forces acting between the CTAC and MFH species are hydrophobic, ion–dipole, and electrostatic interactions. The transfer properties and enthalpy–entropy compensation were also assessed and described comprehensively.

关键词： Moxifloxacin hydrochloride drug Aggregation Alcohol Hydrophobic interaction Critical micelle concentration Thermodynamic properties

Interaction of cetyltrimethylammonium bromide with cefixime trihydrate drug at different temperatures and compositions: Effect of different electrolytes

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Chinese Journal of Chemical Engineering 2019年第8期27卷 1895-1903页

作者： Marzia Rahman Md.anamul hoque Malik Abdul Rub Mohammed Abdullah Khan Department of Chemistry Jahangirnagar UniversitySavarDhaka 1342Bangladesh Chemistry Department Faculty of ScienceKing Abdulaziz UniversityJeddah 21589Saudi Arabia Center of Excellence for Advanced Materials Research King Abdulaziz UniversityJeddah 21589Saudi Arabia

Herein,conductivity measurements have been carried out to explore the interaction between cetyltrimethylammonium bromide(CTAB,a cationic surfactant) and antibiotic drug(cefixime trihydrate(CMT)) in water and also in occurrence of inorganic salts(NaCl,Na2 SO4 and Na3 PO4) over the temperature range of 303.15-323.15 K with an interval of 5 *** all cases,two critical micelle concentrations(c^*) were achieved for the CMT-surfactant *** of CMT drug to CTAB solution decreases the values of c^* which indicates the interaction between CMT and *** values of c^* for CMT-CTAB mixture in the presence of salts are lower in magnitude compared to the aqueous medium which indicates that micellization of the CMT-CTAB mixed system is favorable in salt *** values of △Gm^0 were obtained to be negative indicating the spontaneity of the micellization process and the extent of spontaneity further increases by means of rising *** obtained outcomes from the ΔHm^0 and ΔSm^0 values disclose that the interactions between CMT and CTAB are mostly electrostatic along with hydrophobic in *** thermodynamic parameters of transfer and enthalpy-entropy compensation phenomenon were also determined and discussed in detail.

关键词： Cefixime trihydrate CTAB Critical micelle concentration Compensation temperature Free energy of transfer

Antioxidant Defense Mechanisms of Salinity Tolerance in Rice Genotypes

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Rice science 2017年第3期24卷 155-162页

作者： Mohammad Golam KIBRIA Mahmud HOSSAIN Yoshiyuki MURATA Md.anamul hoque Department of Soil Science Bangladesh Agricultural University Graduate School of Natural Science and Technology Okayama University

In order to elucidate the role of antioxidant responses in salinity tolerance in rice genotypes under salt stress, experiments were conducted using four rice varieties, including salt-sensitive BRRI dhan 28 and three salt-tolerant varieties BRRI dhan 47, BINA dhan 8 and BINA dhan 10. Thirty-day-old rice seedlings were transplanted into pots. At the active tillering stage(35 d after transplanting), plants were exposed to different salinity levels(0, 20, 40 and 60 mmol/L NaCl). Salt stress caused a significant reduction in growth for all the rice genotypes. Growth reduction was higher in the salt-sensitive genotype than in the salt-tolerant ones, and BINA dhan 10 showed higher salt tolerance in all measured physiological parameters. The reduction in shoot and root biomass was found to be minimal in BINA dhan 10. Chlorophyll content significantly decreased under salt stress except for BINA dhan 10. Proline content significantly increased in salt-tolerant rice genotypes with increased salt concentration, and the highest proline content was obtained from BINA dhan 10 under salt stress. Catalase and ascorbate peroxidase activities significantly decreased in salt-sensitive genotype whereas significantly increased in salt-tolerant ones with increasing salt concentration. However, salt stress significantly decreased guaiacol peroxidase activity in all the rice genotypes irrespective of salt tolerance. K^+/Na^+ ratio also significantly decreased in shoots and roots of all the rice genotypes. The salt-tolerant genotype BINA dhan 10 maintained higher levels of chlorophyll and proline contents as well as catalase and ascorbate peroxidase activities under salt stress, thus, this might be the underlying mechanism for salt tolerance.

关键词： antioxidant enzyme salinity chlorophyll content proline content K+/Na+ ratio rice

Effect of different additives on the phase separation behavior and thermodynamics of p-tert-alkylphenoxy poly (oxyethylene) ether in absence and presence of drug

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Chinese Journal of Chemical Engineering 2018年第5期26卷 1110-1118页

作者： Marzia Rahman Md. anamul hoque Mohammed Abdullah Khan Malik Abdul Rub Abdullah M. Asiri Department of Chemistry Jahangirnagar University Savar Dhaka 1342 Bangladesh Chemistry Department Faculty of Science King Abdulaziz University Jeddah 21589 Saudi Arabia Center of Excellence for Advanced Materials Research King Abdulaziz UniversityJeddah 21589 Saudi Arabia

Cloud point(CP) determinations of 4-(1,1,3,3-tetramethylbutyl)phenyl-polyethylene glycol(TX-100(nonionic surfactant)) was carried out in aqueous as well as in the attendance of drug(ceftriaxone sodium trihydrate(CFT))/(CFT + different inorganic salts) and discussed thoroughly. Nonionic surfactants are employed extensively in different formulations. In aqueous solution, the values of CP of TX-100 are obtained to increase by means of enhancing of their concentration in the solution. The CP values of TX-100 solutions were found to decrease in the presence of drug and their values decrease more with rising concentrations of the drug. The values of CP of CFT and TX-100 mixtures were found to further decrease in the attendance of inorganic salts in comparison to their absence. The effect of different sodium salts in decreasing CP values of TX-100 was achieved in the following order: NaCO_3 > Na_2SO_4 > Na Cl. However, in the case of potassium and ammonium salts, the decreasing order obtained is K_2SO_4 > KCO_3 > KCl and(NH4)2 SO_4 > Na_2CO_3 > NH_4Cl respectively. Various thermodynamic parameters for example standard free energy(ΔG_c~Θ), standard enthalpy(ΔH_c~Θ) as well as standard entropy(Δ Sc?)changes of phase separation were also evaluated and discussed in detail on the basis of their behavior.

关键词：分离行为热力学 poly TX-100 添加剂表面活化剂聚乙烯乙二醇 Na2SO4

Interaction of tetradecyltrimethylammonium bromide with bovine serum albumin in different compositions: Effect of temperatures and electrolytes/urea

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Chinese Journal of Chemical Engineering 2021年第1期34卷 279-287页

作者： Joynal Abedin ShamimMahbub Mohammad Majibur Rahman anamul hoque Dileep Kumar Javed Masood Khan Ahmed M.El-Sherbeeny Department of Chemistry Jahangirnagar UniversitySavarDhaka 1342Bangladesh Department of Chemistry&Physics Gono BishwabidyalaySavarDhaka 1344Bangladesh Department of Environmental Sciences Jahangirnagar UniversitySavarDhaka 1342Bangladesh 4 Division of Computational Phys ics Institute for Computational ScienceTon Duc Thang UniversityHo Chi Minh CityViet Nam Faculty of Applied Sciences Ton Duc Thang UniversityHo Chi Minh CityViet Nam Department of Food Science and Nutrition Faculty of Food and Agricultural SciencesKing Saud University2460Riyadh 11451Saudi Arabia Industrial Engineering Department College of EngineeringKing Saud UniversityP.O.Box 800Riyadh 11421Saudi Arabia

Herein,the interaction of a protein,bovine serum albumin(BSA),with tetradecyltrimethylammonium bromide(TTAB,a cationic surfactant),has been investigated using the conductivity measurement technique in pure water and some sodium salts(NaCl,Na_(2) SO_(4),Na_(2) CO_(3), and Na_(3) PO_(4)) solutions at temperature range of 295.15-320.15 *** reveal that,in the plot of specific conductivity versus the concentration of TTAB,only a single critical micelle concentration(cmc) was found for the TTAB+BSA mixed system in all solvents media *** addition of BSA in aqueous TTAB solution,the value of cmc undergoes a change from its pure form,which indicates the presence of strong interaction operating between the BSA and TTAB *** aqueous system,the cmc values of the TTAB+BSA mixtures are obtained higher compared to the values found for single TTAB surfactant However,the addition of salt decreases the cmc value of mixed TTAB+BSA *** values of cmc of the BSA+TTAB mixed system at 310.15 K and 1.00 mmol·kg^(-1) ionic strength of salt followed the order:cmc_(Na_(2) CO_(3))> Cmcc_(Na_(3) PO_(4))> cmcNaCl>cMC_(Na_(2) SO_(4)).The cmc values of TTAB+BSA mixture were found to be lowered in urea solution within the concentrations *** values of degree of dissociation(α) and fraction of counter ion binding(β) were found to be dependent on additives and *** free energy of micellization(AGm) is negative for all the systems,which manifests that the micellization phenomenon is energetically *** enhancement of the negative value of △G_(m)^(0) in aqueous salt solutions reveals an increase of spontaneity of the TTAB+BSA micellization *** values of △G_(m)^(0) also reveal that the spontaneity of micelle formation is enhanced at higher temperatures in all media *** values of free energy of transfer(△G_(m,t)^(o)) were also determined for numerous solvent media used in the present study and described with appropriate reasoning.

关键词： TTAB BSA Conductivity Electrolyte Exothermic interaction

Interaction of cetyltrimethylammonium bromide with drug in aqueous/electrolyte solution:A combined conductometric and molecular dynamics method study

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Chinese Journal of Chemical Engineering 2018年第1期26卷 159-167页

作者： Md.anamul hoque Md.Masud Alam Mohammad Robel Molla Shahed Rana Malik Abdul Rub Mohammad A.Halim Mohammed Abdullah Khan Farida Akhtar Department of Chemistry Jahangirnagar UniversitySavarDhaka 1342Bangladesh Chemistry Department Faculty of ScienceKing Abdulaziz UniversityJeddah 21589Saudi Arabia Center of Excellence for Advanced Materials Research King Abdulaziz UniversityJeddah 21589Saudi Arabia Division of Quantum Chemistry BICCBThe Red-Green Computing Centre218 Elephant RoadDhaka 1205Bangladesh Institut Lumière Matière Université Lyon 1-CNRSUniversitéde Lyon69622 Villeurbanne CedexFrance

Interaction between beta-lactum antibiotic drug ciprofloxacin hydrochloride(CFH)and cationic surfactant cetyltrimethylammonium bromide(CTAB)was performed conductometrically in aqueous as well as in the occurrence of different salts(NaCl,KCl as well as NH_4Cl)over the temperature range of 298.15–323.15 K at the regular interval of 5 *** drug has been suggested for the treatment of bacterial infections such as urinary tract infections and acute sinusitis.A clear critical micelle concentration(CMC)was obtained for pure CTAB as well as(CFH+CTAB)mixed *** decrease in CMC values of CTAB caused by the addition of CFH reveals the existence of the interaction between the components and therefore it is the indication of micelle formation at lower concentration of CTAB and their CMC values further decrease in attendance of salts.A nonlinear behavior in the CMC versus T plot was observed in all the *** ΔG_m^0 values are found to be negative in present study systems demonstrated the stability of the *** values of ΔH_m^0 and ΔS_m^0 reveal the existence of hydrophobic and electrostatic interactions between CFH and *** thermodynamic properties of transfer for the micellization were also evaluated and discussed in *** dynamic simulation disclosed that environment of water and salts have impact on the hydrophobic interaction between CFH and *** water and salts,CTAB adopts spherical micelle in which charged hydrophilic groups are interacted with waters whereas hydrophobic tails form the core of the *** hydrophobic core region is highly conserved and *** addition,micelle formation is more favorable in aqueous Na Cl solution than other solutions.

关键词：相互作用溴化物动力学方法电解质学习分子尿道感染表面活化剂

Effects of arbuscular mycorrhizal fungi,biochar,selenium,silica gel,and sulfur on arsenic uptake and biomass growth in Pisum sativum L.

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Emerging Contaminants 2020年第1期6卷 312-322页

作者： Mohammad Zahangeer Alam Md.anamul hoque Golam Jalal Ahammed Lynne Carpenter-Boggs Department of Environmental Science Faculty of AgricultureBangabandhu Sheikh Mujibur Rahman Agricultural University(BSMRAU)Gazipur1706Bangladesh Department of Soil Science Bangladesh Agricultural University(BAU)MymensinghBangladesh College of Forestry Henan University of Science and TechnologyLuoyang471023PR China Department of Crop and Soil Sciences Washington State University(WSU)Pullman WA99164-6420USA

Arsenic(As)is carcinogenic and highly toxic to *** accumulate As when grown in field soils irrigated with As-contaminated *** accumulation of As in roots,shoots,and grains of pea varieties can negatively affect human health via the food *** research is focused on the biomass growth and alleviation of As accumulation in roots,shoots,and grains of pea varieties in high As soil amended with arbuscular mycorrhizal fungi(AMF),biochar(BC),selenium(Se),silica gel(Si-gel),and sulfur(S).Root,shoot,and grain masses were found higher in pea grown in As soil amended with AMF,Se,Si-gel,and *** with rice husk and sawdust BC was found less effective to increase growth parameters in Bangladesh Agricultural Research Institute(BARI)Motor *** in grains was reduced by 77%,71%,and 69%by AMF,Se,and Si-gel,*** is recommended that soil amendments with AMF,S,and Se have great potential for improving biomass production of pea grown in As-contaminated soil,as well as reducing As transfer to humans through the food chains.

关键词： Arsenic Pea Food chain AMF Food safety Metal

A Review on Plant Responses to Soil Salinity and Amelioration Strategies

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Open Journal of Soil Science 2019年第11期9卷 219-231页

作者： Mohammad Golam Kibria Md. anamul hoque Department of Soil Science Bangladesh Agricultural University Mymensingh Bangladesh

Soil salinity is a major abiotic stress, limiting plant growth and development worldwide. Plants grown under saline soil condition experiences a significant amount of high osmotic stress, ion toxicities and nutritional disorder, and these are responsible for poor soil physical condition as well as lead to reduced plant productivity. Plants exhibit a number of responses under salt stress by affecting morphological, physiological and biochemical process. A complete understanding of how plants respond to soil salinity and comprehensive management approaches of combining physiological and biochemical attributes with molecular tools are essential for mitigating the adverse effects of salinity on plant growth and productivity. Recent reports on the plant responses due to soil salinity highlighted the importance of integration of different advanced strategies to address the problem of soil salinity. This review will focus on morphological and physiological changes of plants under saline soil and an overview of suitable strategies to regulate plant adaptation and tolerance to salinity stress.

关键词： Salinity Antioxidant Enzymes Adaptation To Salinity Proline Plant Physiology

Interaction of ciprofloxacin hydrochloride with sodium dodecyl sulfate in aqueous/electrolytes solution at different temperatures and compositions

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Chinese Journal of Chemical Engineering 2020年第1期28卷 216-223页

作者： Sk.Md.Ali Ahsan Md.Ruhul Amin Shamim Mahbub Mohammad Robel Molla Shahina Aktar Malik Abdul Rub Md.anamul hoque Muhammad Nadeem Arshad Mohammed Abdullah Khan Department of Chemistry Jahangirnagar UniversitySavarDhaka 1342Bangladesh Chemistry Department Faculty of ScienceKing Abdulaziz UniversityJeddah-21589Saudi Arabia Center of Excellence for Advanced Materials Research King Abdulaziz UniversityJeddah-21589Saudi Arabia

Interactions of ciprofloxacin hydrochloride(CPFH)with sodium dodecyl sulfate(SDS)were investigated by conductivity measurement in H2O/electrolyte solutions(NaCl,Na2SO4&Na3PO4)over 298.15–318.15 K temperature range(with 5 K interval)considering the human body *** all cases,two critical micelle concentrations(c*)were observed which are increased in the presence of drug and decreased in the presence of salts enunciating the presence of interaction amongst the studied ***(CPFH+SDS)system in the presence of salt,the c*values at 303.15 K and I=0.50 mmol·kg^-1 followed the order:CNaCl>CNa2SO4>***ΔG1,m0 andΔG2,m0values are found to be negative for all systems that show that the micellization process is thermodynamically ***(CPFH+SDS)system in water,theΔHm0&ΔSm0 values reveal that the micellization processes is both entropy dominated in almost all *** the occurrence of electrolytes,ΔHm0 andΔSm0 values indicate that micellization processes are both entropy&enthalpy restricted at upper temperature but it becomes totally entropy dependent at higher *** higher positiveΔSm0 values indicate the enhanced hydrophobic interaction in presence of *** enthalpy-entropy compensation was determined from the linear relationship betweenΔHm0 andΔSm0 values in every *** transfer energies as well as compensation temperature and intrinsic enthalpy were also evaluated and the behaviors were comparable to other biological system.

关键词： Ciprofloxacin hydrochloride Sodium dodecyl sulfate Critical micelle concentration Thermodynamic indices Hydrophobic effect