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Synthesis of clay-supported nanoscale zero-valent iron using green tea extract for the removal of phosphorus from aqueous solutions

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Chinese Journal of Chemical Engineering 2017年第7期25卷 924-930页

作者： akbar soliemanzadeh Majid Fekri Department of Soil Sdence College of AgricultureShahid Bahonar University of KermanKermanlran

This study addresses the synthesis of nanoscale zero-valent iron(n ZVI) in the presence of natural bentonite(B-n ZVI) using green tea extract. The natural bentonite and B-n ZVI were then applied for the removal of phosphorus from aqueous solutions at various concentrations, p H levels and contact time. The desorption of phosphorus(P) from adsorbents was done immediately after sorption at the maximum initial concentration using the successive dilution method. The characterization of FTIR, SEM, and XRD indicated that n ZVI was successfully loaded to the surface of natural bentonite. The sorption of phosphorus on B-n ZVI was observed to be p H-dependent, with maximum phosphorus removal occurring at the p H range of 2 to 5. The results demonstrate that the maximum sorption capacities of natural bentonite and B-n ZVI were 4.61 and 27.63 mg·g^(-1), ***, Freundlich, and Redlich–Peterson models properly described the sorption isotherm data. For either adsorbent, desorption isotherms did not coincide with their corresponding sorption isotherms, suggesting the occurrence of irreversibility and hysteresis. The average percentages of retained phosphorus released from natural bentonite and B-n ZVI were 80% and 9%, respectively. The results indicated that sorption kinetics was best described by the pseudo-second-order model. The present study suggests that B-n ZVI could be used as a suitable adsorbent for the removal of phosphorus from aqueous solutions.

关键词： Green tea Nano zero-valent iron Natural bentonite Phosphorus Sorption

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Effects of green iron nanoparticles on iron changes and phytoavailability in a calcareous soil

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Pedosphere 2021年第5期31卷 761-770页

作者： akbar soliemanzadeh Majid FEKRI Department of Soil Science College of AgricultureShahid Bahonar University of KermanKerman ***(Iran)

Green iron nanoparticles(Fe NPs)can be a practical solution to combat iron(Fe)deficiency in calcareous agricultural *** main aim of the present work was to assess the effects of green Fe NPs on Fe availability in calcareous *** this purpose,green Fe NPs were synthesized using green tea(G-Fe NPs),Shirazi thyme(T-Fe NPs),walnut green hull(W-Fe NPs),and pistachio green hull(P-Fe NPs)extracts and applied as a source of Fe fertilizer to sorghum(Sorghum bicolor ***)*** of X-ray diffraction(XRD),scanning electron microscopy(SEM),and dynamic light scattering(DLS)indicated that the green Fe NPs were amorphous in nature and the polyphenols obtained from plant-part extracts acted as both capping and reducing *** to the behavior of Fe-ethylenediamine-N,N-bis(2-hydroxyphenyl)acetic acid(Fe-EDDHA)in calcareous soils,G-Fe NPs,T-Fe NPs,W-Fe NPs,and P-Fe NPs increased Fe release compared with the control and FeSO_(4) *** Fe release data fitted well to the power function,intra-particle diffusion,and Elovich kinetic *** to the pot experiment,the increment in soil Fe availability upon Fe-EDDHA and Fe NPs application led to an increase in Fe uptake,growth,and photosynthetic pigment contents of the sorghum *** further research is needed to evaluate the residual effect and environmental impact of green Fe NPs,they may be an appropriate substitute for traditional Fe fertilizers in calcareous soils.

关键词： chlorophyll content Fe fertilizer Fe release green chemistry natural polyphenols sorghum

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