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Fatty Acid Composition of Tobacco Seed Oil and Synthesis of Alkyd Resin

Chinese Journal of Chemistry 2007年第5期25卷 705-708页

作者： mukhtar, azam ULLAH, Habib mukhtar, Hamid Department of Chemistry University of Education Lahore Institute of Chemistry University of the Punjab Lahore 54600 Pakistan Institute of Industrial Biotechnology G C. University Lahore 54000 Pakistan

The fatty acid composition of tobacco seed oil revealed that the oil is rich in unsaturated fatty acids, having linoleic acid （71.63%）, oleic acid （13.46%） and palmitic acid （8.72%） as the most abundant unsaturated and saturated fatty acids respectively. So the tobacco oil was characterized as semi-drying type on the basis of fatty acid composition. The synthesis of alkyd resin was carried out by alcoholysis or monoglyceride process using an alkali refined tobacco seed oil, pentaerythritol, cis-1,2,3,6-tetrahydrophthalic anhydride along with lithium hydroxide as catalyst. The alkyd resin so prepared was found to be bright and of low color with high gloss. The drying and hardness properties and adhesion of the tobacco seed oil derived alkyd resin were also found a bit superior to those of other alkyd resins of the same oil length. In addition, the water and acid resistance of the said alkyd was also found comparable to the other alkyds.

关键词： tobacco oil alkyd fatty acid linoleic acid gloss and adhesion

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Synthesis,Crystal Structure and Spectroscopic Properties of 1,2-Benzothiazine Derivatives:An Experimental and DFT Study

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Chinese Journal of Structural Chemistry 2015年第1期34卷 15-25页

作者： MUHAMMAD Nadeem Arshad TARIQ Mahmood ATHER Faroque Khan MUHAMMAD Zia-Ur-Rehman ABDULLAH M.Asiri ISLAM Ullah Khan RIFFAT-Un-Nisa KHURSHID Ayub azam mukhtar MUHAMMAD Tariq Saeed Chemistry Department Faculty of ScienceKing Abdulaziz University Centre of Excellence for Advanced Materials Research (CEAMR) King Abdulaziz University Department of Chemistry COMSATS Institute of Information TechnologyAbbottabad IRCBM COMSATS Institute of Information Technology Applied Chemistry Research Center PCSIR Laboratories ComplexFerozpur RoadLahore 54600Pakistan Materials Chemistry Laboratory Department of ChemistryGC University Department of Chemistry College of ScienceKing Faisal University Department of Chemistry University of EducationOkara CampusOkara-Pakistan

1,2-Benzothiazine derivatives methyl 3-methoxy-4-oxo-3,4-dihydro-2H-benzo[e] [1,2]thiazine-3-carboxylate 1,1-dioxide（1） and methyl 2-ethyl-3-hydroxy-4-oxo-3,4-dihydro-2Hbenzo[e][1,2]thiazine-3-carboxylate 1,1-dioxide（2） were synthesized, and characterized by spectroscopic techniques; 1H-NMR and infrared（IR） spectroscopy. Crystals of 1 and 2 were grown by slow evaporation of methanol and ethyl acetate, respectively and their crystal structures were investigated by single-crystal X-ray diffraction analysis. Geometric properties were calculated by the B3 LYP method of density functional theory（DFT） at the 6-31G＋（d） basis set to compare with the experimental data. Simulated properties were found in strong agreement with the experimental ones. Intermolecular forces have also been modeled in order to investigate the strength of packing and strong hydrogen bonding was observed in both compounds 1 and 2. Electronic properties such as Ionization Potential（IP）, Electron Affinities（EA） and coefficients of the highest occupied molecular orbital（HOMO） and the lowest unoccupied molecular orbital（LUMO） of com- pounds 1 and 2 were simulated for the first time.

关键词： 1,2-benzothiazine B3LYP/6-31+G (d) density functional theory (DFT) HUMO-LUMO crystal structures

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In Vitro Synthetic Seed Production of Potato under Different Fungicide Levels and Storage Intervals

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Phyton-International Journal of Experimental Botany 2023年第8期92卷 2429-2450页

作者： Tahira Kalsoom Touqeer Ahmed Muhammad azam Khan Mirza Hasanuzzaman mukhtar Ahmed Stefaan P.O.Werbrouck Department of Horticulture PMAS-Arid Agriculture UniversityRawalpindi46300Pakistan Department of Agronomy Sher-e-Bangla Agricultural UniversityDhaka1207Bangladesh Department of Agronomy PMAS-Arid Agriculture UniversityRawalpindi46300Pakistan Department of Plants and Crops Ghent UniversityGhent9000Belgium

Potato propagation through tubers and seed is an inefﬁcient way of propagation thus we propose an alternative method in this study which is in vitro *** were raised from True Potato Seeds(TPS)in test tubes containing 10 mL of Murashige Skoog(MS)*** was done after every 21 days and after four subsequent subculturing,when there was an adequate quantity of stock material,uninodal cuttings of about 3-4 mm in length were prepared from in vitro proliferated potato plants by excising leaves of 1-2 mm on each side of the *** uninodal cuttings were cultured on 1/2 strength MS medium for root primordia *** selected uninodal cuttings with root primordia were encapsulated with sodium alginate solution(3.5%(w/v)),mixed with 1.25%charcoal and different concentration of fungicide(thiophanate methyl,sigma)to enhance the viability percentage of synthetic ***,these encapsulated uninodal cuttings were subjected to different storage intervals to check maximum *** showed that optimum dose for fungicide is 150 mg/L as it resulted in good viability percentage,shoot number,shoot length,rooting percentage,root number,root length and ideal for bead formation with sodium ***,results revealed that encapsulated uninodal cuttings can be stored at a temperature of 4℃ up to 45 days with a survival rate of 63.33%.Encapsulated uninodal cutting stored for 60 days showed a poor viability percentage of about 43.03%.It can be concluded that optimum dose of 150 mg/L with storage time of 45 days should be used to get a better outcome for synthetic potato seed production.

关键词： Synthetic seeds potato storage charcoal sodium alginate fungicide

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Major constraints on shisham(Dalbergia sissoo) plantations and pathological debate on dieback disease in Punjab,Pakistan

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Journal of Forestry Research 2015年第2期26卷 267-271页

作者： Irum mukhtar R.Bajwa G.Nasim Institute of Agricultural Sciences University of the PunjabQuiad-E-Azam CampusLahore 54590Pakistan

Today,shisham plantations in Punjab,Pakistan face major constraints,especially dieback *** article reviews the multidisciplinary team work by forest and plant pathologists and economists to resolve the confusions in the pathology of dieback *** is intended to be of practical use to the foresters and plant pathologists reporting on this issue.

关键词： Shisham Dieback disease Plantations Forest

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