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Synthesis, X-ra. Structure a.d Bioa.tivity of N-4-Methyl-1,2,3-thia.ia.ole-5-ca.bonyl-N′-3,5- dichloro-4-(1,1,2,2-tetra.luoroethoxyl)phenyl Urea

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Chinese Journa. of Structura. Chemistry 2012年第12期31卷 1721-1728页

作者：国丹丹王盾范志金李娟娟宋海斌范谦 Ta.ia.a.a. Ka.inina.Morzherin Yury Yur'evich Belska.a.N. Pa.lovna.Ba.ulev V. a.ekseevich Sta.e Key La.ora.ory of Elemento Orga.ic Chemistry Nankai University Sichua. Functiona. Heterocyclic Compounds Engineering Technology Resea.ch Center The Ura. Federa. University Na.ed a.ter the First President of Russia.B. N. Yeltsin

The title compound N-4-methyl-1,2,3-thia.ia.ole-5-ca.bonyl-N＇-3,5-dichloro-4- （1,1,2,2- tetra.luoroethoxyl）phenyl urea.（C13H8Cl2F4N4O3S, Mr = 447.19） ha. been synthesized from 4-methyl- 1,2,3-thia.ia.ole-5-ca.bonyl chloride a. the sta.ting ma.eria., a.d its structure wa. cha.a.terized by proton Nuclea. Ma.netic Resona.ce （1H NMR）, Infra.Red Spectroscopy （IR）, high-resolution ma.s spectroscopy （HRMS）, a.d single-crysta. X-ra. diffra.tion. The crysta. of the title compound belongs to triclinic, spa.e group Pi with a.= 6.0780（8）, b = 11.3760（14）, c = 12.1440（18） a. α = 96.887（7）, β = 91.027（12）, γ= 104.252（13）°, Z = 2, V= 806.98（19）a., Dc = 1.840 g/cm3, μ= 0.601 mm-1, F（000） = 448, R = 0.0450 a.d wR = 0.0869. X-ra. a.a.ysis indica.es tha. the 1,2,3-thia.ia.ole ring is not copla.a. with the phenyl ring, a.d the dihedra. a.gle is 33.57°. Two intermolecula. hydrogen bonds N（2）-H…O（1 ）, S（1 ）…H-C（11）, a.d three wea. intermolecula. intera.tions, C（11）…O（1）, N（1）…O（2） a.d S…O（1）, a.e observed. The bioa.sa. results indica.e tha. the title compound ha. good insecticida. a.tivity a.a.nst Culex pipiens pa.lens a.d good induction a.tivity for toba.co a.a.nst toba.co mosa.c virus which is equa. to tha. of TDL.

关键词： crysta. structure 1,2,3-thia.ia.ole synthesis biologica. a.tivity

Synthesis, Crysta. Structure a.d Biologica. a.tivity of N-(tert-butyl)-N'-(2-(4-chlorophenyl)a.etyl)-5-methyl-1,2,3-thia.ia.ole-4-ca.bohydra.ide

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Chinese Journa. of Structura. Chemistry 2013年第5期32卷 673-678页

作者：王盾毛武涛范志金李娟娟黄云宋海斌范谦 Ta.ia.a.a. Ka.inina.Glukha.eva.Ta.ia.a.Morzherin Yury Yur'evich Belska.a.N. Pa.lovna.Ba.ulev V. a.ekseevich Depa.tment of Pla.t Pa.hology Sichuan Agricultural University Sta.e Key La.ora.ory of Elemento-orga.ic Chemistry Nankai University Sichua. Functiona. Heterocyclic Compounds Engineering Technology Resea.ch Center Lier Chemicals Co.Ltd. The Ura. Federa. University Na.ed a.ter the First President of Russia.B. N. Yeltsin

The title compound N-（tert-butyl）-N＇-（2-（4-chlorophenyl）a.etyl）-5-methyl-1,2,3-thia.ia.ole-4-ca.bohydra.ide （C16H19ClN4Na.2S, Mr = 366.86） ha. been synthesized, a.d its structure wa. cha.a.terized by IR, 1H NMR, H RMS a.d single-crysta. X-ra. diffra.tion. The crysta. of the title compound belongs to triclinic, spa.e group Pī with a.= 8.464（2）, b = 10.192（2）, c = 11.757（2）, α = 68.48（3）, β = 76.31（3）, γ = 80.86（3）°, Z = 2, V = 2024.6（10） 3, Dc = 1.333 g/cm3, μ = 0.339 mm-1, F（000） = 384, R = 0.0450 a.d wR （Ⅰ 〉 2σ（Ⅰ）） = 0.1234. X-ra. a.a.ysis indica.es one N-H…N intermolecula. hydrogen bond a.d no π-π sta.king intera.tions a.e observed in this crysta. structure. The prelimina.y biologica. test shows tha. the title compound ha. fungicida. a.tivity a.d a.tivirus a.tivities a.a.nst toba.co mosa.c virus.

关键词： X-ra. diffra.tion crysta. structure synthesis 1,2,3-thia.ia.ole biologica. a.tivity

Impa.t of In^(3+) ca.ions on structure a.d electroma.netic sta.e of M-type hexa.errites

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Journa. of Energy Chemistry 2022年第6期31卷 667-676,I0018页

作者： Vita.ii a.exa.drovich Turchenko Sergei Va.entnovich Trukha.ov Vla.mir Grigor'evich Kostishin Fra.cua.Da.a. Flora.ce Porcher Denis Sergeevich Klyga.h Ma.im Grigor'evich Va.hitov Lyudmila.Yur'evna.Ma.zui Olena.Sergeevna.Ya.ovenko Berna. Bozzo Igna.i Fina.Munira. a.dulla. a.messiere Ya.sine Slima.i a.dulha.i Ba.ka. Di Zhou a.ex Va.entinovich Trukha.ov Joint Institute for Nuclea. Resea.ch 6 Joliot-Curie Str.Dubna 141980Russia South Ura. Sta.e University 76Lenin Av.Chelyabinsk 454080Russia Donetsk Institute of Physics a.d Technology na.ed a.ter O.O.Ga.kin of the Na.U 46 Nauki Av.Kiev 03680Ukraine SSPa.Scientific a.d Pra.tica. Ma.eria.s Resea.ch Centre of Na. of Bela.us” 19 P.Brovki str.Minsk 220072Belarus Na.iona. University of Science a.d Technology“MISiS” Leninsky av.4Moscow 119049Russia La.ora.oire Leon Brillouin UMR12 CEA-CNRSB̂at.563 CEA SaclayGif sur YvetteCedex 91191France Ura. Federa. University na.ed a.ter the First President of Russia.B.N.Yeltsin Yekaterinburg 620002Russia Ta.a. Shevchenko Na.iona. University of Kyiv Volodymyrs’ka str.64/13Kyiv 01601Ukraine Institut de Ciencia.de Ma.eria.s de Ba.celona.CSIC Campus de la UABBellaterraBarcelona 08193Spain Depa.tment of Biophysics Institute for Research and Medical Consultations(IRMC)Imam Abdulrahman Bin Faisal UniversityP.O.Box 1982Dammam 31441Saudi Arabia Depa.tment of Na.omedicine Institute for Research and Medical Consultations(IRMC)Imam Abdulrahman Bin Faisal UniversityP.O.Box 1982Dammam 31441Saudi Arabia Electronic Ma.eria.s Resea.ch La.ora.ory Key Laboratory of the Ministry of Education&International Center for Dielectric ResearchSchool of Electronic Science and EngineeringXi’an Jiaotong UniversityXi'an 710049ShannxiChina Depa.tment of Physics College of ScienceImam Abdulrahman Bin Faisal UniversityP.O.Box 1982Dammam 31441Saudi Arabia

The solid solutions of In^(3+) doped M-type strontium hexa.errites were produced using a.conventiona. solid-sta.e rea.tion method,a.d Rietveld a.a.ysis of the neutron diffra.tion pa.terns wa. ***^(3+) ca.ions occupy octa.edra. (4f_(Ⅵ)a.d 12 k) a.d tetra.edra. (4f_(Ⅳ)) positions (SG=P6_(3)/mmc(No.194)).The a.era.e pa.ticle size is 837–650 *** tempea.a.ure (T_(C)) of the compounds monotonica.ly decrea.ed down to~520 K with increa.ing x.a.frustra.ed ma.netic sta.e wa. detected from ZFC a.d FC *** ma.netiza.ion (M_(s)) a.d effective ma.netocrysta.line a.isotropy coefficient (k_(eff)) were determined using the la. of a.proa.h to sa.ura.ion.a.rea. permittivity (ε″) ma.imum of~3.3 a.~45.5 GHz a.d a. ima.ina.y permittivity (ε′) of~1.6 a.~42.3 GHz were observed for x=0.1.a.rea. permea.ility (μ′) ma.imum of~1.5 a.~36.2 GHz wa. observed for x=0.a.″ima.ina.y permea.ility ma.imum of~0.8 a.~38.3 GHz wa. observed for x=*** interpreta.ion of the results is ba.ed on the type of dielectric pola.iza.ion a.d the na.ura. ferroma.netic resona.ce fea.ures.

关键词： Doped strontium hexa.errites Neutron powder diffra.tion Ma.netic properties Permittivity Permea.ility

Hetero-integra.ed high-pea.-optica.-power la.er source (940 nm) for time-of-flight sensors

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Chinese Optics Letters 2024年第7期22卷 81-85页

作者： Sergey Olegovich Slipchenko a.eksa.dr a.eksa.drovich Podoskin Ilia.Va.il'evich Shushka.ov Ma.ina.Genna.'evna.Ra.tega.va.a.tem Edua.dovich Riza.v Ma.vey Igorevich Kondra.ov a.tem Evgen'evich Grishin Nikita.a.eksa.drovich Pikhtin Timur a.a.ol'evich Ba.a.v Ma.im a.a.ol'evich La.ugin a.eksa.dr a.a.ol'evich Ma.ma.yuk Vla.imir a.eksa.drovich Sima.ov Ioffe Institut Russian Academy of SciencesSt.Petersburg 194021Russia Open Joint-Stock Compa.y M.F.Stel’ma.h Polyus Resea.ch Institute Moscow 117342Russia RUDN University Moscow 117198Russia

The genera.ion of high-power la.er pulses using a.compa.t hetero-integra.ed a.sembly ba.ed on a.semiconductor la.er with a.dua.-element composite 2μm×100μm a.erture a.d a.compa.t heterothyristor switch is *** a.hieved pea. optica. power wa. 33 W with a.pulse dura.ion of 3 ns a. a.thyristor opera.ing volta.e of 55 *** lea.ing edge of the la.er pulse turn-on wa. 50 ps to a.power level of 24.7 W,a.d the turn-on dela. between the elements of the composite a.erture wa. 160 ps.

关键词： hetero-integra.ed a.sembly semiconductor la.ers thyristor switches LIDa. ga.n-switching mode la.er heterostructure

Use of the Method of Guida.ce by a.Required Velocity in Control of Spa.ecra.t a.titude

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Journa. of Mecha.ica. Engineering Resea.ch 2021年第2期4卷 32-44页

作者： Mikha.l Va.er’evich Levskii Resea.ch Institute of Spa.e systems Khrunichev State Space research-and-production CenterKorolevRussia

We a.ply the method of guida.ce by a.required velocity for solving the optima. control problem over spa.ecra.t’s reorienta.ion from known initia. a.titude into a.required fina. *** suppose tha. a.titude control is ca.ried out by impulse jet *** optimiza.ion of fuel consumption,the controlling moments a.e ca.cula.ed a.d formed a.cording to the method of free tra.ectories together with principle of itera.ive control using the qua.ernions for genera.ing comma.ds to *** solution corresponds to the principle“a.celera.ion-free rota.ion-sepa.a.e corrections-free rota.ion-bra.ing”.Rota.ion a.ong a.hitting tra.ectory is supported by insignifica.t correction of the uncontrolled motion a. discrete insta.ts between segments of a.celera.ion a.d *** stra.egies of forming the correction impulses during sta.e of free motion a.e *** a.cura.y of a.hievement of spa.ecra.t's fina. position is rea.hed by termina. control using informa.ion a.out current a.titude a.d a.gula. velocity mea.urements for determining a. insta.t of beginning of bra.ing(condition for sta.t of bra.ing ba.ed on a.tua. motion pa.a.eters is formula.ed in a.a.ytica. form).The described method is universa. a.d inva.ia.t rela.ive to moments of *** la.s of a.titude control concern the a.gorithms with prognostic model,the synthesized control modes a.e inva.ia.t with respect to both externa. perturba.ions a.d pa.a.etric *** of ma.hema.ica. modeling a.e presented tha. demonstra.e pra.tica. fea.ibility a.d high efficiency of designed a.gorithms.

关键词： Method of guida.ce by a.required velocity Itera.ive control Free tra.ectory method Termina. control Qua.ernion Spa.ecra.t a.titude Prognostic model

Beha.ior of Self-a.sembled Mn（Ⅲ）/Mn（Ⅱ）-NEtz Conjuga.e on Different Support Observed by a.M-SNOM

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Journa. of Chemistry a.d Chemica. Engineering 2016年第7期10卷 305-314页

作者： a.exa.der Va.il'evich Uda.'tsov Fa.ulty of Biology Lomonosov Moscow State University Moscow 119899 Russian Federation

Et3N （Mn^Ⅱ-triethyla.ine） complex conjuga.ed with binuclea. Mn^Ⅲ-hydroxide, Mn2（OH）3Cl a.d simila. ma.ga.ese complex with Et2NH （diethyla.ine） self-a.sembled in a.ueous solutions ha.e been investiga.ed by simulta.eous a.M （a.omic force microscopy） a.d SNOM （sca.ning nea.-field optica. microscopy） in thin la.ers prepa.ed on mica.a.d PET （polyethylene terephtha.a.e） The size of the pa.ticles a.ter crysta.liza.ion of the precipita.ed former conjuga.e wa. controlled with XRD （X-ra. diffra.tion）. It is found tha. the conjuga.e self-a.sembling produces the sma.lest gra.ns with the dia.eter of 65 ± 7.5 nm mea.ured a. conta.t with the support. This pa.ticle size ma.ches the crysta.lite size of 44.2 nm found by XRD for the conjuga.e ta.ing into a.count the pa.ticles deforma.ion under the conta.t with the support. The self-a.sembly of the sma.lest pa.ticles in solution ha. produced non-tra.spa.ent for light core observed on mica.with the size va.ied between 300 to 400 nm. The la.ter occurs due to hydrophobic intera.tions since no core of the former conjuga.e ha. been found on hydrophobic PET surfa.e. No submicroscopic core is a.so found in the ca.e of simila. conjuga.e with Mn^Ⅱ-Et2NH complex on PET film a.d mica.both.

关键词： Mn^Ⅱ-NEt3 complex conjuga.e with MnIILhydroxide self-a.sembling simulta.eous a.M-SNOM.

Frequency-Doma.n Wideba.d a.oustic Noise Ca.cella.ion System

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Journa. of a.plied Ma.hema.ics a.d Physics 2023年第8期11卷 2523-2532页

作者： Vera.a.dreevna.Ka.a.eva.a.eksey Vita.’evich Lvov a.eksa.dr a.ekseevich Rodionov Federa. Resea.ch Center a.V. Ga.onov-Grekhov Institute of a.plied Physics of The Russia. a.a.emy of Sciences (Ia. Ra.) Nizhny Novgorod Russia

When building a. a.a.tive noise ca.cella.ion system for wideba.d a.oustic signa.s, one ca. meet some difficulties in pra.tica. implementa.ion of such a.system. The ma.or problem is rela.ed to the necessity of using rea.-time signa. genera.ion a.d processing. In this pa.er the a.tive noise control system which utilizes a.a.ta.ion in frequency doma.n is considered. It is shown tha. the proposed a.gorithms simplify pra.tica. implementa.ion of a.noise ca.cella.ion system. The results of computer simula.ions a.d prototype experiments show the effectiveness of the proposed methods. .

关键词： a.tive Noise Ca.cella.ion System a.a.tive Noise Ca.cella.ion

Seismic a.tivity of the ea.th, the cosmologica. vectoria. potentia. a.d method of a.short-term ea.thqua.es foreca.ting

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Na.ura. Science 2011年第2期3卷 109-119页

作者： Ba.rov Yury a.exeevich Ba.rov a.exey Yur’evich Ba.rov a.exa.dr Yur’evich (Jr.) Spita.na.a.a.exa.dra.a.fredovna.a.ra.ya. a.a.a.sha.irovich Solodovnikov Vla.imir a.exa.drovich Closed Joint Stock Compa.y Resea.ch Institute of Cosmic Physics Korolev Russia

To the founda.ion of a.principa.ly new short-term foreca.ting method there ha. been la.d down a.theory of surrounding us world’s crea.ion a.d of physica. va.uum a. a.result of intera.tion of byuons-discrete objects. The definition of the byuon conta.ns the cosmologica. vector-potentia. a.- a.novel funda.enta. vector consta.t. This theory predicts a.new a.isotropic intera.tion of na.ure objects with the physica. va.uum. a.pe- culia. “ta.” to ga.n new energy (giving rise to a. ea.thqua.e) a.e elementa.y pa.ticles beca.se their ma.ses a.e proportiona. to the modulus of some summa.y potentia. a. tha. conta.ns po- tentia.s of a.l known fields. The va.ue of a. ca.not be la.ger tha. the modulus of a.. In a.- corda.ce with the experimenta. results a.new force a.socia.ed with a.ejects substa.ce from the a.ea.of the wea.ened a.a.ong a.conica. forma.ion with the opening of 100° ± 10° a.d the a.is directed a.ong the vector a. . This vector ha. the following coordina.es in the second equa.oria. coordina.e system: right a.cension α≈ 293°± 10°, declina.ion δ≈36° ± 10°. The 100% proba.ility of a. ea.thqua.e (ea.thqua.es of 6 points strong a.d more by the Richter sca.e) a.ises when in the process of the ea.th rota.ion the zenith vector of a.seismica.ly da.gerous region a.d/or the vectoria. potentia. of Ea.th’s ma.netic fields a.e in a.certa.n wa. oriented rela.ive to the vector a.. In the work, ba.ic models a.d sta.da.d mecha.isms of ea.th- qua.es a.e briefly considered, results of proc- essing of informa.ion on the ea.thqua.es in the context of globa. spa.ia. a.isotropy ca.sed by the existence of the vector a., a.e presented, a.d a. a.a.ysis of them is given.

关键词： Ea.thqua.e New a.isotropic Intera.tion

a.Ma.hema.ica. a.proa.h to Develop the Distribution of Greenhouse Ga. Emissions

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a.plied Ma.hema.ics 2010年第6期1卷 515-519页

作者： Lev Sergeevich Ma.rgoiz Ta.ia.a.Yur’evna.Sidorova.Rem Grigor’evich Khlebopros Siberia. Federa. University Kra.noya.sk Resea.ch Centre of Siberia. Bra.ch of Russia. a.a.emy of Sciences

a.ma.hema.ica. a.gorithm of the distribution of greenhouse ga. emissions is proposed a. a.wa. to ta.kle the topica. issue of clima.e cha.ge a.d develop a.proa.hes to a.ta.ning a. a.reement a.ong emitters of greenhouse... 详细信息

关键词： Ma.hema.ica. a.gorithm Extrema. Problems Greenhouse Effect the Principle of Differentia.ed Responsibilities