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science china(Technological sciences) 2005年第5期48卷 510-520页

作者： SU Juanhua1,2. LIU Ping2. DONG Qiming2.& LI Hejun1 1. College of materials science and {2., Northwestern Polytechnical university, Xi’an 710072. china 2. College of materials science and {2., Henan university of science and technology, Luoyang 471003, china 1. College of materials science and {2. Northwestern Polytechnical University 710072 Xi’an China 2. College of materials science and {2. Henan University of Science and Technology 471003 Luoyang China

The thermomechanical treatment process is effective in enhancing the properties of the lead frame copper alloy. In this study, an optimal pattern of the thermomechanical processes for Cu-Cr-Zr was investegated using an intelligent control technique consisting of neural networks and genetic algorithms. The input parameters of the artificial neural network (ANN) are the reduction ratio of cold rolling, aging temperature and aging time. The outputs of the ANN model are the two most important properties of hardness and conductivity. Based on the successfully trained ANN model, genetic algorithms (GA) are used to optimize the input parameters of the model and select perfect combinations of thermomechanical processing parameters and properties. The good generalization performance and optimized results of the integrated model are achieved.

关键词： Cu-Cr-Zr alloy, thermomechanical processing optimization, artificial neural network, genetic algorithms.

Large-eddy simulations and vortex structures of turbulent jets in crossflow

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science china(Physics,Mechanics & Astronomy) 2007年第1期50卷 118-132页

作者： GUAN Hui1,2.& WU ChuiJie2.1 school of Mechanical and Power engineering,{2.,shanghai 2.02.7,china 2.Research Center for Fluid Dynamics,PLA university of science and technology,Nanjing 2.1101,china 1. school of Mechanical and Power engineering East China University of Science and Technology Shanghai 200237 China 2. Research Center for Fluid Dynamics PLA University of Science and Technology Nanjing 211101 China

Using the method of large-eddy simulation, the 3-dimensional turbulent jets in crossflow with stream-wise and transverse arrangements of nozzle are simulated, emphasizing on the dynamical process of generation and evolution of vortex structures in these flows. The results show that the basic vortex structures in literatures, such as the counter-rotating vortex pair, leading-edge vortices, lee-side vortices, hanging vortices, kidney vortices and anti-kidney vortices, are not independent physical substances, but local structures of the basic vortex structure of turbulent jets in crossflow-the 3-D stretching vortex rings originating from the orifice of the nozzle, which is discovered in this study. Therefore, the most important large-scale structures of turbulent jets in crossflow are unified to the 3-D vortex rings which stretch and twist in stream-wise and swing in transverse directions. We also found that the shedding frequencies of vortex rings are much lower than the one corresponding to the appearance of leading-edge and lee-side vortices in the turbulent jets.

关键词： turbulent jet in crossflow coherent structure large-eddy simulation

Phase transition in the Zr_(60)Al_(15)Ni_(2.) bulk metallic glass subjected to rolling at room temperature

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science china(Technological sciences) 2006年第6期49卷 655-662页

作者： YAN Zhijie1, 2. LI Jinfu1, ZHOU Yaohe1 & WU Yanqing3 1. State Key Laboratory of Metal Matrix Composites, school of materials {2. and engineering, shanghai Jiao Tong university, shanghai 2.0030, china 2. school of materials {2. and engineering, Taiyuan university of {2. and technology, Taiyuan 03002., china 3. school of Environmental {2. and engineering, shanghai Jiao Tong university, shanghai 2.0030, china State Key Laboratory of Metal Matrix Composites School of Materials Science engineering Shanghai Jiao Tong University Shanghai 200030 China school of materials {2. engineering Taiyuan University of Science technology Taiyuan 030024 China school of Environmental science engineering Shanghai Jiao Tong University Shanghai 200030 China

The microstructure evolution of the Zr60Al15Ni2. metallic glass during rolling at room temperature is investigated by X-ray diffraction (XRD), differential scanning calorimetry (DSC); high-resolution transmission electron microscopy (HREM). The results show that the values of full width at half maximum (FWHM) of the XRD patterns; exothermic enthalpy ΔH of DSC plots do not monotonically change with the variation of deformation degrees . As is not large than 2.%, the values of FWHM; ΔH are lower than that of the as-cast state. When reaches 30%, the values of FWHM; ΔH become larger than that of the as-cast state, while their values begin to decrease again as reaches about 85%. These results indicate that the reversible transitions between ordered; disordered atomic configurations occur during rolling, which is further verified by the HREM images. The reversible phase transition can be explained by the competition between the diffusion controlled reordering; shear-induced disordering during rolling.

关键词： metallic glasses, plastic deformation, phase transformations, shear bands.

Surface Nanocrystallization of Magnesium Alloy AZ91D by High-Energy Shot Peening

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Journal of Wuhan university of technology({2. science) 2009年第4期24卷 515-519页

作者：张津 school of materials {2. & engineering University of Science and Technology Beijing College of materials science & {2. Chongqing University of Technology

High-energy shot peening （HESP）, a method to produce severe plastic deformation by high velocity flying balls, was applied on die cast magnesium alloy AZ91D. Effects of surface nanocrystallization by HESP and heat treatment at different temperatures were investigated. The mi- crostructure evolution was conducted using X-ray diffraction （XRD） and field emission scanning electronic microscopy （FESEM）. The hardness was measured by microhardness tester. The experimental results show that surface nanocrystrallization of AZ91D obtained by HESP would lead to the increase of microhardness. Low temperature heated at 100℃ for 1 h do not change the property obviously. However, both the microstructure and microhardness vary greatly after heat treatment at 400℃ for 1 h.

关键词： AZ91 D surface nanocrystallization HESP microhardnss corrosion resistance

Chemical Extraction Preparation of Delithiated Cathode materials of Li-ion Battery

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Journal of Wuhan university of technology({2. science) 2009年第6期24卷 863-866页

作者：闫时建 school of materials {2. and engineering Taiyuan University of Science and Technology

A method of conventional chemical reaction to prepare delithiated cathode materials of Li-ion battery was introduced. The cathode material of Li-ion battery was mixed with oxidizing agent Na2.2.8 in water solution, and the solution was stirred continuously to make the chemical reaction proceed sufficiently, then the reaction product was filtered and finally the insoluble delithiated cathode material was obtained. A series of tests were conducted to verify the composition, crystal structure and electrochemical property of the delithiated cathode materials were all desirable. This method overcomes the shortcomings of battery charging preparation and chemical extraction preparation employing other oxidizing agents.

关键词： chemical extraction delithiated cathode material Li-ion battery

Early Age Compressive Strength of Pastes by Electrical Resistivity Method and Maturity Method

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Journal of Wuhan university of technology({2. science) 2011年第5期26卷 983-989页

作者：肖莲珍 school of materials {2. and engineering Wuhan Institute of Technology

The compressive strength development of Portland cement pastes was investigated by the electrical resistivity method and the maturity *** experiments were carried out on the cement pastes with different water-cement ratios at different curing *** results show that the application of the maturity method has limitation to obtain the *** is found that both of the compressive strength and the electrical resistivity follow hyperbolic trend for all the *** hyperbolic equation of each mix is obtained to estimate the ultimate resistivity value which can probably be *** relationship between electrical resistivity and compressive strength of the cement pastes is established based on the test results and interpreted by the empirical Archie equation and a strength-porosity *** relationship between the electrical resistivity after temperature correction and the compressive strength was linear and independent of curing temperature and water-cement ratio.

关键词： electrical resistivity cement hydration compressive strength maturity method

Study on rare earth/alkaline earth oxide-doped CeO_2.solid electrolyte

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Rare Metals 2007年第4期26卷 311-316页

作者： YAN Kai ZHEN Qiang Song Xiwen school of materials {2. and engineering Shanghai University Shanghai 200072 China Research Center of Nanoscience and Nanotechnology Shanghai Univeesity Shanghai 200444 China school of materials {2. and engineering Inner Mongolia University of Science and Technology B aotou 014010 China

Five types of rare earth/alkaline earth oxide-doped CeO2.superfine-powders were synthesized by a low-temperature combustion technique. The relevant solid electrolyte materials were also sintered by pressureless sintering at different temperatures. The results of X-ray diffraction and transmission electron microscopy showed that the grain size of the powders was approximately 2.-30 nm, and rare earth/alkaline earth oxides were completely dissolved into ceria-based solid solution with fluorite structure. The electrical conductivities of the SmzO3-CeO2.system were measured by the ac impedance technique in air at temperatures ranging from 513-900℃. The results indicated that the ionic conductivities of Srno.2.Ce0.8Ol.875 solid electrolyte increase with increasing sintering temperature, and the relationship between the conductivities and measuring temperature obeys the An＇henius equation. Then the SmzO3-CeO2.material was further doped with other rare earth/alkaline earth oxide, and the conductivities improve with the effective index.

关键词： doped ceria rare earth/alkaline earth oxide solid electrolyte conductivity effective index

Preparation of semi-solid AlSi7Mg alloy slurry with big capability

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Rare Metals 2010年第6期29卷 642-645页

作者： LI Sha and MAO Weimin school of materials {2. and engineering,university of {2. and technology Beijing,Beijing 100083,china school of materials {2. and engineering University of Science and Technology Beijing Beijing China

Semi-solid AlSi7Mg alloy slurry was prepared by low superheat pouring and weak traveling-wave electromagnetic *** effects of pouring temperature and stirring power on the microstructure of AlSi7Mg alloy slurry were *** results show that the semi-solid AlSi7Mg alloy slurry of 5 kg can be *** new technology can save energy and make the pouring process *** the pouring temperature is decreased at a stirring power of 0.41 kW,the shape of primary α-Al grains gradually changes from dendritic-like to *** the alloy melt is poured at the temperature（630°C） with a certain superheat,the pouring process becomes easier,and the spherical microstructure of AlSi7Mg alloy slurry can be prepared by the weak traveling-wave electromagnetic *** the pouring temperature is 630°C,increasing the stirring power appropriately can result in better spherical primary α-Al grains,but if the stirring power is increased to a certain value（1.72.kW）,the shape of primary α-Al grains does not obviously improve when the stirring power is continually increased.

关键词： aluminum alloys metal forming semisolid slurry electromagnetic stirring microstructure

Synthesis and Lubrication of Phosphorylcholine Derivative

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Journal of Bionic engineering 2010年第3期7卷 254-258页

作者： Zhenliang Qiao~1, Dangsheng Xiong~1, Lude Lu~2. Pengju Jiang~2.1. Department of materials science and {2., Nanjing university of science and technology, Nanjing 2.0094, P.R. china 2. school of Chemical {2., Nanjing university of science and technology, Nanjing 2.0094, P. R. china [a] Department of materials science engineering Nanjing University of Science technology Nanjing 210094 P.R. China [b] School of Chemical Engineering Nanjing University of Science technology Nanjing 210094 P. R. China

The monomer of phosphorylcholine derivative, O-(5-（2.methacryloxy）-3, 3-dimethyl-3-azapentyl)-O’-（ω-hydroxy-octyl）-phosphatequaternary ammonium salt, was designed and synthesized successfully. It was characterized by the spectra ofHNMR and Mass spectra （ESI+）, and every signal was assigned. Then the lubricating characteristics of the phosphorylcholinederivative were investigated on the tribological setup of ball-oh-flat. The Ultra-High Molecular Weight Polyethylene（UHMWPE） flat was rotated against a stainless steel ball with 6 mm diameter. The load was 2.3 N, which corresponded to amaximal Hertz contact pressure of 2. MPa. Water, phosphorylcholine derivative, and Acrylic Acid （AA） solution were used aslubricants, respectively. Compared with AA, the phosphorylcholine derivative shows significant lubrication. It can be stronglyhydrated under water due to the charged segment in chemical structure. The thick water layers within the chains serves asboundary lubricants, and this is thought to be the molecular origins of lubricating behavior.

关键词： artificial joint articular cartilage molecular lubrication mechanism phosphorylcholine synthesis UHMWPE

Dynamic damage and stress-strain relations of ultra-high performance cementitious composites subjected to repeated impact

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science china(Technological sciences) 2010年第6期53卷 1520-1525页

作者： LAI JianZhong1 & SUN Wei2.1 Department of materials science and {2.,Nanjing university of science and technology,Nanjing 2.0094,china 2.College of materials science and {2.,Southeast university,Nanjing 2.1189,china 1. Department of materials science and {2. Nanjing University of Science and Technology Nanjing 210094 China2. College of Materials Science and Engineering Southeast University Nanjing 211189 China

Ultra-high performance cementitious composites (UHPCC) were prepared by replacing 60% of cement with ultra-fine industrial waste *** dynamic damage and compressive stress-strain relations of UHPCC were studied using split Hopkinson pressure bar (SHPB).The damage of UHPCC subjected to repeated impact was measured by the ultrasonic pulse velocity *** show that the dynamic damage of UHPCC increases linearly with impact times and the abilities of repeated impact resistance of UHPCC are improved with increasing fiber volume *** stress waves on impact were recorded and the average stress,strain and strain rate of UHPCC were calculated based on the wave propagation *** effects of strain rate,fibers volume fraction and impact times on the stress-strain relations of UHPCC were *** show that the peak stress and elastic modulus decrease while the strain rate and peak strain increase gradually with increasing impact times.

关键词： ultra-high performance cementitious composites (UHPCC) split Hopkinson pressure bar (SHPB) repeated impact damage stress-strain