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Binding Materials of Dehydrated Phases of Waste Hardened Cement Paste and Pozzolanic Admixture

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Journal of wuhan University of technology(Materials {2.) 2009年第1期24卷 140-144页

作者：吕林女 School of science Wuhan University of Technology

Fly ash （FA） and ground granulated blast-furnace slag （GGBFS） were added to improve the performances of regenerated binding materials （RBM） which refer to dehydrated phases with rebinding ability of waste hardened cement paste. Flowability tests, compressive strength tests, SEM, TG-DSC, and non-evaporable water content tests were employed to study the performances of the combined binding materials and the interactions between RBM, FA, and GGBFS. Results show that adding FA or GGBFS can improve the workability of RBM paste, and GGBFS has positive effects on strength of RBM. Pozzolanic reactions happen between RBM, FA, and GGBFS. And the activation effect of RBM to FA and GGBFS is superior to that of P.O grade-32.5 cement, especially at earlier ages, because of the high reactive f-CaO existing in RBM. On the advantages of the synergetic effects of RBM and pozzolanic admixtures such as FA and GGBFS, new combined binding materials can be prepared by blending them together.

关键词： combined binding materials dehydrated phase fly ash granulatedblast-furnace slag

Preparation and Characterization of Chitosan/Carboxymethylated Konjac Glucomannan Blend Films

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wuhan University Journal of Natural sciences 2002年第1期7卷 107-112页

作者： Zheng Hua 1 , Du Yu-min 2.1. Department of Chemical Engineering, wuhan University of technology, {2., Hubei, china 2. College of Chemistry and Molecular sciences, wuhan University, wuhan 430072. Hubei, china Department of Chemical Engineering Wuhan University of Technology Wuhan Hubei China College of Chemistry and Molecular sciences Wuhan University Wuhan Hubei China

In order to improve the mechanical and water swelling properties of the chitosan (CS) film, a series of transparent films were prepared by blending 2.(weight) chitosan acetic acid solution with 1.5%(weight) carboxymethylated konjac glucomannan (CMKGM) aqueous solution according to predetermined ratio and drying at 30°C. The morphological structure, miscibility, thermal stability, mechanical properies, and swelling capacity of the blend films were studied by infrared (IR), X-ray diffraction (XRD), differential thermal analysis (DTA), scanning electron micrograph (SEM), and measurements of the mechanical properties and swelling properties. The results demonstrated that there was strong interaction and good miscibility between CS and CMKGM resulted from intermolecular hydrogen bonding and electrostatic force. The mechanical properties in dry state and wet state, thermostability, and water swelling properties of the blend films were obviously improved. The best values of the tensile strength in the dry and wet state achieved 89 MPa and 49 MPa, respectively, when the CMKGM content was 30%(weight). The CS/ CMKGM blend films provided promising biomedical applications.

关键词： Key words chitosan carboxymethylated konjac glucomannan blend films structure characterization

Fabrication and Characterization of Nano Silver Powder Prepared by Spray Pyrolysis

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Journal of wuhan University of technology(Materials {2.) 2009年第6期24卷 871-874页

作者：章桥新 School of Mechanical and Electronic Engineering Wuhan University of Technology State Key Laboratory of Advanced technology for Materials Synthesis & Processing Wuhan University of Technology

Silver powder was fabricated by spray pyrolysis, using 2.-2.% AgNO3 solution, 336-500 mL/h flux of AgNO3 solution, 0.2.-0.32.MPa flux of carrier gas and in the 62.-82. ℃ temperature range. The effects of furnace set temperature, concentration of AgNO3 aqueous solution, flux of AgNO3 aqueous solution as well as carrier gas on the morphology and particle size distribution of silver powder, were investigated. The experimental results showed that with the high concentration of AgNO3 aqueous solution, the average grain size of silver decreased with the increasing of furnace set temperature. But the gain size distribution was not homogenous, the discontinuous grain growth occurred. With the low concentration of AgNO3 aqueous solution, the higher furnace set temperature made the nano sliver grains sintered together to grow. Nano silver powder about 100 nm was fabricated by spray pyrolysis, using 2.t% AgNO3 solutions, 336 mL/h flux of AgNO3 aqueous solution, 0.32.MPa flux of carrier gas at 72. ℃ furnace set temperature.

关键词： nano silver powder fabrication characterization spray pyrolysis

Evaluation of a Novel Bioabsorbable PRGD/PDLLA/β-TCP/NGF Composites in Repair of Peripheral Nerves

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Journal of wuhan University of technology(Materials {2.) 2009年第3期24卷 409-414页

作者：王永红李世普 Hospital Wuhan University of Technology Biomedical Materials and Engineering Research Center Wuhan University of Technology

Peripheral nerve regeneration using a novel nerve conduit （PRGD/PDLLA/β TCP/NGF） was evaluated, which was made of RGD peptide modified poly{（lactic acid）-co-[（glycolic acid）-alt-（L-lysine）]} （PRGD）, poly（d,l-lactic acid）（PDLLA） and β-tricalcium phosphate （β-TCP）. And the effectiveness was compared with that of PRGD/PDLLA/β-TCP, PDLLA and autograft in terms of nerve regeneration across a gap. Both of biodegradablity and cell-biocompatibility of the novel nerve conduit were evaluated in vitro. The results show that PRGD/PDLLA/β-TCP/NGF composite ma terials have better biodegradation properties and cell affinity than PDLLA, and could promote the RSC96 Schwann cells adhesion, proliferation and growth on the surface of materials. PRGD/PDLLA/ β-TCP/NGF composite conduit was significantly superior to that of the PDLLA conduit in histological and axon morphologic index. PRGD/PDLLA/β-TCP/NGF conduit is more beneficial to nerve regeneration than PDLLA conduit. The biodegradable PDLLA/PRGD/β-TCP/NGF conduit has a good biocompatibility with rats tissue and it could effectively promote the nerve regeneration after bridging sciatic nerve defect of rats, the effect is as good as that of the autograft nerve, significantly superior to the PRGD/PDLLA/β-TCP conduit and PDLLA conduit. PDLLA/PRGD/β-TCP/NGF composite conduit is a potential ideal conduit.

关键词： peripheral nerve nerve conduit PDLLA/PRGD/β-TCP/NGF composite regeneration

The Role of Calcium in Microstructural Refinement of AZ91 Magnesium Alloy

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Journal of wuhan University of technology(Materials {2.) 2006年第4期21卷 45-47页

作者：刘生发 School of Materials science and Engineering Wuhan University of Technology Wuhan 430070China

The effect of calcium addition on the microstructures of AZ91 magnesium alloy was investigated. It was found that a small amount of calcium in AZ91 allay produced a large decrease in the α- Mg grain size and the dispersed fine β-Mgt7 Alt2.phases. In addition, some Al4Ca particles were found to exist in the AZ91 alloy containing 0.5wt% Ca. EDS analysis and water-quenched technique revealed that the grain-refining mechanism of calcium for the AZ91 alloys was mainly attributed to the role of restricting growth of calcium in the primary α-Mg crystals.

关键词： AZ91 magnesium alloy calcium microstructural refinement

Flexural-tensile Properties of Layered Steel Fiber Reinforced Rubber Concrete

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Journal of wuhan University of technology(Materials {2.) 2009年第5期24卷 846-848页

作者：易贤仁 School of sciences Wuhan University of Technology

Layered steel fiber reinforced rubber concrete （LSFRRC）, a new type of pavement concrete based on the requirements of national standard were experimentally researched. The different properties of flexural-tensile strength from plain concrete （PC）, rubber concrete （RC）, layered steel fiber reinforced concrete （LSFRC） and LSFRRC were presented. Experimental results show that the tensile strength of LSFRRC is improved by 4.12. compared with PC, by 13.75% compared with RC. The load-deflection curve on flexural-tensile propertiesis put forward. The flexural-tensile toughness index I10 of LSFRRC is improved 10.32.times compared with PC.

关键词： RC LSFRRC flexural-tensile strength load-deflection curve experimental re-search

Photocatalytic Degradation of Rhodamine B Dye with High Purity Anatase Nano-TiO_2.Synthesized by a Hydrothermal Method

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Journal of wuhan University of technology(Materials {2.) 2011年第4期26卷 600-605页

作者：史晓亮 School of Mechanical and Electronic Engineering Wuhan University of Technology State Key Laboratory of Advanced technology for Materials Synthesis & Processing Wuhan University of Technology

High purity anatase nano-TiO2.powders with high photocatalytic activity were prepared by a hydrothermal synthesis method. X-ray diffraction （XRD）, field emission transmission electron microscopy （FETEM）, ultraviolet-visible （UV-Vis） light absorption spectrum and photoluminescence （PL） spectrum were adopted to characterize the catalyst. Effects of temperature, time and sol concentration of hydrothermal synthesis on particle size and phases were investigated. Photocatalytic activities in the degradation of Rhodamine B Dye were studied. The experimental results indicated that photocatalytic activity of the nano-TiO2.powers was much higher than that of P2. （Degussa）.

关键词： TiO2 hydrothermal synthesis photocatalytic activity high purity anatase

Synthesis and Characterization of Ibuprofen-Rectorite Composites by Solution Intercalation Method

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Journal of wuhan University of technology(Materials {2.) 2009年第4期24卷 654-657页

作者：王慧燕 Hospital Wuhan University of Teehnology

The ibuprofen-rectorite composites were prepared by the solution intercalation method using ibuprofen and rectorite as raw materials, and were characterized by X-ray diffraction （XRD） analysis, Fourier transform infrared analysis and scanning electron microscopy （SEM）. The experimental results show that the ibuprofen is intercalated into the interlayer spaces of rectorite. The values of the （001） peaks of the ibuprofen-rectorite composite are larger than that of Na-rectorite and reach the largest when the reaction time and ibuprofen amount is 2.h and 0.36 g, respectively. The layered structure of Na-rectorite is destroyed to some extent with the intercalation of ibuprofen into the interlayer space in the structure of Na-rectorite. A part of ibuprofen in the ibuprofen Na-rectorite covers on the surface of Na-rectorite besides some ibuprofen enters into the interlayer space.

关键词： ibuprofen rectorite solution intercalation composites clay

Numerical simulations and experimental investigations on transverse effects of two-wave mixing in a photovoltaic photorefractive crystal

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science china(Physics,Mechanics & Astronomy) 2010年第5期53卷 856-863页

作者： CAI Xin1,2.LIU JinSong1 & WANG ShengLie1 1 wuhan National Laboratory for Optoelectronics,School of Optoelectronic science and Engineering,Huazhong University of science and technology,wuhan 430074,china 2.School of science,wuhan University of technology,wuhan 430070,china wuhan National Laboratory for Optoelectronics School of Optoelectronic Science and Engineering Huazhong University of Science and Technology Wuhan China School of science Wuhan University of Technology Wuhan China

The transverse effects of two Gauss waves mixing in a photovoltaic photorefractive crystal,i.e.,the dynamical evolutions of signal beam with different parameters,are traced numerically and *** the one-dimensional numerical simulations and two-dimensional experimental investigations show that the self-focusing effect of signal beam becomes more obvious as the intensity of pump beam and the angle between the signal and pump beams *** accordance with these results,the state of two Gaussian waves mixing is controllable.

关键词： numerical simulation experimental investigation two-wave mixing transverse effects Gaussian distribution