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Geochemistry and mineralogy of the Late Permian coals from the Songzao Coalfield, Chongqing, southwestern china

science china earth sciences 2007年第5期50卷 678-688页

作者： DAI ShiFeng1,2, ZHOU YiPing3, REN DeYi1, WANG XiBo1, 2, LI Dan1, 2 & ZHAO Lei1, 2 1 State Key Laboratory of Coal resources and Safe mining (china university of mining and technology), beijing 100083, china 2 department of resources and earth science, china university of mining and technology, beijing 100083, china 3 Kunming Research Institute of Coal science, Kunming 650041, china State Key Laboratory of Coal resources and Safe mining (china university of mining and technology) Beijing 100083 China department of resources and earth science China University of Mining and Technology Beijing 100083 China Kunming Research Institute of Coal science Kunming 650041 China State Key Laboratory of Coal resources and Safe mining (china university of mining and technology) Beijing 100083 China

Mineralogy and geochemistry of the four main workable coal seams (No.6, No.7, No.8, and No.11) of Late Permian age from the Songzao Coalfield, Chongqing, Southwest china, were examined using in- ductively coupled plasma-mass spectrometry (ICP-MS), X-ray fluorescence spectrometry (XRF), cold-vapor absorption spectrometry (CV-AAS), ion-selective electrode (ISE), scanning electron mi- croscopy equipped with an energy-dispersive X-ray spectrometer (SEM-EDX), and X-ray diffraction analysis (XRD). The results showed that the main workable No.8 Coal that accounts for about 60% of the total coal reserves in the Songzao Coalfield was not enriched in hazardous trace elements. The No.11 Coal has high concentrations of alkaline elements, Be (9.14 μg/g), Sc (12.9 μg/g), Ti (9508 μg/g), Mn (397 μg/g), Co (23.7 μg/g), Cu (108 μg/g), Zn (123 μg/g), Ga (32 μg/g), Zr (1304 μg/g), Nb (169 μg/g), Hf (32.7 μg/g), Ta (11.4 μg/g), W (24.8 μg/g), Hg (0.28 μg/g), Pb (28.1 μg/g), Th (24.1 μg/g), and rare earth elements (509.62 μg/g). The concentration of Nb and Ta in the No. 11 Coal is higher than the industrial grade, and their potential utilization should be further studied. Besides pyrite, quartz, calcite, and clay minerals, trace minerals including chalcopyrite, marcasite, siderite, albite, mixed-layer clay minerals of illite and smectite, monazite, apatite, anatase, chlorite, and gypsum were found in the No.11 Coal. It should be noted that alabandite of hydrothermal origin and anatase occurring as cement were identi- fied in coal. In addition, the clayey microbands derived from alkaline volcanic ashes were identified in the coal. The dominant compositions of these clayey microbands were mixed-layer clay minerals of illite and smectite, which were interlayered with organic bands. The modes of occurrence of alkaline volcanic ash bands indicate that the volcanic activities were characterized by the multiple eruptions, short time interval and small scale for each eruption during peat accumu

关键词： coal trace elements mineral alkaline volcanic ash Late Permian period Songzao Coalfield

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Comparative study on CO_2 corrosion behavior of N80,P110,X52 and 13Cr pipe lines in simulated stratum water

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science china(Technological sciences) 2010年第9期53卷 2342-2349页

作者： CAI YiDong1,GUO PengChao1,LIU DaMeng1,CHEN ShiYu2 & LIU JunLai3 1 School of Energy resources,china university of Geosciences,beijing 100083,china 2 School of Materials science and Engineering,university of science and technology beijing,beijing 100083,china 3 School of earth sciences and resources,china university of Geosciences,beijing 100083,china School of Energy resources China University of Geosciences Beijing China School of Materials science and Engineering University of Science and Technology Beijing Beijing China School of earth sciences and resources China University of Geosciences Beijing China

To better understand the carbon dioxide (CO2) corrosion behavior of carbon steel and its influence on petroleum development (including drilling,production and transportation) in the Daqing Oilfield,CO2 corrosion behaviors of N80,P110,X52 and 13Cr pipe lines in simulated solution at high temperature and high pressure condition are investigated by dynamic corrosion experiments,scanning electron microscope (SEM) and energy dispersive X-ray spectroscopy (EDS) *** show that the corrosion rate of all pipe lines increases quickly when CO2 partial pressure increases from 0.5 to 1.5 MPa,but it slows down when CO2 partial pressure further increases from 1.5 to 4.5 MPa,during which localized corrosion is *** the experimental temperature ranges from 60 to 120°C,localized corrosion *** corrosion rate of all pipe lines decreases sharply when the temperature changes from 60 to 100°C,and it becomes stable after the temperature is higher than 100°*** the flow rate is in the range of 0–1.5 m/s,the corrosion rate of sample X52 remains unchanged,but localized corrosion gradually becomes very serious when the flow rate further *** analyzing the corrosion product scales of sample 13Cr,some remarkable phenomena are *** the temperature range of 60–100°C,the corrosion product scales are loose and thick,but become very compact when the temperature increases above 100°*** the later case,localized corrosion is *** main components of the corrosion product scales are FeCO3 and Cr2O3.

关键词： CO2 corrosion pipe lines weight loss SEM EDS

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Spatio-temporal carbon isotope variation during the Ediacaran period in South china and its impact on bio-evolution

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science china earth sciences 2009年第10期52卷 1520-1528页

作者： WANG XinQiang1 & SHI XiaoYing1,2 1 School of earth science and Mineral resources, china university of Geosciences, beijing 100083, china 2 State Key Laboratory of Geological Processes and Mineral resources, beijing 100083, china School of earth science and Mineral resources China University of Geosciences Beijing China State Key Laboratory of Geological Processes and Mineral resources Beijing China

The Ediacaran period is characterized by the extremely negative carbon isotope anomalies and great biotic evolution in earth history. At least four negative carbon isotope anomalies have been reported from this interval in South china so far. It is traditionally argued that the isotope variations can be used as a useful tool for global correlation of Ediacaran succession; however, more and more researches argued against this idea. We reviewed the previously published carbon isotope data in South china, and distributed the mean values of a certain time to the paleogeographic maps. The results show that the carbon isotope values (δ13C) vary greatly in different environments, but a clear tendency of becoming lighter from shallow platform to deep basin, with a maximum variation up to 1‰ Moreover, the important changes in Ediacaran biota, marked by the introducing of new taxa or ecologic groups, seemed to always postdate the negative anomalies but coincide with the positive shift. If the negative excursions represented the oxidation of a large dissolved organic carbon (DOC) reservoir in the ocean, the diverse Ediacaran organisms and the carbon isotope anomalies may suggest totally different environments: oxic and anoxic/euxinic. We also suggest that the elimination of euxinic state through precipitation of pyrites is one of the important environment factors in prompting the Ediacaran bio-evolution.

关键词： Ediacaran South china carbon isotope spatio-temporal variations bio-evolution

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A Comprehensive Utilization Process for Black Manganese-silver Ores by Pyrite Reducing Method

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Rare Metals 2001年第3期20卷 142-146页

作者： Huimin Lu, Xing Zou department of Nonferrous Metallurgy, university of science and technology beijing, beijing 100083, china 北京科技大学北京 100083

On a 5 kg bench scale, the separating of Mn-Ag from black manganese-silver ores by pyrite reducing method was investigated. Leached Mn content of 98.3% (mass fraction) along with silver loss of 1.5% is achieved. The purification of solution by the precipitation method was effectively used. Chemical grade gamma -MnO2 with TMn content of 60.13% (mass fraction) and MnO2 content of 92.28% (mass fraction) is obtained. Mn recovery efficiency is 94.04%. The residues from leaching Mn process of black Mn-Ag ores was employed for silver extraction by cyanidation with leached silver content of 92.17% (mass fraction), displacement ratio of 99.5%, recovery efficiency of 90.79%. Therefore, the present study provides a feasible process for making full use of black manganese-silver ore resources.

关键词： black manganese-silver ores leaching cyanidation pyrite manganese silver

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Optimum Design of Movable Screen Jig Cycle

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International Journal of Minerals,Metallurgy and Materials 1999年第4期13卷 246-249页

作者： Chunbao Sun Yubo Sun(1 resources Engineering School, university of science and technology beijing, beijing 100083. china2 department of Mineral Engineering, Northeastern university. Shenyang 10006. china) resources Engineering School University of Science and Technology Beijing Beijing 100083 China department of Mineral Engineering Northeastern University Shenyang 110006 China

The basic method for designing and calculating reasonable jig cycle of movable screen jig was presented. The reasonabilityand reliability of designed jig cycle were verified by' means of the test on artificial mixed materials. An iron ore (12-100 mm) was treatedin tile TJD-75 model movable screen jig with the jig cycle. The good results were achieved. This would provide a reliable basis for designof commercial movable-screen jig.

关键词： movable-screen jig jig cycle optimum design

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Fractal Characteristics of Coal Pores Based on Classic Geometry and Thermodynamics Models

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Acta Geologica Sinica(English Edition) 2011年第5期85卷 1150-1162页

作者： CAI Yidong~1,LIU Dameng~(1,*),YAO Yanbin~1,LI Junqian~1 and LIU Junlai~2 1 School of Energy resources,china university of Geosciences,beijing 100083,china 2 School of earth science and resources,china university of Geosciences,beijing 100083,china School of Energy resources China University of Geosciences Beijing 100083 China School of earth science and resources China University of Geosciences Beijing 100083 China

To better understand the characteristics of coal pores and their influence on coal reservoirs, coal pores in eight main coalfields of North china were analyzed by mercury porosimetry and scanning electron microscopy（SEM）.Fractal characteristics of coal pores（size distribution and structure） were researched using two fractal models:classic geometry and *** two models establish the relationship between fractal dimensions and coal pores *** results include:（1） SEM imaging and fractal analysis show that coal reservoirs generally have very high heterogeneity;（2） coal pore structures have fractal characteristics and fractal dimensions characteristic of pore structures are controlled by the composition（e.g.,ash,moisture,volatile component） and pore parameters（e.g.,pore diameter,micro pores content） of coals;（3） the fractal dimensions（D;and D;） of coal pores have good correlations with the heterogeneity of coal pore *** fractal dimensions correlate to higher heterogeneity of pore *** fractal dimensions（D;and D;） have strong negative linear correlations with the sorted coefficient of coals （R;=0.719 and 0.639,respectively） that shows the heterogeneity of coal pores;（4） fractal dimension D;and petrologic permeability of coals have a strong negative exponential correlation（R;=0.82）.However, fractal dimension D;and petrologic permeability of coals have no obvious correlation;and（5） the model of classic geometry is more accurate for fractal characterization of coal pores in coal reservoirs than that of thermodynamics by optimization.

关键词： coal pores mercury porosimetry fractal dimensions thermodynamics model classic geometry model

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On three-dimensional geological modeling and visualization

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science china earth sciences 2004年第8期47卷 739-748页

作者： WU Qiang1 & XU Hua2 1. department of Resource Exploitation Engineering, china university of mining and technology, beijing 100083, china 2. beijing Institute of Petrochemical technology, beijing 102617, china department of Resource Exploitation Engineering China University of Mining and Technology Beijing China beijing Institute of Petrochemical technology Beijing China

The technology of 3D geological modeling will bring about great changes in the methods of geological data acquiring, storing, processing and displaying. However, no perfect or convenient software systems have been developed up to now since the geologic data which re-flect geological entities bear the feature of diversity, uncertainty and complexity. Some supervoxel models, mathematical models of fault and geometrical models of fold have been contrived so as to show the space geometric configuration of the complicated geologic structures. The application-oriented system architecture for 3D geological modeling is established; and a novel design concept based on spatial data processing is also proposed with the technology of solid modeling as its core and the application of models as its objective. Theories and methods for 3D geological modeling will hopefully be enriched and developed. In the light of these theories and methods, a feature-based navigation visualization technique is also put forward in the paper. By integrating geo-database, graphics libraries and KBS with 3D dynamic simulation systems, geologists will be able to capture the partial characteristics and whole structure embodied in the geological data in a direct-viewing, figurative and accurate manner.

关键词： 3D geological modeling,geometrical model,system architecture,visualization

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science china earth sciences 2004年第10期47卷 896-911页

作者： ZHANG Changhou1,2, WU Ganguo1,2, WANG Genhou2, ZHANG Weijie2 & SONG Honglin2 1. Key Laboratory of Lithospheric Tectonics and Lithoprobing technology, china university of Geosciences, Ministry of Education of china, beijing 100083, china 2. School of earth sciences and Mineral resources, china university of Geosciences, beijing 100083, china Key Laboratory of Lithospheric Tectonics and Lithoprobing technology China University of Geosciences Ministry of Education of China Beijing China School of earth sciences and Mineral resources China University of Geosciences Beijing China

The northwest trending tectonic belt in the middle part of the Mesozoic intraplate Yanshan Orogenic Belt, northeast Hebei Province, is composed of thrusts, extensional faults, strike-slip faults and syntectonic sedimentations as well. The northeastward basement-involved major thrusting deformation occurred between 174Ma and 168MaBP and was followed by an intrusion of the granitic plutonic rocks. As a part of the post-thrusting extensional deformations a northwest extending volcano-sedimentation system of Late Jurassic and Early Cretaceous formed in the southwest side of the belt. These volcano-sedimentary sequences are divided into Tuchengzi Formation, Zhangjiakou Formation, Yixian Formation and Jiufotang Formation re- spectively. They are characterized by southeastward migration as a result of the increasing down-dip slip displacement along the major extensional fault toward the southeast of the belt. The provenance area of the Jiufotang Formation north to it experienced southwestward thrusting during and after its later sedimentation. The thrusting in this stage resulted in the formation of an asymmetric footwall syncline with vergence to SW in the Jiufotang Formation in the NE side of the basin. Finally a dextral strike-slip deformation occurred along the NW tectonic belt. The striking tectono-geomorphological features and present seismic activities along this belt indicate that it has been being active since Cenozoic era and is still in the active state at present. This northwest extending tectonic belt was following the same direction and location as the existing fault systems within the basement as revealed by former geological and geophysical studies. So it is reasonable to infer the Mesozoic deformation along this belt to be a result of reactivation of the basement structures in a favorable tectonic stress field. The reactivation of basement struc- tures might be taken as one of the mechanisms of intraplate deformation and orogeny.

关键词： Yanshan Orogenic Belt, northwest extending tectonic complex, thrust system, geochronology.

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South china's Gondwana connection in the Paleozoic:Paleomagnetic evidence

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Progress in Natural science:Materials International 2004年第1期14卷 86-91页

作者： ZHANG Shihong*(School of earth sciences and resources, china university of Geosciences, beijing 100083, china) china Univ Geosci Sch Earth Sci & Resources Beijing 100083 Peoples R China

The reconstruction in which the South china Block (SCB) lies along the Great India Australia region of Gondwana margin is tested by using existing Paleozoic paleomagnetic data. Under the proposed reconstruction, all six high quality paleopoles from the SCB between the Early Cambrian and late Early Devonian (～400 Ma) are in good agreement with coeval paleopoles from Gondwana. Thereafter, the apparent polar wander paths for the SCB and Gondwana diverge markedly. This indicates that the SCB had been part of Gondwana and the connection was intact from at least Early Cambrian until late Early Devonian, but they began to separate by late Middle Devonian (～375 Ma).

关键词： South china block Gondwana paleomagnetism reconstruction

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Indian Ocean-MORB-type isotopic signature of Yushigou ophiolite in North Qilian Mountains and its implications

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science china earth sciences 2006年第6期49卷 561-572页

作者： HOU Qingye1,2, ZHAO Zhidan1,2, ZHANG Hongfei3, ZHANG Benren3 & CHEN Yuelong2 1. State Key Laboratory of Geological Processes and Mineral resources, china university of Geosciences, beijing 100083, china 2. School of earth science and Mineral resources, china university of Geosciences, beijing 100083, china 3. Faculty of earth sciences, china university of Geosciences, Wuhan 430074, china State Key Laboratory of Geological Processes and Mineral resources China University of Geosciences Beijing China School of earth science and Mineral resources China University of Geosciences Beijing China Faculty of earth sciences China University of Geosciences Wuhan China

In order to explore the disputed issue concerning the tectonic affinity ofthe ancient ocean mantle of North Qilian Mountains (NQM), geochemical and Sr, Nd, Pb isotopiccompositions of pillow basalts of the Yushigou Ophiolite (YSGO) suite from NQM have been analyzedsystematically. The pillow basalts exhibit tholeiitic characteristics, with flatchondrite-normalized REE patterns ((La/Yb)_N = 0.98—1.27). They display no Nb, Ta, Zr, Hf negativeanomalies, and show MORB features in 2Nb-Zr/4-Y and Ti/100-Zr-YX3 tectonic discrimination *** results indicate that the Yushigou ophiolite is most likely to be formed in a mid-ocean ridgeor mature back-arc basin. Their isotopic data show a relatively broad and enriched ^(87)Sr/^(86)Sr(0.70509 — 0.70700), restricted ^(143)Nd/^(144)Nd (0.512955-0.512978). Pb isotopes are in the rangeof ^(206)Pb/^(204)Pb (18.054-20.562), ^(207)Pb/^(204)Pb (15.537-15.743) and ^(208)Pb/^(204)Pb(38.068-38.530). These isotopic data imply that the basalts originated from the depleted mantle(DMM), with the involvement of enriched mantle components (mainly EMII). Geochemical comparisonsbetween the basalts in YSGO and the MORB-type basalts of ophiolite suites occurring in the knownancient Tethyan tectonic domain indicate that the ancient oceanic mantle represented by YSGO suiteforming in early Paleozoic in the North Qilian Moutains is very similar to the Tethyan mantle inboth trace elements and isotopic compositions. The North Qilian Mountains should be a part of theTethyan tectonic domain in early Paleozoic. This further implies that the Tethyan tectonic domaincan be deduced to early Paleozoic in the study area, which will be helpful to discussing thetectonic affinity and evolution of the North Qilian Mountains.

关键词： geochemistry, Indian Ocean-MORB-type isotopic signatures, Tethyan tectonic domain, Yushigou ophiolite, North Qilian Mountains.

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