Synthesis and characterization of cuprous selenide nanocrystals at room temperature

作     者：Tai Shan Li Shao Pu Liu Zhao Xia Lu Zhong Fang Liu 

作者机构：School of Chemistry and Chemical Engineering Southwest University Chongqing 400715 China School of Chemical Engineering and Biological Technology Hebei Polytechnic University Tangshan 063000 China 

出 版 物：《Chinese Chemical Letters》 (中国化学快报（英文版）)

年 卷 期：2007年第18卷第5期

页      面：617-620页

核心收录：

学科分类：080903[工学-微电子学与固体电子学] 0809[工学-电子科学与技术（可授工学、理学学位）] 08[工学] 080501[工学-材料物理与化学] 0805[工学-材料科学与工程（可授工学、理学学位）] 080502[工学-材料学] 

基　　金：This work was supported by the National Natural Science Foundation of China (No. 20475045) 

主　　题：Cuprous selenide Nanocrystals Synthesis Characterization 

摘      要：A simple method has been developed to prepare cuprous selenide nanocrystals by the reaction of copper nitrate trihydrate with selenium and sodium mercaptoacetate in aqueous ammonia system. CuESe nanocrystals were characterized by transmission electron microscopy （TEM）, high resolution transmission electron microscopy （HRTEM）, X-ray diffraction （XRD）, electron diffraction （ED）, fluorescence spectrum and ultraviolet-visible absorption spectrum. Cu2Se nanocrystals showed berzelianite structure with 20-40 nm in length and 10-20 nm in width. A possible mechanism is also discussed.