CdS纳米粒子的水热微乳法制备
Preparation of CdS Nanoparticles by Hydrothermal Method in Microemulsion作者机构：浙江大学材料系硅材料国家重点实验室杭州310027
出 版 物：《无机化学学报》 (Chinese Journal of Inorganic Chemistry)
年 卷 期：2006年第22卷第5期
页 面：917-920页
核心收录：
学科分类：081704[工学-应用化学] 07[理学] 08[工学] 0817[工学-化学工程与技术] 0805[工学-材料科学与工程（可授工学、理学学位）] 080502[工学-材料学] 0703[理学-化学] 070301[理学-无机化学]
基 金：国家自然科学基金项目(No.50372060) 863项目(No.2004AA32G040)资助
摘 要：The CdS nanoparticles with good crystallinity were prepared by hydrothermal method in microemulsion composed of poly oxyethylene lauryl ether/water/ cyclohexane/butanol. The structure and the size of the nanoparticles were analyzed by TEM and XRD. The UV-Vis optical absorption of the samples was also *** results show that hydrothermal treatment is an effective method to prepare CdS nanoparticles of hexagonal structure at low temperature. The particles were in dimensional uniformity. The diameter of the nanoparticles decreased with the increase of the molar ratio of water to surfactant. The minimum diameter of the nanoparticles prepared in this work was 10 nm. Obvious blue-shift were observed in the UV-Vis absorption.
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