Synthesis and optical characterization of porous ZnO
作者机构：Department of PhysicsNational Institute of Technology WarangalWarangal-506004Andhra PradeshIndia
出 版 物：《Journal of Advanced Ceramics》 (先进陶瓷（英文）)
年 卷 期：2013年第2卷第3期
页 面：260-265页
核心收录：
学科分类：08[工学] 0805[工学-材料科学与工程（可授工学、理学学位）] 080502[工学-材料学]
主 题：semiconductors porous ZnO optical properties
摘 要：In this paper,a simple and cheap method to prepare porous ZnO by using zinc nitrate,ethanol and triethanolamine(TEA)is *** as-prepared sample consisted of nano and micro *** sample was calcined at 300℃,400℃and 500℃with different heating *** 500℃,the nano pores disappeared but the sample maintained its micro *** emission scanning electron microscopy(FE-SEM)pictures confirmed that the size and growth of ZnO nanoparticles depended on the heating *** infrared(IR)absorption peak of Zn-O stretching vibration positioned at 457 cm^(-1)was split into two peaks centered at 518 cm^(-1)and 682 cm^(-1)with the change of *** results confirmed that Fourier transform infrared(FT-IR)spectrum was sensitive to variations in particle size,shape and *** photoluminescence(PL)spectrum of porous ZnO contained five emission peaks at 397 nm,437 nm,466 nm,492 nm and 527 *** intensity enhanced monotonously with increase of temperature and the change was rapid between temperatures of 300℃and 500℃.This was due to the elimination of organic species and improvement in the crystallanity of the sample at 500℃.
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