Synthesis, Characterization and X-ray Crystal Structure of O,O~ˊ-Dipropyl α-（2,4-Dichlorolphenoxyacylamido）-α-（4-methoxyphenyl） Methylphosphonates

作     者：宁丽红 彭浩 贺红武 

作者机构：Key Laboratory of Pesticide and Chemical Biology Ministry of Education and College of Chemistry Central China Normal University College of Science Huazhong Agricultural University 

出 版 物：《Chinese Journal of Structural Chemistry》 (结构化学（英文）)

年 卷 期：2013年第32卷第9期

页      面：1392-1396页

核心收录：

学科分类：07[理学] 070205[理学-凝聚态物理] 08[工学] 080501[工学-材料物理与化学] 0805[工学-材料科学与工程（可授工学、理学学位）] 0703[理学-化学] 0702[理学-物理学] 

基　　金：supported by the National Basic Research Program of China(2010CB126100) 

主　　题：X-ray crystallography phosphonate 

摘      要：A new crystal of O,Oˊ-dipropyl-α-（2,4-dichlorolphenoxyacylamido）-α-（4-methoxyphenyl） methylphosphonates has been prepared at room temperature and characterized by elemental analysis and IR,MS,1H NMR spectra,13C NMR spectra and X-ray single-crystal *** complex crystallizes in triclinic,space group P1 with a = 7.858（2）,b = 12.621（4）,c = 12.621（4）,α = 96.17（3）,β = 90.960（3）,γ = 90.960（3）°,V = 1243.9（7）3,Dc = 1.346 Mg/m3,Z = 2,μ = 0.362 mm-1and F（000） = 528.