Synthesis and Crystal Structure of 2-Nitrophenyl N,N-Bis(2-chloroethyl)-N'-(4-methylbenzene- sulfonamino)ethyl-phosphorodiamidate

作     者：ZHANG Gai-Hong CHEN Ru-Yu HUANG You MIAO Zhi-Wei 

作者机构：Institute and State Key Laboratory of Elemento-organic Chemistry Nankai University Tianjin 300071 China 

出 版 物：《Chinese Journal of Structural Chemistry》 (结构化学（英文）)

年 卷 期：2006年第25卷第7期

页      面：797-800页

核心收录：

学科分类：07[理学] 0703[理学-化学] 

基　　金：Corresponding author. Chen Ru-Yu  born in 1919  professor  member of the Chinese Academy of Sciences  

主　　题：sulfonamide crystal structure phosphorodiamidate 

摘      要：The crystal structure of 2-nitrophenyl N,N-bis（2-chloroethyl）-N＇-（4-methylbenzene-sulfonamino）ethyl-phosphorodiamidate （C19H25Cl2N4O6PS） was determined by single-crystal X-ray diffraction analysis. The compound crystallizes in the triclinic system, space group PI^- with a = 9.3664（13）, b = 9.9560（14）, c = 13.1803（18） ,A, α = 87.338（2）, β= 87.632（2）, γ = 79.536（2）°, Dc = 1.484 g/cm^3, Z = 2, λ = 0.71073 A, μ（MoKα） = 0.465, Mr = 539.36, V = 1206.7（3） A^3, F（000） = 560, the final R = 0.0426 and wR = 0.1097 for 3463 observed reflections with I 〉 2σ（I）.