Tensile-WAXD Apparatus:An Improved and Accurate System for the In situ Study of Extension-induced Segmental Orientation in Highly Stretched Elastomer
作者机构:Center for Advanced Material Diagnostic TechnologyShenzhen Technology UniversityShenzhen518118China Laboratoire de Physique des SolidesCNRSUniversitéParis-SudUniversitéParis-SaclayOrsay91400France
出 版 物:《Chinese Journal of Polymer Science》 (高分子科学(英文版))
年 卷 期:2024年第42卷第12期
页 面:2002-2010,I0011页
核心收录:
学科分类:08[工学] 0805[工学-材料科学与工程(可授工学、理学学位)] 080502[工学-材料学]
基 金:financial support of China CSC Scholarship(No.201604910522)
主 题:X-ray apparatus Elongation calculation Segmental orientation In situ measurement
摘 要:An improved X-ray apparatus that combines tensile testing and X-ray diffraction has been designed and constructed to conduct timeresolved experiments during uniaxial *** utilizing mortise-like clamping jaws and dogbone-shaped specimens,this setup allows for the simultaneous recording of high-quality mechanical responses and 2D diffraction patterns due to the minimization of experimental errors from sample slippage or premature ***,the local extension ratio can be accurately determined based on thickness variation,and the Hermans orientation function was demonstrated to be a reliable method with high accuracy to calculate the segmental orientation parameter〈P_(2)〉in elastomeric samples under high degree of *** summary,this innovative tensile-WAXD instrument has proven to be a promising and powerful technique for investigating the“stress-deformation-segmental orientationrelationship in elastomers with high extensibilities.