Study on quality standard of Danmu exract syrup
作者机构:Hainan Provincial Key Laboratory of R&D on Tropical HerbsHaikou 571199 School of Pharmaceutical Sciences Hainan Medicine UniversityHaikou 571199China
出 版 物:《Journal of Hainan Medical University》 (海南医学院学报(英文版))
年 卷 期:2021年第27卷第9期
页 面:10-15页
学科分类:1008[医学-中药学(可授医学、理学学位)] 1006[医学-中西医结合] 100602[医学-中西医结合临床] 10[医学]
基 金:Key science and technology project of Hainan province(No.ZDKJ201805)
主 题:Danmu exract syrup Quality standards Strictosamide Chlorogenic acid High performance liquid chromatography Thin layer chromatography
摘 要:Objective:To establish the quality standard of Danmu exract ***:TLC method was used to qualitatively identify Nauclea officinalis in Danmu exract *** content of strictosamide and chlorogenic acid in Danmu exract syrup was determined by high efficiency axillary ***:The spots were clear and there was no negative *** linear relationship of strictosamide was good in the range of 100~300ug/ml(R^(2)=0.9997).The average recovery was 99.1%and RSD was 1.16%(n=9).Chlorogenic acid had a good linear relationship in the range of 6.7~20.2ug/ml(R^(2)=0.9991).The average recovery was 99.9%and RSD was 1.10%(n=9).Conclusion:The standard is safe and reasonable,the method is simple,accurate and reproducible,and it can be used for the quality control of Danmu exract syrup.