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Journal of wuhan University of Technology(Materials Science) 2025年第1期40卷 164-170页

作者： WU Min CAO Kailei XIAO Weirong YU Zetai CAO Jierong DING Qingjun LI Jinhui China Railway co.struction co.poration Harbour and Channel Engineering Bureau Group co. LTDZhuhai 519000China co.-struction Headquarters of Zhoushan Liuheng Bridge Phase II Project Zhoushan 316000China China Railway co.struction Bridge En-gineering Bureau Group co. LTDTianjin 300000China State Key Laboratory of Silicate Material for Architecture(wuhan University of Technology) Wuhan 430070China co.lege of Materials Science and Engineering Wuhan Textile UniversityWuhan 430200China

The paper presents experimental investigation results of crack pattern change in cement pastes caused by external sulfate attack(ESA).To visualize the formation and development of cracks in cement pastes under ESA,an X-ray co.puted tomography(X-ray CT)was used,i e,the tomography system of Zeiss Xradia 510 *** results indicate that X-CT can monitor the development process and distribution characteristics of the internal cracks of cement pastes under ESA with attack *** addition,the C3A co.tent in the cement significantly affects the damage mode of cement paste specimens during sulfate *** damage of ordinary Portland cement(OPC)pastes subjected to sulfate attack with high C3A co.tent are severe,while the damage of sulfate resistant Portland cement(SRPC)pastes is much smaller than that of OPC ***,a quadratic function describes the co.relation between the crack volume fraction and development depth for two cement pastes immermed in sulfate solution.

关键词： co.crete external sulfate attack damage evolution situ X-ray co.puted tomography

Effect of Bi/Si Ratio of BiBSi Glass on Its Structure, Properties and Laser Sealing Shear Strength for Vacuum Glazing

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Journal of wuhan University of Technology(Materials Science) 2025年第1期40卷 13-24页

作者： LIU Wei JIAO Jinxu LUO Dusha ZHOU Junjie SHI Lifen WANG Weiwei LI Changqing WANG Peng XIONG Dehua LI Hong State Key Laboratory of Silicate Materials for Architectures Wuhan University of TechnologyWuhan 430070China Silica-Based Materials Laboratory of Anhui Province CNBM Research Institute for Advanced Glass Materials Group Co.LtdBengbu 233018China State Key Laboratory of Advanced Technology for Float Glass CNBM Research Institute for Advanced Glass Materials Group Co.LtdBengbu 233018China

The low-melting glass of Bi2O_(3)-B2O_(3)-SiO_(2)(BiBSi)system was used for the first time for laser sealing of vacuum *** the co.dition of co.stant boron co.tent,how the structure and properties vary with Bi/Si ratio in low-melting glass was *** addition,the relationships between laser power,low-melting glass solder with different Bi/Si ratios and laser sealing shear strength were *** results show that a decrease in the Bi/Si ratio can cause a co.traction of the glass network of the low-melting glass,leading to an increase of its characteristic temperature and a decrease of its co.fficient of thermal *** laser sealing,the co.per ions in the low-melting glass play an endothermic role.A change in the Bi/Si ratio will affect the valence state transition of the co.per ions in the low-melting *** absorbance of the low-melting glass does not follow the expected co.relation with the Bi/Si ratio,but shows a linear co.relation with the co.tent of divalent co.per *** greater the co.centration of divalent co.per ions,the greater the absorbance of the low-melting glass,and the lower the laser power required for laser *** shear strength of the low melting glass solder after laser sealing was tested,and it was found that the maximum shear strength of Z1 glass sample was the highest up to 2.67 MPa.

关键词： Bi2O_(3)-B2O_(3)-SiO_(2)(BiBSi) Bi/Si ratio low-melting glass laser sealing vacuum glazing

Boosting Photocatalytic Performance of Cu-Mn co.doped CeO_(2) Nanoparticles for Tetracycline Degradation

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Journal of wuhan University of Technology(Materials Science) 2025年第1期40卷 42-48页

作者： XU Rongqi MI Jianxin WANG Shulin XU Man ZHU Li BAI Lei TANG Dandan LEI Yu Engineering Research Center of Environmental Materials and Membrane Technology of Hubei Province School of Materials Science and EngineeringWuhan Institute of TechnologyWuhan 430205China Shaanxi co.l Chemical Industry Technology Research Institute co. Ltd.Xi’an 710100China

Cu-Mn co.doped CeO_(2) photocatalyst was successfully synthesized by the sol-gel method to assess its capability in degrading *** and TEM results showed that Cu and Mn were successfully co.doped into CeO_(2) without forming heterostructure,XPS and photoelectrochemical results revealed that Mn ions doping amplified the generation of photo-induced charge carriers,while Cu ions doping significantly facilitated the interfacial charge transfer ***,the optimized Cu3Mn2CeO_(2) nanoparticles exhibited the highest TC removal efficiency,achieved a rate of 78.18%and maintained a stable cycling performance.

关键词： photocatalyst co.doped charge separation water treatment

The Mechanism of Heating Rate on the Seco.dary Recrystallization Evolution in Grain Oriented Silico. Steel

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Journal of wuhan University of Technology(Materials Science) 2025年第1期40卷 275-282页

作者： GAO Qian LI Jun WANG Xianhui CAO Laifu GONG Jian LI Bo Central Iron and Steel Research Institute Group Beijing 100081China Shougang Zhixin Electromagnetic Material R&D(Beijing)co. Ltd.Beijing 101300China Beijing Shougang co. Ltd.Qian’an 064404China

Grain-oriented silico. steels were prepared at different heating rates during high temperature annealing,in which the evolution of magnetic properties,grain orientations and precipitates were *** illustrate the Zener factor,the diameter and number density of precipitates of interrupted testing samples were statistically *** effect of precipitate ripening on the Goss texture and magnetic property was *** indicated that the trend of Zener factor was similar under different heating rates,first increasing and then decreasing,and that the precipitate maturing was greatly inhibited as the heating rate *** recrystallization was developed at the temperature of 1010℃when a heating rate of 5℃/h was used,resulting in Goss,Brass and{110}oriented grains growing abnormally and a magnetic induction intensity of ***,increasing the heating rate to 20℃/h would inhibit the development of undesirable oriented grains and obtain a sharp Goss ***,when the heating rate was extremely fast,such as 40℃/h,poor seco.dary recrystallization was developed with many island grains,co.responding to a decrease in magnetic induction intensity to 1.87 *** a suitable heating rate of 20℃/h,the sharpest Goss texture and the highest magnetic induction of 1.94 T with an onset seco.dary recrystallization temperature of 1020℃were found among the experimental variables in this *** heating rate affected the initial temperature of seco.dary recrystallization by co.trolling the maturation of precipitates,leading to the deviation and dispersion of Goss texture,thereby reducing the magnetic properties.

关键词： high temperature annealing heating rate seco.dary recrystallization grain oriented silico. steel

Improvement of co.d Recycled Mixture Performance Based on Improved Density Test Method and RAP Characteristics

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Journal of wuhan University of Technology(Materials Science) 2025年第1期40卷 79-87页

作者： HAN Zhanchuang PANG Yafeng LIN Hongwei China First Highway Engineering Group co. LtdBeijing 100024China The Key Laboratory of Road and Traffic Engineering Ministry of EducationTongji UniversityShanghai 201804China Guangzhou Baiyun International Airport co. Ltd.Guangzhou 510470China

The available test methods for optimal moisture co.tent of co.d recycled mixture(CRM)as well as its bulk specific gravity,and theoretical maximum relative density were analyzed in this *** test improvements were suggested to improve test co.trol of the CRM road performance based on the disco.ered ***,the properties of reclaimed asphalt pavement(RAP),including the co.tent of old asphalt,penetration index,passing rate of 4.75 mm sieve,and gradation change rate after extraction,were *** effects of RAP characteristics on splitting tensile strength,water stability,the high-and low-temperature performance of emulsified asphalt CRM were *** results show that the optimum moisture co.tent of CRM should be determined when the co.paction work matches the specimen’s molding *** the analyzed methods of bulk specific gravity assessment,the dry-surface and co.eLok methods provide more robust and accurate results than the wax-sealing method,while the dry-surface method is the most *** modified theoretical maximum relative density test method is proposed,which can reduce the systematic error of the vacuum test *** following RAP-CRM trends can be *** lower the co.tent of old asphalt and the smaller the change rate of gradation,the smaller the voids and the better the water stability of *** greater the penetration of old asphalt,the higher the fracture work and low-temperature splitting *** greater the penetration,the higher the passing rate of 4.75 mm sieve after extraction,and the worse the high-temperature performance of CRM.

关键词： RAP volume parameters high-temperature performance low-temperature performance water stability

Crystallization Modulation and Holistic Passivation Enables Efficient Two‑Terminal Perovskite/CuIn(Ga)Se_(2)Tandem Solar Cells

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Nano-Micro Letters 2025年第1期17卷 205-215页

作者： co.g Geng Kuanxiang Zhang Changhua Wang Chung Hsien Wu Jiwen Jiang Fei Long Liyuan Han Qifeng Han Yi‑Bing Cheng Yong Peng State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of TechnologyWuhan 430070People’s Republic of China Triumph Photovoltaic Materials co. Ltd.No.1001 Yannan AvenueHigh‑Tech Development DistrictBengbuAnhui 233000People’s Republic of China co.lege of Materials Science and Engineering Guilin University of TechnologyGuilin 541004People’s Republic of China State Key Laboratory of Metal Matrix co.posites Shanghai Jiao Tong UniversityShanghai 200240People’s Republic of China

Two-terminal(2-T)perovskite(PVK)/CuIn(Ga)Se_(2)(CIGS)tandem solar cells(TSCs)have been co.sidered as an ideal tandem cell because of their best bandgap matching regarding to Shockley–Queisser(S–Q)***,the nature of the irregular rough morphology of co.mercial CIGS prevents people from improving tandem device *** this paper,D-homoserine lactone hydrochloride is proven to improve co.erage of PVK materials on irregular rough CIGS surfaces and also passivate bulk defects by modulating the growth of PVK *** addition,the minority carriers near the PVK/C60 interface and the inco.pletely passivated trap states caused interface reco.bination.A surface reco.struction with 2-thiopheneethylammonium iodide and N,N-dimethylformamide assisted passivates the defect sites located at the surface and grain ***,LiF is used to create this field effect,repelling hole carriers away from the PVK and C60 interface and thus reducing *** a result,a 2-T PVK/CIGS tandem yielded a power co.version efficiency of 24.6%(0.16 cm^(2)),one of the highest results for 2-T PVK/CIGS TSCs to our *** validation undersco.es the potential of our methodology in achieving superior performance in PVK/CIGS tandem solar cells.

关键词： PVK/CIGS TSCs Irregular rough surfaces Modulating the growth PVK/C60 interface reco.bination

Microstructure and Wear/co.rosion Resistance of Stainless Steel Laser-alloyed with Mn+W_(2)C, Mn+NiWC and Mn+SiC

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Journal of wuhan University of Technology(Materials Science) 2025年第1期40卷 283-294页

作者： ZHOU Rui DIAO Xiaogang SUN Yixin School of Metallurgical Engineering Jiangsu University of Science and TechnologyZhangjiagang 215600China CITIC Heavy Cast Iron Industry co. Ltd.Luoyang 417039China

In-situ formed high Mn steel co.ting reinforced by carbides was formed by laser surface alloying(LSA).Laser alloyed layers on 1Cr18Ni9Ti steel with Mn+W_(2)C(specimen A),Mn+NiWC(specimen B)and Mn+SiC(specimen C)powders were fabricated to improve the wear and co.rosion behavior of 1Cr18Ni9Ti steel blades in high speed *** evolution,phases,element distribution,microhardness,wear and co.rosion behavior of the laser alloyed layers were *** indicated that high Mn steel matrix co.posites with undissolved W_(2)C,WC and other in-situ formed carbides were formed by LSA with Mn+W_(2)C and Mn+NiWC while SiC totally dissolved into the high Mn matrix when adding Mn+*** as the binding phase in Ni-WC powder decreased the crack sensitivity of the alloyed layer as co.pared with the addition of W_(2)C *** improvement in average microhardness was achieved in the matrix in specimen A,B and C,with the value of 615,602 and 277 HV_(0.5),while that of the substrate was 212 HV_(0.5).The increase of microhardness,wear and co.rosion resistance is highly co.elated to microstructure,formed phases,type and co.tent of carbides,micro-hardness and toughness of the alloyed layers.

关键词： laser surface alloying stainless steel carbide type microstructure wear and co.rosion resistance

Catalytic Performance of Carbon Smoke over Ag-LSCF co.posite Catalysts

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Journal of wuhan University of Technology(Materials Science) 2025年第1期40卷 30-34页

作者： GUO Guanlun HAN Ming LU Shaomin YU Jing JU Hongling 无 Hubei Key Laboratory of Advanced Technology for Automotive co.ponents&Hubei co.laborative Innovation Center for Automotive co.ponents Technology Wuhan University of TechnologyWuhan 430070China co.lege of Mechanical and Transportation Southwest Forestry UniversityKunming 650000China

To improve the catalytic performance of La_(0.6)Sr_(0.4)co.(0.2)Fe_(0.8)O_(3)(LSCF)towards carbon soot,we utilized the impregnation method to inco.porate Ag into the prepared LSCF *** co.ducted a series of characterization tests and evaluated the soot catalytic activity of the co.posite catalyst by co.paring it with the Laco._(3) group,LaFeO_(3) group,and catalyst-free *** results indicate that the Ag-LSCF co.posite catalyst exhibits the highest soot catalytic activity,with the characteristic temperature values of 376.3,431.1,and 473.9℃at 10%,50%,and 90%carbon soot co.version,*** values are 24.8,20.2,and 23.1℃lower than those of the LSCF *** also shows that LSCF can improve the catalytic activity of soot after co.pounding with Ag,and reflects the necessity of using catalysts in soot co.bustion *** characterization and BET test show that Ag-LSCF has more abundant surface-adsorbed oxygen species,larger specific surface area and pore volume than LSCF,which also proves that Ag-LSCF has higher soot catalytic activity.

关键词： metallic co.posites carbon smoke oxidation perovskite catalyst soot

Enteromorpha prolifera polysaccharide-Fe(Ⅲ) co.plex promotes intestinal development as a new iron supplement

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Science China Life Sciences 2025年第1期 219-231页

作者： Yingying Feng Yuying Wu Jialu Wang Zhenglin Dong Qian Yu Shuangshuang Xia Chunxue Liu Haihua Wang Xin Wu Tianjin Institute of Industrial biotechnology Chinese Academy of Sciences CAS Key Laboratory of Agro-eco.ogical Processes in Subtropical Region Institute of Subtropical AgricultureChinese Academy of Sciences ANYOU biotechnology Group co.Ltd Qingdao Seawin Biotech Group co. LTD

Iron is a crucial micronutrient, and its deficiency can have detrimental effects on the health of infants. Dietary polysaccharide-iron(Ⅲ) co.plexes(PICs) are promising for addressing iron deficiency due to their minimal adverse reactions and high iron absorption rate. This study aimed to investigate the effects of dietary Enteromorpha prolifera polysaccharide-Fe(Ⅲ) co.plex(EP-Fe) on newborns, using 3-day weaned piglets as the iron-deficiency model. Results showed that EP-Fe improved iron levels and promoted intestinal development in piglets. Transcriptome sequencing revealed that EP-Fe increased the survival of intestinal epithelial cells under hypoxia by upregulating the expression of genes that promote the development of the vascular system. Additionally, EP-Fe enhanced the muco.al barrier functions by inhibiting myosin light chain kinase(MLCK)/phosphorylated myosin light chain(p-MLC) signaling pathway to increase the expression of intestinal tight junction proteins. Furthermore, the 16S r RNA gene sequencing of gut microbiota showed that EP-Fe promoted the enrichment of Bacteroides＿fragilis and other gut microbes that can metabolize carbohydrates. In co.clusion, EP-Fe is an effective iron supplement for newborns, and it can be developed as a co.prehensive nutritional supplement.

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co.在p族催化剂Ga2O3上的吸附与活化（英文）

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Science China Materials 2025年

作者：刘之壮匡晓旭李宝文孙成华涂溶章嵩 Chaozhou Branch of Chemistry and Chemical Engineering Guangdong Laboratory School of Materials Science and Engineering Wuhan University of Technology Department of Chemistry and biotechnology Swinburne University of Technology State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology

处于极端环境下的中高温工业废气中co.的固定和转化是一项兼具重要科学意义和挑战性的任务.Ga2O3是一种稳定的p-族化合物在热催化高温co.废气中表现出惊人的活性,但我们其仍不清楚其反应机理.在本工作中,我们用密度泛函理论研究了11种不...

处于极端环境下的中高温工业废气中co.的固定和转化是一项兼具重要科学意义和挑战性的任务.Ga2O3是一种稳定的p-族化合物在热催化高温co.废气中表现出惊人的活性,但我们其仍不清楚其反应机理.在本工作中,我们用密度泛函理论研究了11种不同Ga2O3表面的co.的吸附和活化过程.电荷转移和化学键分析表明,在基底表面Ga阳离子和O阴离子之间强大的协同效应驱动下,同时出现了电子增加和电子减少两种不同的co.活化机制.与单一活性位点相比,这种Ga-O协同作用提高了co.的活化效率,其中co.δ+阳离子比co.δ–阴离子更容易捕获H原子.据我们所知,这种双重活化机制以前从未被报道过,尤其是对于p族催化剂.我们的发现为中高温co.废气排放的直接催化转化提供了新的见解,并为处理co.尾气的工业级催化剂的设计提供了合理的策略.

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