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Energy Engineering 2024年第4期121卷 1007-1026页

作者： Zhuo Chen Ningning Wang Wenbo Jin Dui Li The Second oil Production Plant Sinopec Northwest Oilfield CompanyUrumqi830011China Yingmaili oil and Gas Production Management Area PetroChina Tarim Oilfield CompanyKorla841001China College of Petroleum Engineering Xi’an Shiyou UniversityXi’an710065China

A hard problem that hinders the movement of waxy crude oil is wax deposition in oil *** ensure the safe operation of crude oil pipelines,an accurate model must be developed to predict the rate of wax deposition in crude oil *** at the shortcomings of the ENN prediction model,which easily falls into the local minimum value and weak generalization ability in the implementation process,an optimized ENN prediction model based on the IRSA is *** validity of the new model was confirmed by the accurate prediction of two sets of experimental data on wax deposition in crude oil *** two groups of crude oil wax deposition rate case prediction results showed that the average absolute percentage errors of IRSA-ENN prediction models is 0.5476% and 0.7831%,***,it shows a higher prediction accuracy compared to the ENN prediction *** fact,the new model established by using the IRSA to optimize ENN can optimize the initial weights and thresholds in the prediction process,which can overcome the shortcomings of the ENN prediction model,such as weak generalization ability and tendency to fall into the local minimum value,so that it has the advantages of strong implementation and high prediction accuracy.

关键词： Waxy crude oil wax deposition rate chaotic map improved reptile search algorithm Elman neural network prediction accuracy

Hydrodynamic resistance of pore–throat structures and its effect on shale oil apparent permeability

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International Journal of Coal Science & Technology 2024年第2期11卷 101-110页

作者： Wendong Wang Qian Zhang Jilong Xu Da Zheng Lifeng Liu Yuliang Su Key Laboratory of Unconventional oil and Gas Development Ministry of EducationQingdao 266580China School of Petroleum Engineering China University of Petroleum(East China)Qingdao 266580ShandongChina PetroChina oil Gas and New Energies CompanyBeijing 100083China Research Institute of Petroleum Exploration and Development PetroChinaBeijing 100083China

oil transport is greatly affected by heterogeneous pore–throat structures present in *** is therefore very important to accurately characterize pore–throat ***,it remains unclear how pore–throat structures affect oil transport *** this paper,using finite element(FE)simulation and mathematical modeling,we calculated the hydrodynamic resistance for four pore–throat *** addition,the influence of pore throat structure on shale oil permeability is *** to the results,the hydrodynamic resistance of different pore throat structures can vary by 300%.The contribution of additional resistance caused by streamline bending is also in excess of 40%,even without slip ***-thermore,Pore–throat structures can affect apparent permeability by more than 60%on the REV scale,and this influence increases with heterogeneity of pore size distribution,organic matter content,and organic matter ***,modeling shale oil flow requires consideration of porous–throat structure and additional resistance,otherwise oil recovery and flow capacity may be overestimated.

关键词： Pore–throat structure Hydrodynamic resistance Apparent permeability REV-scale Shale oil

In situ modification of heavy oil catalyzed by nanosized metal-organic framework at mild temperature and its mechanism

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Chinese Journal of Chemical Engineering 2024年第3期67卷 166-173页

作者： Li Wang Ji-Xiang Guo Rui-Ying Xiong Chen-Hao Gao Xiao-Jun Zhang Dan Luo The Unconventional oil and Gas Institute China University of Petroleum-BeijingBeijing 102200China Beijing Institute of Nanoenergy and Nanosystems Chinese Academy of SciencesBeijing 101400China

Two catalysts, nano-sized cobalt-metal-organic framework(Co-MOF) and nickel(Ni)-MOF, were successfully prepared by the modification method. Tetralin(C10H12) was used as the hydrogen donor for the catalytic cracking and hydrogenation modification study of the dehydrated crude oil from the Shengli oilfield. The optimal reaction conditions were determined through orthogonal experiments, and the components of the crude oil and modified oil samples were analyzed. The results revealed that the nanoMOF catalysts were successfully prepared and exhibited high catalytic activity. They could catalyze the cracking of large molecules in heavy oil at mild temperatures(oil at 50°C from 15761.9 m Pa.s to 1266.2 m Pa.s,with a viscosity reduction rate of 91.97%. The modification effect of Co-MOF was the next best, which could reduce the viscosity of heavy oil to 2500.1 m Pa.s with a viscosity reduction rate of 84.14%. Molecular dynamics simulations revealed a strong interaction force between the MOF surface and asphaltene molecules. In the process of heavy-oil catalytic hydrogenation, the nano-MOF catalyst exhibited high catalytic activity. On the one hand, the empty d orbitals outside the metal atoms in the catalyst could polarize the carbon atoms in the organic matter, accelerating the breaking of long chains. On the other hand, the metal atoms in the catalyst could bond with the carbon σ bonds, breaking the carbon-carbon bonds. This disrupted the structure of the recombined components in the crude oil, irreversibly reducing the viscosity of the heavy oil and improving its fluidity.

关键词： Nano-sized MOF Petroleum Viscosity reduction Catalyst Nanomaterials

Combined use of fly ash and silica to prevent the long-term strength retrogression of oil well cement set and cured at HPHT conditions

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Petroleum Science 2024年第2期21卷 1122-1134页

作者： Guo-Dong Cheng Xue-Yu Pang Jin-Sheng Sun Zheng-Song Qiu Chuang-Chuang Wang Jian-Kun Qin Ning Li School of Petroleum Engineering China University of Petroleum(East China)Qingdao266580ShandongChina National Key Laboratory of Deep oil and Gas China University of Petroleum(East China)Qingdao266580ShandongChina oil and Gas Engineering Research Institute(Tarim oilfield Company) China National Petroleum CorporationTarim841000XinjiangChina

The long-term strength retrogression of silica-enriched oil well cement poses a significant threat to wellbore integrity in deep and ultra-deep wells, which is a major obstacle for deep petroleum and geothermal energy development. Previous attempts to address this problem has been unsatisfactory because they can only reduce the strength decline rate. This study presents a new solution to this problem by incorporating fly ash to the traditional silica-cement systems. The influences of fly ash and silica on the strength retrogression behavior of oil well cement systems directly set and cured under the condition of 200°C and 50 MPa are investigated. Test results indicate that the slurries containing only silica or fly ash experience severe strength retrogression from 2 to 30 d curing, while the slurries containing both fly ash and silica experience strength enhancement from 2 to 90 d. The strength test results are corroborated by further evidences from permeability tests as well as microstructure analysis of set cement. Composition of set cement evaluated by quantitative X-ray diffraction analyses with partial or no known crystal structure(PONKCS) method and thermogravimetry analyses revealed that the conversion of amorphous C-(A)-S-H to crystalline phases is the primary cause of long-term strength *** addition of fly ash can reduce the initial amount of C-(A)-S-H in the set cement, and its combined use with silica can prevent the crystallization of C-(A)-S-H, which is believed to be the working mechanism of this new admixture in improving long-term strength stability of oil well cement systems.

关键词： Fly ash Long-term strength retrogression High temperature Quantitative X-ray diffraction(QXRD) Partial or no known crystal structure(PONKCS)

Wellbore Cleaning Degree and Hydraulic Extension in Shale oil Horizontal Wells

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Fluid Dynamics & Materials Processing 2024年第3期20卷 661-670页

作者： Xin Ai Mian Chen College of Petroleum Engineering China University of Petroleum(Beijing)BeijingChina Daqing oil Field Company Limited DaqingChina

The efficient development and exploitation of shale oil depends on long-distance horizontal wells. As the degreeof cleaning of the wellbore plays a key role in these processes, in this study, this problem is investigated experimentallyby focusing on the dimensionless cuttings bed height. A method is proposed to calculate the horizontalwellhydraulic extension taking into account the influence of the wellbore cleaning degree on the wellborepressure distribution and assess the effect of a variety of factors such as the bottom hole pressure, the circulatingpressure drop, the drilling pump performance and the formation properties. The analysis shows that the hydraulicextension of horizontal wells decreases with an increase in the cuttings bed height, and the higher the displacementof drilling fluid, the faster the hydraulic extension declines. The annular pressure drop of the horizontalsection increases with the increase of the cuttings bed height, resulting in a higher bottom-hole pressure. Severalarguments are provided to guide the safe drilling of shale oil horizontal wells and overcome the limits of currenttechnological approaches.

关键词： Shale oil horizontal well hydraulic extension wellbore cleaning degree pressure distribution mechanism analysis

Application of fuzzy comprehensive evaluation method to assess effect of conformance control treatments on water-injection wells

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Petroleum 2024年第1期10卷 165-174页

作者： Hu Jia Pengwu Li Wei Lv Jianke Ren Chen Cheng Rui Zhang Zhengjun Zhou Yanbin Liang State Key Laboratory of oil and Gas Reservoir Geology and Exploitation Southwest Petroleum University oil and Gas Technology Research Institute PetroChina Changqing Oilfield Company oil Production Technology Institute of PetroChina Dagang oilfield Company

As an effective method to prolong the life of mature field, conformance control in water-injection well has been used wildly. Naturally, effect evaluation of conformance control has attracted great attention because it is an important guideline for the design of later enhanced oil recovery(EOR) plan. Usually,production responses such as excessive water reduction and oil production increment are widely used as the indicators. However, production responses may be unreliable due to the difficulty in determining an effective injection well which is caused by a large number of treated water-injection wells in a well group. Therefore, with the application of fuzzy comprehension evaluation(FCE), five evaluation indexes(injection pressure, injectivity index, slope of hall curve, variation coefficient and homogenization coefficient of injection profile) describe injection responses were selected to establish a new evaluation method in this paper. Based on fuzzy mathematics, FCE reflects the difference of evaluation ***, weights of evaluation indexes were obtained by analytic hierarchy process(AHP), which made the results more convincing. Taking Bai 239 oilfield as an example, the five injection responses indexes were used to assess treatment effect on five water-injection wells by single index evaluation and FCE. The results showed that among the five evaluation indexes mentioned above, the slope of hall curve was the most important factor affected evaluation result. In single index evaluation, opposite results may be produced easily on account of the one-sidedness of single index or human error. Furthermore, we found that effective treatment was a relative concept actually. The result of FCE was consistent with single index evaluation but FCE was more acceptable. This study suggests that FCE could be applied to another field such as water flooding, acidizing and hydraulic fracturing

关键词： Enhanced oil recovery Injection responses Fuzzy mathematics Analytic hierarchy process Effect evaluation

Study on the Impact of Massive Refracturing on the Fracture Network in Tight oil Reservoir Horizontal Wells

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Fluid Dynamics & Materials Processing 2024年第5期20卷 1147-1163页

作者： Jianchao Shi Yanan Zhang Wantao Liu Yuliang Su Jian Shi Exploration and Development Research Institute Changqing Oilfield CompanyXi’an710018China National Engineering Laboratory for Exploration and Development of Low Permeability oil and Gas Fields Xi’an710018China Key Laboratory of Unconventional oil and Gas Development(China University of Petroleum(East China)) Ministry of EducationQingdao266580China

Class III tight oil reservoirs have low porosity and permeability,which are often responsible for low production rates and limited *** repeated fracturing is a well-known technique to fix some of these *** such methods,existing fractures are refractured,and/or new fractures are created to facilitate communication with natural *** study explored how different refracturing methods affect horizontal well fracture networks,with a special focus on morphology and related fluid flow *** particular,the study relied on the unconventional fracture model(UFM).The evolution of fracture morphology and flow field after the initial fracturing were analyzed *** simulation results indicated that increased formation energy and reduced reservoir stress differences can promote fracture *** was shown that the length of the fracture network,the width of the fracture network,and the complexity of the fracture can be improved,the oil drainage area can be increased,the distance of oil and gas seepage can be reduced,and the production of a single well can be significantly increased.

关键词： Type III tight oil reservoirs refracturing methods horizontal wells fracture network study fracture network evolution

CO_(2)flooding in shale oil reservoir with radial borehole fracturing for CO_(2)storage and enhanced oil recovery

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Petroleum Science 2024年第1期21卷 519-534页

作者： Jia-Cheng Dai Tian-Yu Wang Jin-Tao Weng Kang-Jian Tian Li-Ying Zhu Gen-Sheng Li State Key Laboratory of Petroleum Resources and Prospecting China University of PetroleumBeijing102249China China National oil and Gas Exploration and Development Company Limited Beijing100034China

This study introduces a novel method integrating CO_(2)flooding with radial borehole fracturing for enhanced oil recovery and CO_(2)underground storage,a solution to the limited vertical stimulation reservoir volume in horizontal well fracturing.A numerical model is established to investigate the production rate,reservoir pressure field,and CO_(2)saturation distribution corresponding to changing time of CO_(2)flooding with radial borehole fracturing.A sensitivity analysis on the influence of CO_(2)injection location,layer spacing,pressure difference,borehole number,and hydraulic fractures on oil production and CO_(2)storage is *** CO_(2)flooding process is divided into four *** in layer spacing will significantly improve oil production rate and gas storage ***,serious gas channeling can occur when the spacing is lower than 20 *** the pressure difference between the producer and injector,the borehole number,the hydraulic fracture height,and the fracture width can also increase the oil production rate and gas storage *** analysis shows that layer spacing and fracture height greatly influence gas storage and oil *** outcomes are expected to provide a theoretical basis for the efficient development of shale oil reservoirs in the vertical direction.

关键词： Shale oil Radial borehole fracturing Embedded discrete fracture model Enhanced oil recovery Carbon storage

Impact of Osmotic Pressure on Seepage in Shale oil Reservoirs

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Fluid Dynamics & Materials Processing 2024年第6期20卷 1365-1379页

作者： Lijun Mu Xiaojia Xue Jie Bai Xiaoyan Li Xueliang Han oil and Gas Technology Research Institute PetroChina Changqing Oilfield CompanyXi’an710018China

Following large-scale volume fracturing in shale oil reservoirs,well shut-in measures are generally *** tests and field trials have underscored the efficacy of fracturing fluid imbibition during the shut-in phase in augmenting shale oil *** conventional reservoirs,shale oil reservoirs exhibit characteristics such as low porosity,low permeability,and rich content of organic matter and clay ***,the osmotic pressure effects occurring between high-salinity formation water and low-salinity fracturing fluids are *** current understanding of the mobilization patterns of crude oil in micro-pores during the imbibition process remains nebulous,and the mechanisms underpinning osmotic pressure effects are not fully *** study introduces a theoretical approach,by which a salt ion migration control equation is derived and a mathematical model for spontaneous imbibition in shale is introduced,which is able to account for both capillary and osmotic *** indicate that during the spontaneous imbibition of low-salinity fluids,osmotic effects facilitate the migration of external fluids into shale pores,thereby complementing capillary forces in displacing shale *** considering both capillary and osmotic pressures,the calculated imbibition depth increases by 12%compared to the case where only capillary forces are *** salinity difference between the reservoir and the fracturing fluids significantly influences the imbibition *** for the shutin phase reveal that the pressure between the matrix and fractures reaches a dynamic equilibrium after 28 days of *** the production phase,the maximum seepage distance in the target block is approximately 6.02 m.

关键词： Shale oil osmotic pressure numerical simulation effective seepage distance

Few-layered hexagonal boron nitride nanosheets stabilized Pt NPs for oxidation promoted adsorptive desulfurization of fuel oil

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Green Energy & Environment 2024年第3期9卷 495-506页

作者： Peiwen Wu Xin Song Linlin Chen Lianwen He Yingcheng Wu Duanjian Tao Jing He Chang Deng Linjie Lu Yanhong Chao Mingqing Hua Wenshuai Zhu School of Chemistry and Chemical Engineering Jiangsu UniversityZhenjiang212013China College of Chemical Engineering and Environment State Key Laboratory of Heavy Oil ProcessingChina University of Petroleum-BeijingBeijing102249China College of Chemistry and Chemical Engineering Jiangxi Normal UniversityNanchang330022China College of Science State Key Laboratory of Heavy Oil ProcessingChina University of Petroleum-BeijingBeijing102249China

A few-layered hexagonal boron nitride nanosheets stabilized platinum nanoparticles(Pt/h-BNNS)is engineered for oxidation-promoted adsorptive desulfurization(OPADS)of fuel *** was found that the few-layered structure and the defective sites of h-BNNS not only are beneficial to the stabilization of Pt NPs but also favor the adsorption of aromatic *** employing Pt/h-BNNS with a Pt loading amount of 1.19 wt%as the active adsorbent and air as an oxidant,a 98.0%sulfur removal over dibenzothiophene(DBT)is achieved along with a total conversion of the DBT to the corresponding sulfones(DBTO_(2)).Detailed experiments show that the excellent desulfurization activity originates from the few-layered structure of h-BNNS and the high catalytic activity of Pt *** addition,the OPADS system with Pt/h-BNNS as the active adsorbent shows remarkable stability in desulfurization performance with the existence of different interferents such as olefin,and aromatic ***,the Pt/h-BNNS can be recycled 12 times without a significant decrease in desulfurization ***,a process flow diagram is proposed for deep desulfurization of fuel oil and recovery of high value-added products,which would promote the industrial application of such OPADS strategy.

关键词： Desulfurization Adsorption Catalytic oxidation Active adsorbent Dibenzothiophene