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Insights into in-situ imbibition behavior of fracturing fluid in propped shale fractures based on nuclear magnetic resonance:A case study from Longmaxi Formation shale,Sichuan Basin,China

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petroleum Science 2024年第1期21卷 410-429页

作者： Jing-Jing Guo Kai-Xiang Di Lie-Hui Zhang Yu-Long Zhao Hui-Ying Tang Rui-Han Zhang Ye Tian National key laboratory of Oil and Gas Reservoir geology and Exploitation Southwest Petroleum UniversityChengdu610500SichuanChina

Shale gas is an important component of unconventional oil and gas *** the imbibition behavior is helpful to optimize flowback parameters and enhance gas *** imbibition studies have focused on shale matrix,and the pressure conditions discussed were mostly *** initial imbibition behavior begins from propped fractures to matrix,but there are few studies working on explaining the imbibition behavior in propped fractures or the phenomenon of many shale wells exhibit higher productivity after a“soaking”***,propped fracture samples were designed for imbibition and migration *** order to accurately study the mechanism and main influencing factors of fracturing fluid imbibition and migration in propped and unpropped shale fractures under high temperature and high pressure,a series of experiments based on nuclear magnetic resonance(NMR)were carried *** showed that NMR T_(2) spectra of all samples exhibited a bimodal *** final imbibition volume of fracturing fluid was positively related to pressure and fracture *** imbibition effect of fracturing fluid was more evident in matrix pores under high *** the migration during soaking stage,the fracturing fluid gradually migrated from large pores to small pores and gradually displaced the shale gas from the matrix,thus allowing the water blocking in propped fractures to self-unlock to some *** permeability decreased in the imbibition stage,while it recovered in the migration stage to some extent.

关键词： Forced imbibition Migration Soaking NMR T_(2)spectra Propped fracture Permeability recovery

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Mottled dolomite in the lower Cambrian Longwangmiao formation in the Northern Sichuan Basin, South China

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petroleum 2024年第1期10卷 19-29页

作者： Xuefei Yang Hao Tang Junyi Zhang Yao Du Ruifeng Tang Shuang Pan Xiang Zhou Yan Xu State key laboratory of Oil and Gas Reservoir geology and Exploitation Southwest Petroleum University Sichuan Provincial key laboratory of Gas geology Southwest Petroleum University CCDC Chuandong Drilling Company Exploration Department Petrochina Southwest Oil& Gasfield Company

At the end of Early Cambrian time, the Sichuan basin（South China） was located in a wide carbonate platform, with hundreds of meters of carbonate deposited. The Longwangmiao Formation carbonate in Sichuan basin is partially to completely dolomitized, displaying a mottled texture in the northern area of the exposure. The mottled dolomitic limestone developed parallel to bedding, with shape irregular boundaries with limestone that has not been dolomitized. The mottled dolomite is composed of powder crystalline and finely crystalline dolomite, while the matrix limestone is composed of micritic calcite. the isotopic composition of mottled dolomite(δ13C = +0.29‰PDB, δ18O =-1.15‰PDB) is similar to that of micrite calcite(δ13C =-0.49‰PDB, δ18O =-1.45‰PDB). Both isotopic values and trace element data indicate that the dolomitized fluid is originated from sea water. Some beds contain gypsum pseudomorphs and mud cracks, indicating a shallow and evaporative environment with local high salinity during deposition. Dolomitization likely took place early, in part as a result of sea water salinity concentration. Trace fossils thalassinoides horizontalis, thalassinoides callianassa and planolites developed in the Longwangmiao Formation, and the sharp edges of mottled dolomite are similar to these trace fossils. The beds are intensely bioturbated. In the burrow network, the sediments and burrow fill were coarse and loose with little clay, and it is interpreted here as being easier to be dolomitized than the surrounding *** dolomitization is thus interpreted to have occurred in the burrow system, and the degree of dolomitization was related to the degree of bioturbation, which is controlled by the trace-making creatures.

关键词： Mottled dolomite Dolomitization Longwangmiao Formation Early Cambrian Northern Sichuan basin

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Experimental investigation on pyrolysis products and pore structure characteristics of organic-rich shale heated by supercritical carbon dioxide

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petroleum Science 2024年第4期21卷 2393-2406页

作者： Bai-Shuo Liu Chuan-Jin Yao Jia-Long Qi Ya-Qian Liu Liang Xu Jing-Xuan Hou State key laboratory of Deep Oil and Gas China University of Petroleum (East China) key laboratory of unconventional Oil & Gas Development (China University of petroleum (East China)) Ministry of Education School of petroleum Engineering China University of Petroleum (East China)

The efficient pyrolysis and conversion of organic matter in organic-rich shale,as well as the effective recovery of pyrolysis shale oil and gas,play a vital role in alleviating energy *** state of carbon dioxide（CO2） in the pyrolysis environment of shale reservoirs is the supercritical *** unique supercritical fluid properties not only effectively heat organic matter,displace pyrolysis products and change shale pore structure,but also achieve carbon storage to a certain *** samples were made into powder and three sizes of cores,and nitrogen（N2） and supercritical carbon dioxide（ScCO2）pyrolysis experiments were performed at different final pyrolysis *** properties and mineral characteristics of the pyrolysis products were studied based on gas chromatography analysis,Xray diffraction tests,and mass spectrometry ***,the pore structure characteristics at different regions of cores before and after pyrolysis were analyzed using N2adsorption tests to clarify the impact of fracturing degree on the pyrolysis *** results indicate that the optimal pyrolysis temperature of Longkou shale is about 430℃.Compared with N2,the oil yield of ScCO2pyrolysis is *** pyrolysis oil obtained by ScCO2extraction has more intermediate fractions and higher relative molecular *** ScCO2can effectively improve the pore diameter of shale and its effect is better than that of *** micropores are produced in shale after pyrolysis,and the macropores only are generated in ScCO2pyrolysis environments with temperatures greater than 430℃.The pore structure has different development characteristics at different pyrolysis temperatures,which are mainly affected by the pressure holding of volatile matter and products *** to the surface of the core,the pore development effect inside the core is *** the decrease in core size,the pore diameter,specific surface area,and pore volume of cores all increase after pyrolysis.

关键词： Organic-rich shale Supercritical carbon dioxide In-situ pyrolysis Pore structure Core size and region

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Risk Assessment of Deep-Water Horizontal X-Tree Installation

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China Ocean Engineering 2024年第2期38卷 210-220页

作者： MENG Wen-bo FU Guang-ming HUANG Yi LIU Shu-jie HUANG Liang GAOYong-hai CNOOC China Limited Zhanjiang BranchZhanjiang 524057China key laboratory of unconventional Oil and Gas Development Ministry of Education(China University of Petroleum(East China))Qingdao 266580China

Due to the high potential risk and many influencing factors of subsea horizontal X-tree installation,to guarantee the successful completion of sea trials of domestic subsea horizontal X-trees,this paper established a modular risk evaluation model based on a fuzzy fault ***,through the analysis of the main process oftree down and combining the Offshore&Onshore Reliability Data(OREDA)failure statistics and the operation procedure and the data provided by the job,the fault tree model of risk analysis of the tree down installation was ***,by introducing the natural language of expert comprehensive evaluation and combining fuzzy principles,quantitative analysis was carried out,and the fuzzy number was used to calculate the failure probability of a basic event and the occurrence probability of a top ***,through a sensitivity analysis of basic events,the basic events of top events significantly affected were determined,and risk control and prevention measures for the corresponding high-risk factors were proposed for subsea horizontal X-tree down installation.

关键词： subsea horizontal X-tree risk assessment fuzzy fault tree modular risk evaluation model

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Geological conditions and reservoir characteristics of various shales in major shalehosted regions of China

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China geology 2024年第1期7卷 138-149页

作者： Shu-jing Bao Tian-xu Guo Jin-tao Yin Wei-bin Liu Sheng-jian Wang Hao-han Li Zhi Zhou Shi-zhen Li Xiang-lin Chen the key laboratory of unconventional petroleum geology China Geological SurveyMinistry of Natural Resources100083 BeijingChina Oil and Gas Survey China Geological Survey100083 BeijingChina Research Institute of Yanchang petroleum(Group)CO.LTD 710076 Xi’anChina

China is home to shales of three facies:Marine shale,continental shale,and marine-continental transitional *** types of shale gas are associated with significantly different formation conditions and major controlling *** study compared the geological characteristics of various shales and analyzed the influences of different parameters on the formation and accumulation of shale *** general,shales in China’s several regions exhibit high total organic carbon(TOC)contents,which lays a sound material basis for shale gas *** strata generally show high degrees of thermal *** contrast,continental shales manifest low degrees of thermal evolution,necessitating focusing on areas with relatively high degrees of thermal evolution in the process of shale gas surveys for these *** shales of the Wufeng and Silurian formations constitute the most favorable shale gas reservoirs since they exhibit the highest porosity among the three types of *** shales are followed by those in the Niutitang and Longtan *** contrast,the shales of the Doushantuo,Yanchang,and Qingshankou formations manifest low ***,the shales of the Wufeng and Longmaxi formations exhibit high brittle mineral *** a low siliceous mineral content,the shales of the Doushantuo Formation feature a high carbonate mineral content,which can increase the shales’brittleness to some *** marine-continental transitional shales,where thin interbeds of tight sandstone with unequal thicknesses are generally found,it is recommended that fracturing combined with drainage of multiple sets of lithologic strata should be employed to enhance their shale gas production.

关键词： Shale gas Marine shale Continental shale Marine-continental transitional shale Neoproterozoic-Cretaceous strata Geological conditions Reservoir characteristics petroleum geological survey engineering

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Linearized waveform inversion for vertical transversely isotropic elastic media:Methodology and multi-parameter crosstalk analysis

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petroleum Science 2024年第1期21卷 252-271页

作者： Ke Chen Lu Liu Li-Nan Xu Fei Hu Yuan Yang Jia-Hui Zuo Le-Le Zhang Yang Zhao National key laboratory of petroleum Resources and Engineering Unconventional Petroleum Research InstituteChina University of Petroleum(Beijing)Beijing102249China Aramco Beijing Research Center Aramco AsiaBeijing100102China University of Lausanne LausanneCH-1015Switzerland Bureau of Geophysical Prospecting China National Petroleum CorporationZhuozhou 072750HebeiChina

Seismic migration and inversion are closely related techniques to portray subsurface images and identify hydrocarbon *** migration aims at obtaining structural images of subsurface geologic *** specifically,seismic migration estimates the reflectivity function(stacked average reflectivity or pre-stack angle-dependent reflectivity)from seismic reflection *** the other hand,seismic inversion quantitatively estimates the intrinsic rock properties of subsurface *** seismic inversion methods are applicable to detect hydrocarbon reservoirs that may exhibit lateral variations in the inverted *** there exist many differences,pre-stack seismic migration is similar with the first iteration of the general linearized seismic ***,seismic migration and inversion techniques assume an acoustic or isotropic elastic *** reservoirs such as shale and tight sand formation have notable anisotropic *** present a linearized waveform inversion(LWI)scheme for weakly anisotropic elastic media with vertical transversely isotropic(VTI)*** is based on two-way anisotropic elastic wave equation and simultaneously inverts for the localized perturbations(ΔVp_(0)/Vp_(0)/Vs_(0)/Vs_(0)/,Δ∈,Δδ)from the long-wavelength reference *** proposed VTI-elastic LWI is an iterative method that requires a forward and an adjoint operator acting on vectors in each *** derive the forward Born approximation operator by perturbation theory and adjoint operator via adjoint-state *** inversion has improved the quality of the images and reduces the multi-parameter crosstalk comparing with the adjoint-based *** have observed that the multi-parameter crosstalk problem is more prominent in the inversion images for Thomsen anisotropy ***,the Thomsen parameter is the most difficult to *** also analyze the multi-parameter crosstalk using scattering radiation patte

关键词： Elastic Anisotropy Least-squares imaging Waveform inversion Computational geophysics

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Dynamic evaluation on sealing capacity of caprocks of the Meso-Neoproterozoic reservoirs in Ordos Basin,China

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Energy Geoscience 2024年第1期5卷 99-107页

作者： Yusong Yuan Yunqin Hao Rongqiang Zhang key laboratory of geology and Resources in Deep Stratum Petroleum Exploration and Production Research InstituteSINOPECBeijing 102206China

The Meso-Neoproterozoic is a new play in the Ordos Basin.A deeper understanding about the dynamic relationship between the caprocks and the source rocks is *** on the comprehensive analysis of hydrocarbon source development characteristics of the Meso-Neoproterozoic and its overlying strata,as well as the formation contact relationships,lithology characteristics and exploratory drilling data,it is recognized that the Meso-Neoproterozoic contains two types of petroleum accumulation assemblage,that is,the“self-sourced indigenous”and“upper source rock-lower reservoir”*** former is mainly controlled by the development and distribution of source rocks of the Changcheng System,with the Lower Cambrian shale sequence as its *** later is controlled by the superposition between the Meso-Neoproterozoic and its overlying source rocks and this assemblage is mainly distributed in Hangjinqi and Pingliang areas with the Carboniferous-Permian shale sequence as its *** dynamic evaluation on the displacement pressure serves to reconstruct the displacement pressure history of the *** results show that the shale sequence of the Cambrian Maozhuang Formation in well XY 1 in the southern Ordos Basin has possibly acquired the ability of sealing natural gas since the early of Late *** displacement pressure increased rapidly up to 20 MPa during the Late Triassic-Jurassic and keeps at 9.2 MPa at present,indicating fair sealing *** Carboniferous-Permian caprocks in Hangjinqi area could have acquired the ability to seal natural gas in the Late Jurassic-Early Cretaceous,and the present-day displacement pressure is 9e12 MPa,indicating good sealing *** upper Paleozoic caprock in Pingliang area has been able to seal natural gas since the Early Jurassic,with a maximum displacement pressure of 23 MPa during the Cretaceous period and a current value of 17 e20 MPa,indicative of strong ability to seal natural *** sealing ability of

关键词： Ordos Basin Meso-Neoproterozoic Caprock sealing ability Displacement pressure

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Vibration Control of A Flexible Marine Riser System Subject to Input Dead Zone and Extraneous Disturbances

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China Ocean Engineering 2024年第2期38卷 271-284页

作者： ZHOU Li WANG Guo-rong WAN Min School of Mechatronic Engineering Southwest Petroleum UniversityChengdu 610500China Energy Equipment Institute Southwest Petroleum UniversityChengdu 610500China National key laboratory of Oil and Gas Reservoir geology and Exploitation Southwest Petroleum UniversityChengdu 610500China

An observer-based adaptive backstepping boundary control is proposed for vibration control of flexible offshore riser systems with unknown nonlinear input dead zone and uncertain environmental *** control algorithm can update the control law online through real-time data to make the controller adapt to the environment and improve the control ***,based on the adaptive backstepping framework,virtual control laws and Lyapunov functions are designed for each *** direction interference observers are designed to track the timevarying boundary *** this basis,the inverse of the dead zone and linear state transformation are used to compensate for the original system and eliminate the adverse effects of the dead *** addition,the stability of the closed-loop system is proven by Lyapunov stability *** the system states are bounded,and the vibration offset of the riser converges to a small area of the initial ***,four examples of flexible marine risers are simulated in MATLAB to verify the effectiveness of the proposed controller.

关键词： adaptive backstepping control disturbance observer flexible marine riser input dead zone vibration control

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Investigation of pore structure alteration and permeability enhancement of shale matrix by supercritical water treatment after hydraulic fracturing

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petroleum 2024年第2期10卷 265-274页

作者： Yili Kang Peisong Li Wangkun Cao Mingjun Chen Lijun You Jiang Liu Zhehan Lai State key laboratory of Oil and Gas Reservoir geology and Exploitation Southwest Petroleum University Institute of Engineering Technology PetroChina Coalbed Methane Company Limited Chemical and petroleum Engineering University of Calgary

Shale gas reservoirs are unconventional tight gas reservoirs, in which horizontal wells and hydraulic fracturing are required to achieve commercial development. The fracture networks created by hydraulic fracturing can increase the drainage area extensively to enhance shale gas recovery. However, large volumes of fracturing fluid that is difficult to flow back to the surface and remained in the shale formation, will inevitably lead to damages of the shale formations and limit the effectiveness of *** water(SCW) treatment after hydraulic fracturing is a new method to enhance shale gas recovery by using appropriate heat treatment methods to the specific formation to convert the retained fracturing fluid into a supercritical state(at temperatures in excess of 373.946°C and pressures in excess of 22.064 MPa). An experiment was conducted to simulate the reaction between shale and SCW, and the capacity of SCW treatment to enhance the permeability of the shale was evaluated by measuring the response of the shale porosity and permeability on SCW treatment. The experimental results show that the shale porosity and permeability increase by 213.43% and 2198.37%, respectively. The pore structure alteration and permeability enhancement of the shale matrix were determined by analyzing the changes in pore structure and mineral composition after SCW treatment. The mechanisms that affect pore structure and mineral composition include oxidative catalysis decomposition of organic matters and reducing minerals, acid-catalyzed decomposition of carbonate minerals and feldspar minerals, hydrothermal catalysis induced fracture extension and cementation weakening induced fracture *** treatment converts harm into a benefit by reducing the intrusion of harmful substances into the shale formation, which will broaden the scope and scale of shale formation stimulation.

关键词： Shale gas Formation damage control Formation heat treatment Supercritical water

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Development review and the prospect of oil shale in-situ catalysis conversion technology

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petroleum Science 2024年第2期21卷 1385-1395页

作者： Li Wang Chen-Hao Gao Rui-Ying Xiong Xiao-Jun Zhang Ji-Xiang Guo The unconventional Oil and Gas Institute China University of Petroleum-BeijingBeijing102200China

As an unconventional resource, oil shale possesses abundant reserves and significant potential for industrial applications. The rational and efficient development of oil shale resources holds immense importance in reducing national energy demand. In-situ catalytic technology, characterized by its high efficiency, low pollution, and minimal energy consumption, represents a key direction for future oil shale development. This paper provides a comprehensive review of research progress in in-situ oil shale mining technology, oil shale pyrolysis catalysts, the pyrolysis mechanism of kerogen, and the compatibility of different heating processes and catalysts. Furthermore, the paper proposes future research directions and prospects for oil shale in-situ catalytic technology, including reservoir modification, highefficiency catalyst synthesis, injection processes, and high-efficiency heating technology. These insights serve as valuable technical references for the advancement of oil shale in-situ catalytic technology.

关键词： Oil shale In-situ catalytic technology Pyrolysis catalyst Kerogen pyrolysis mechanism

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