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Multiple metal sources in polymetallic W-Sn ore deposits revealed by mercury stable isotopes

Science China Earth Sciences 2024年第11期67卷 3465-3475页

作者： Zhendong TIAN Bernd LEHMANN Changzhou DENG Xingchun ZHANG Anbo LUO Yinghua CHEN Runsheng YIN state key laboratory of ore deposit geochemistry Institute of Geochemistry Chinese Academy of Sciences Mineral Resources Technical University of Clausthal Faculty of Land Resource Engineering Kunming University of Science and Technology

Granite-related W-Sn ore systems are commonly associated with coeval Pb-Zn mineralization. It remains unclear whether these metals are derived from the same sources or not. Mercury（Hg） is a common minor component in such systems. Hg isotopes undergo unique mass-independent fractionation(expressed as Δ199Hg values), which is mainly generated during Hg photochemical reactions on Earth's surface and not affected by magmatic-hydrothermal processes, offering an excellent opportunity to trace metal sources in hydrothermal systems. We observed near-zero Δ199Hg values in wolframite（-0.10‰ to0.08‰, n=11）, and in skarn-（-0.17‰ to 0.12‰, n=48） and greisen-type（-0.12‰ to 0.10‰, n=11） bulk tin-tungsten ore from eight major ore deposits in South China. These values are identical to those of coeval highly evolved granites（-0.13‰ to 0.12‰,n=49）, supporting that Hg in W-Sn ores were sourced from granite. However, sulfides（e.g., pyrite, chalcopyrite, arsenopyrite,galena, and sphalerite） in these deposits exhibit negative to near-zero Δ199Hg values（-0.42‰ to 0.09‰, n=124）, which indicates a contribution of Hg and by inference other metals from both Precambrian basement rocks(Δ199Hgore-related *** study demonstrates that multiple sources of metals were involved in the formation of the polymetallic W-Sn deposits, and further highlights that extraction of metals from basement rocks may be a critical control on the formation of economically important mineralization of base metal sulfides（e.g., Pb, Zn） in granite-related magmatic-hydrothermal systems.

关键词： Tin-tungsten deposit Mercury isotope Metal source Metal zonation South China

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Age and petrogenesis of the newly discovered Early Permian granite in the Kumtor gold field， Kyrgyz Tien-Shan

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Journal of Earth Science 2024年

作者： Kyiazbek Asilbekov Rustam Orozbaev Etienne Skrzypek Christoph Hauzenberger Elena Ivleva Daniela Gallhofer Jian-Feng Gao Nikolay Pak Anatoliy Shevkunov Anatoliy Bashkirov Aizat Zhaanbaeva Institute of Geology， National Academy of Sciences of the Kyrgyz Republic Institute of Earth Sciences， University of Graz state key laboratory of ore deposit geochemistry， Institute of geochemistry， Chinese Academy of Sciences Kumtor Gold Company CJSC

Permian intrusions are widespread in the Middle and Southern Tien Shan， with fewer occurrences in the Northern Tien-Shan. Notably， many of these intrusions are spatially associated with a variety of ore deposits， indicating a significant link between magmatic activity and mineralization processes in these areas. We studied granite samples recently recovered from drilling in the Kumtor gold field to evaluate their potential relationships with gold mineralization. We report major and trace element geochemistry， zircon U-Pb age and Hf isotope data for this so-called Kumtor granite. The Kumtor granite is metaluminous to peraluminous and belongs to the high-K and calc-alkaline series with I-type geochemical characteristics. The relatively high K2O and Na2O concentrations and low high field strength elements （HFSE） and heavy rare earth elements （HREE）， the presence of biotite within these I-type granites， together with their low zircon saturation temperatures （731–779 °C）， suggest that they were likely derived from a hydrous source formed by dehydration melting of mica-bearing， medium- to high-K metabasaltic rocks. Our zircon U-Pb dating results indicate that the Kumtor granite intruded at 293 ± 1.7 Ma， which is consistent with the age range of other Middle Tien-Shan granitoids. The zircon Hf isotopic composition is εHf（t）= –7.56 to –5.05， indicating an ancient （1.39 to 1.52 Ga） crustal origin. Petrographical， geochemical and geochronological data indicate that the Kumtor granite is similar to leuco-granites of the Terekty complex. Our results indicate that the Kumtor granite was emplaced in the early Permian in a post-collision setting and may have temporal and genetic relationships with gold mineralization.

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Metallogenesis of the Baidi Au-Sb deposit, southwest Guizhou Province, China: mineralogical and geochemical evidence from sulfur-bearing minerals

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Acta Geochimica 2024年第2期43卷 199-213页

作者： Jun Yan Yong Xia Qinping Tan Zhuojun Xie Guosong Ji state keylaboratory of ore deposit geochemistry Institute of GeochemistryChineseAcademy of SciencesGuiyang 550081China Guizhou InstituteofTechnology Guiyang550003China No.102 GeologicalTeam Guizhou Bureau of Geologyand Mineral Exploration&DevelopmentZunyi563003China

The Baidi Au-Sb deposit, which contains 8 t of Au and 10,979 Mt of Sb, is a typical and rare paragenetic deposit located in southwestern Guizhou Province, *** studies have focused on individual ores, but have not combined them to identify their paragenetic mechanism or metallogenic regularity. Therefore, we used field investigations, microscopic observations, and in situ analyses to identify the spatial distribution, mineral paragenesis, compositional evolution, and metallogenic material sources of the ore bodies. We also determined the Au and Sb paragenetic characteristics and the metallogenesis of the deposit. The main Au-bearing minerals in the deposit were early(Apy1–2) and late(Apy3) stage arsenopyrites, as well as pre-mineralization(Py1), mineralization(Py2–5), and late mineralization(Py6–7) stage pyrites. The main Sb-bearing minerals were stibnite(Snt), skinnerite, bournonite,and valentinite. The minerals formed in the order of Py1,Py2–3 + Apy1, Py4–5 + Apy2, Snt, and Py6–7 + *** δ34S values of the arsenopyrites and pyrites ranged from-5 to 5‰, while those of stibnite were mostly less than-5‰ in the later mineralization stages. Sulfur was provided by deep magmatic hydrothermal fluids, but sedimentary sulfur was added in the later stages. Moreover,the trace elemental contents fluctuated and eventually became similar to those of the sedimentary strata. By comprehensively considering the ores along with the geological characteristics of the deposit, we determined that deep magma provided the Au during ore formation. Later tectonic changes provided Sb from the sedimentary strata,which precipitated along fault expansion areas and produced Au and Sb paragenesis.

关键词： Au-Sb mineralization Arsenopyrite Pyrite Stibnite Metallogenetic process

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The Weixi High-silica Granitoids in the Central Sanjiang Orogenic Belt,Southwest China:Implications for Growth of the Continental Crust

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Acta Geologica Sinica(English Edition) 2024年第3期98卷 641-656页

作者： WANG Qiuyu CHEN Shouming ZHANG Hongrui LI Saisai SinoProbe laboratory Institute of GeologyChinese Academy of Geological SciencesBeijing 100037China Guangxi key laboratory of Hidden Metallic ore deposit Exploration GuilinGuangxi 541004China

High-silica granitoids record the formation and evolution of the continental crust.A new intrusive complex has been recognized among silicic volcanic rocks of the Weixi arc,Southwest *** intrusions consist of granites,granitic porphyries,and *** U-Pb age data indicate that the Weixi granitoids formed at 248-240 Ma and were coeval with silicic volcanic rocks of the Weixi *** Weixi granitoids are enriched in Rb,Th,and U,depleted in Ba,Sr,Nb,Ta,and Ti,and have high light/heavy rare earth element ratios and slightly negative Eu *** Weixi granitoids have negative ε_(Nd)(t)values(-9.8 to-7.8)and negative zircon ε_(Hf)(t)values(-12.02 to-5.11).The geochemical and isotopic features suggest the Weixi granitoids were derived by partial melting of ancient crustal *** Weixi granitoids and silicic volcanic rocks were derived from the same magma by crystal accumulation and melt extraction,respectively,and they record the formation of a continental arc in the central Sanjiang orogenic belt.

关键词： granitoids geochemistry crystal accumulation continental crust Sanjiang orogen

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Dating Kimberlite Using Apatite U-Pb Geochronology: A Case Study from Diamond-Bearing Dikes in South China

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Journal of Earth Science 2024年第3期35卷 1059-1062页

作者： Jiawei Zhang Huan Wang Defeng He Yuhua Zhu Kun Wang Yuan Qiu Guizhou Geological Survey Bureau of Geology and Mineral Exploration and Development of Guizhou ProvinceGuiyang 550081China College of Resources and Environmental Engineering Guizhou UniversityGuiyang 550025China Yanduzhongshi Geological Analysis laboratory Ltd. Beijing 100080China state key laboratory of ore deposit geochemistry Institute of GeochemistryChinese Academy of SciencesGuiyang 550081China

Kimberlite,one of the deepest known magmatic rocks on Earth,offers valuable glimpses into the deep mantle composition(Woodhead et al.,2019),craton structure(Gardiner et al.,2020),global geodynamic variation(Tappe et al.,2018),and diamond formation(Giuliani et al.,2023).The accurate determination of the emplacement of this special rock is crucial for revealing such ***,dating kimberlite is challenging due to its silica-poor,volatile-rich,strongly altered,and hybrid nature(Mitchell et al.,2019).Zircon is unsuitable for dating kimberlite and related rocks due to its preference for crystallizing in intermediate to felsic melts(Gervasoni et al.,2016)rather than silica-poor *** if present,zircon is prone to Pb loss through hydrothermal alteration(Zi et al.,2022)in a volatile-rich system like kimberlitic magmas.

关键词： dating magma alteration

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Multiple Uplift and Exhumation of the Southeastern Tibetan Plateau:Evidence from Low-Temperature Thermochronology

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Acta Geologica Sinica(English Edition) 2024年第3期98卷 569-584页

作者： WU Limin PENG Touping FAN Weiming ZHAO Guochun GAO Jianfeng DONG Xiaohan PENG Shili MIN Kang Tin Aung MYINT state key laboratory of Isotope geochemistry Guangzhou Institute of GeochemistryChinese Academy of SciencesGuangzhou 510640China Chinese Academy of Sciences Center for Excellence in Deep Earth Science Guangzhou 510640China University of Chinese Academy of Sciences Beijing 100049China Chinese Academy of Sciences Center for Excellence in Tibetan Plateau Earth Sciences Beijing 100101China Department of Earth Sciences The University of Hong KongHong Kong 999077China state key laboratory of ore deposit geochemistry Institute of GeochemistryChinese Academy of SciencesGuiyang 550081China Southern Marine Science and Engineering Guangdong laboratory(Zhuhai) ZhuhaiGuangdong 519085China Department of Geology University of MandalayMandalay 05011Myanmar

Since the Cenozoic,the Tibetan Plateau has experienced large-scale uplift and outgrowth due to the India-Asia ***,the mechanism and timing of these tectonic processes still remain ***,using apatite fission track dating and inverse thermal modeling,we explore the mechanism of different phases of rapid cooling for different batholiths and intrusions in the southeastern Tibetan *** contrast to previous views,we find that the coeval granitic batholith exposed in the same tectonic zone experienced differential fast uplift in different sites,indicating that the present Tibetan Plateau was the result of differential uplift rather than the entire lithosphere uplift related to lithospheric collapse during Cenozoic *** addition,we also suggest that the 5-2 Ma mantle-related magmatism should be regarded as the critical trigger for the widely coeval cooling event in the southeastern Tibetan Plateau,because it led to the increase in atmospheric CO_(2)level and a hotter upper crust than before,which are efficient for suddenly fast rock weathering and ***,we propose that the current landform of the southeastern Tibetan Plateau was the combined influences of tectonic and climate.

关键词： apatite fission track rapid cooling differential uplift magmatism southeastern Tibetan Plateau

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High-pressure minerals and new lunar mineral changesite-(Y) in Chang’e-5 regolith

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Matter and Radiation at Extremes 2024年第2期9卷 90-97页

作者： Jing Yang Wei Du Center for Lunar and Planetary Sciences Institute of GeochemistryChinese Academy of SciencesGuiyang 550081China state key laboratory of ore deposit geochemistry Institute of GeochemistryChinese Academy of Sciences(CAS)Guiyang 550081China CAS Center for Excellence in Comparative Planetology Hefei 230026China

Forty-five years after the Apollo and Luna missions, China’s Chang’e-5 (CE-5) mission collected ∼1.73 kg of new lunar materials from one ofthe youngest basalt units on the Moon. The CE-5 lunar samples provide opportunities to address some key scientific questions related to theMoon, including the discovery of high-pressure silica polymorphs (seifertite and stishovite) and a new lunar mineral, changesite-(Y). Seifertitewas found to be coexist with stishovite in a silica fragment from CE-5 lunar regolith. This is the first confirmed seifertite in returned lunarsamples. Seifertite has two space group symmetries (Pnc2 and Pbcn) and formed from an α-cristobalite-like phase during “cold” compressionduring a shock event. The aftershock heating process changes some seifertite to stishovite. Thus, this silica fragment records different stagesof an impact process, and the peak shock pressure is estimated to be ∼11 to 40 GPa, which is much lower than the pressure condition forcoexistence of seifertite and stishovite on the phase diagram. Changesite-(Y), with ideal formula (Ca_(8)Y)◻Fe^(2+)(PO_(4))_(7) (where ◻ denotes avacancy) is the first new lunar mineral to be discovered in CE-5 regolith samples. This newly identified phosphate mineral is in the form ofcolumnar crystals and was found in CE-5 basalt fragments. It contains high concentrations of Y and rare earth elements (REE), reaching upto ∼14 wt. % (Y,REE)2O3. The occurrence of changesite-(Y) marks the late-stage fractional crystallization processes of CE-5 basalts combinedwith silicate liquid immiscibility. These new findings demonstrate the significance of studies on high-pressure minerals in lunar materials andthe special nature of lunar magmatic evolution.

关键词： evolution minerals basalt

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撞击过程对月表氧逸度的改造:来自嫦娥五号月壤中撞击玻璃珠的启示

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Science Bulletin 2024年第10期69卷 1495-1505页

作者：庞润连杨晶李瑞刘世荣李琼朱丹杜蔚刘耘 state key laboratory of ore deposit geochemistry Institute of GeochemistryChinese Academy of SciencesGuiyang 550081China Center for Lunar and Planetary Sciences Institute of GeochemistryChinese Academy of SciencesGuiyang 550081China state key laboratory of Environmental geochemistry Institute of GeochemistryChinese Academy of SciencesGuiyang 550081China College of Earth and Planetary Sciences University of Chinese Academy of SciencesBeijing 101408China Center for Excellence in Comparative Planetology Chinese Academy of SciencesHefei 230026China Research Center for Planetary Science College of Earth ScienceChengdu University of TechnologyChengdu 610059China

Lunar materials are overall more reducing compared with their terrestrial counterparts,but the mechanism remains to be *** this study,we present a possible explanation for the changes in redox state of the lunar regolith caused by impact events,based on our investigations of the impact glass beads from Chang’e-5 *** glass beads contain iron metal grains and show concentration gradients of FeO and K_(2)O(with or without Na_(2)O)from their rims to *** compositional profiles exhibit errorfunction-like shapes,which indicates a diffusion-limited *** numerical modeling results suggest that the iron metal grains on the surface of the glass beads were generated through the reduction of FeO by elemental K and(or)Na produced during the impact ***,the iron metal grains inside the bead may have formed due to oxygen diffusion driven by redox potential ***,our study suggests that impact processes intensify the local reducing conditions,as evidenced by the presence of calcium sulfide particles within troilite grains that coexist with iron metal grains on the surface of the glass *** study provides insights into the oxygen diffusion kinetics during the formation of iron metal spherules and sheds light on the changes in redox conditions of lunar materials caused by impact events.

关键词： Chang’e-5 Lunar sample Glass beads Impact Oxygen fugacity Redox change

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Permian tectonic evolution and continental accretion in the eastern Central Asian Orogenic Belt:A perspective from the intrusive rocks

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Geoscience Frontiers 2024年第2期15卷 433-451页

作者： Anzong Fu Hongyan Geng Changzhou Deng Chenglu Li Jishuang Ding Bizheng Yang Wenpeng Yang Heilongjiang Institute of Natural Resources Survey Harbin 150036China state key laboratory of ore deposit geochemistry Institute of GeochemistryChinese Academy of SciencesGuiyang 550002China Science Unit Lingnan UniversityHong KongChina College of Earth Sciences Jilin UniversityChangchun 130061China

The tectonic evolution and history of continental accretion of the eastern Central Asian Orogenic Belt(CAOB)are not yet fully *** this study,we investigate Permian intrusive rocks from the Jiamusi Block of the eastern CAOB to constrain the tectonic evolution and continental accretion of this region during the late-stage evolution of the Paleo-Asian *** new data show that Early Permian gabbro-diorites were derived from the partial melting of depleted mantle metasomatized by oceanic-slab-released *** Permian adakitic granites have low Na2O and MgO and high K2O contents,indicating a thickened-lower-crust *** Permian S-type granites were derived from the partial melting of continental crust.A compilation of the available geochronological data for Permian intrusive rocks(including adakitic and A-,S-,and I-type granites and mafic rocks)from the eastern CAOB reveals that the A-type granites formed mainly during the Early–Middle Permian,S-type and adakitic granites mostly during the Middle–Late Permian,and I-type granites and mantle-derived mafic rocks throughout the *** A-type granites,which are proposed to have been sourced from thinned continental crust,indicate an extensional setting in the eastern CAOB during the Early *** Middle–Late Permian adakitic granites imply a thickened continental crust,which indicates a compressional ***,the eastern CAOB underwent a transition from extension to compression during the Middle Permian,which was probably triggered by the late-stage subduction of Paleo-Asian oceanic *** the petrogenesis of the intrusive rocks and inferred regional tectonic evolution of the eastern CAOB,we propose that vertical underplating of mantle-and oceanic-slabderived magmas contributed the materials for continental crust accretion.

关键词： Permian Intrusive rocks Eastern Central Asian Orogenic Belt Paleo-Asian Ocean Tectonic evolution

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Zircon U-Pb Ages and Sr-Nd-Hf Isotopic Characteristics of the Huichizi Granitic Complex in the North Qinling Orogenic Belt and Their Geological Significance

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Journal of Earth Science 2018年第3期29卷 492-507页

作者： Youwei Chen Ruizhong Hu Xianwu Bi Shaohua Dong Yue Xu Ting Zhou state key laboratory of ore deposit geochemistry Chinese Academy of Sciences

The Huichizi granite complex is the largest Paleozoic 1-type intrusion located in the North Qinling orogenic belt （NQB）. In this study, we present systematic geochemical element data, zircon U-Pb ages, Ln-Hf isotopic data, and Sr-Nd isotopic data for the Huichizi granites. In terms of mineral and chemical compositions, these granites are biotite monzonitic and alkali-feldspar granites, both of which are characterized by high SiO2 and total alkali contents and low MgO, TiO2, and TFeO contents. These granites are weakly peraluminous （A/CNK values are 1-1.06 for biotite mon- zonitic granites and 1.04-1.09 for alkali-feldspar granites） and possess the geochemical characteristics of adakitic rocks, e.g., high Sr contents （319 ppm-633 ppm）, Sr/Y ratios （18.5-174）, and （La/Yb）N ratios （17.6-57） and low MgO （0.04 wt.%-0.83 wt.%）, Y （3.0 ppm-17.2 ppm）, and heavy rare-earth element （HREE） contents. This indicates that these rocks were most likely derived from the partial melting of a thickened lower crust. In situ zircon U-Pb dating of these granites yields Early Caledonian ages （437 Ma for biotite monzonitic granites and 424 Ma for alkali-feldspar granites）, indicating that the Huichizi granitic complex is the product of multi-periodic magmatism. The positive but varying zircon tHe（t） values （＋0.6 to ＋8.5） suggest that this thickened lower crust was mainly juvenile, i.e., accreted from depleted mantle during the Neo-Mesoproterozoic Period, but involved the ancient recycled crust. Biotite monzonitic granites formed during crust thickening at the extrusion stage, whereas the alkali granites formed during crust thickening at the extension stage （post extrusion）. The Huichizi granite complex witnessed the process of extrusion to extension because of the collision between the NCB and the Qinling microcontinent in the Caledonian.

关键词： U-Pb age Sr-Nd-Hf isotope Huichizi granitic complex adakitic granite North Qinling orogen.

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