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Design and fabrication of lightweight AlCrFeNiTix compositionally complex alloys with exceptional specific strength

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Rare Metals 2024年第7期43卷 3314-3328页

作者： Jun-Zhi Li Wei-Zong Bao Jie Chen Bo-Hua Yu Kun Zuo Tian Gao Ze-Yun Cai Guo-Qiang Xie School of Materials Science and Engineering Harbin Institute of Technology (Shenzhen) state key laboratory of advanced welding and Joining Harbin Institute of Technology

This study focuses on compositionally complex alloys（CCAs）,aiming to achieve a balance between high strength and low density for new energy and aerospace *** composition of AlCrFeNiTixCCAs is strategically guided by employing density functional theory and the theoretical design of thermodynamic *** CCAs,particularly AlCrFeNiTi0.25alloy,demonstrate remarkable specific yield strength（1640.8 MPa） and 22.7% maximum *** incorporation of Ti facilitates the formation of lightweight and high-strength L21phase,contributing to the overall high specific *** effects of grain boundary strengthening,solid solution strengthening,Orowan strengthening and Peierls flow stress further enhance *** exploration of micros tructural changes during fracture reveals the role of ordered phases in suppressing crack propagation and absorbing energy within disordered phases,thereby improving the toughness and fracture resistance of *** methods and discoveries establish a robust foundation for advancing the development of novel lightweight CCAs.

关键词： Lightweight Compositionally complex alloys Specific yield strength

Microstructure,mechanical and fracture properties of friction stir welded 2195 Al-Li alloy joints

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Chinese Journal of Aeronautics 2024年第1期37卷 345-361页

作者： Guangda SUN Weizhao SUN Li ZHOU Sanfeng LUO Zili ZHANG Debo LIU Huiqiang WU state key laboratory of advanced welding and Joining Harbin Institute of TechnologyHarbin 150001China Shandong Provincial key laboratory of Special welding Technology Harbin Institute of Technology(Weihai)Weihai 264209China Beijing Institute of Astronautical Systems Engineering Beijing 100076China

The 8 mm-thick 2195 Al-Li alloy joints were achieved by Friction Stir welding(FSW).The microstructural evolution,temperature-dependent mechanical properties,and fracture properties were *** T1,δ’/β’and θ’precipitates were observed in the Base Metal(BM)and the Heat Affected Zone(HAZ).Most of the precipitates,except for re-precipitated δ’/β’phases,were dissolved in the Nugget Zone(NZ).The tensile specimens that failed at cryogenic temperatures(-196℃)had the maximum Ultimate Tensile Strength(UTS),and the fracture surface showed the inter-granular fracture *** to those at room temperature(25℃),the decreasing tensile properties at high temperature(180℃)were related to microstructure and strain hardening *** NZ presented the optimal fracture toughness,and the Crack Tip Opening Displacement(CTOD)was mutually dominated by microhardness and grain *** on Fatigue Crack Growth(FCG)rates indicates that the Thermal-Mechanically Affected Zone(TMAZ)exhibited the most superior fatigue resistance performance at stress intensity range below17 MPa.m1/2due to compressive residual stress and the crack closure *** fatigue fracture surfaces reveal that the crack propagation zone was characterized by the striations and secondary ***,inter-granular fracture behavior was responsible for the fastest FCG rates in the NZ.

关键词： Aluminum alloys Friction stir welding Microstructural evolution Mechanical properties Fracture mechanism

A novel seal-flow multi-vortex friction stir lap welding of metal to polymer matrix composites

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Chinese Journal of Aeronautics 2024年第1期37卷 451-462页

作者： Shuaiqiang NIAN Mingshen LI Shude JI Wei HU Zhiqing ZHANG Zelin SUN College of Aerospace Engineering Shenyang Aerospace UniversityShenyang 110136China state key laboratory of advanced welding and Joining Harbin Institute of TechnologyHarbin 150001China

The friction stir lap welding(FSLW)of metal to polymer is a challenging work due to the unavoidable polymer *** this problem,a novel seal-flow multi-vortex friction stir lap welding(SM-FSLW)technology based on the subversively-designed multi-step pin was put *** 7075 aluminum alloy and short glass fiber-reinforced polyether ether ketone(PEEK)as research subjects,the welding temperature,material flow,formation and tensile shear strength of dissimilar materials lap joint under the SM-FSLW were studied and compared with those under traditional FSLW based on the conical *** multi-step pin rather than the conical pin effectively hindered the polymer overflowing due to the formation of vortexes by the step,thereby attaining a joint with a smooth *** with traditional FSLW,the SMFSLW obtained the higher welding temperature,the more violent material flow and the larger area with high flow velocity,thereby producing the macro-mechanical and micro-mechanical interlockings and then heightening the joint loading *** tensile shear strength of lap joint under SM-FSLW was 27.8% higher than that under traditional *** SM-FSLW technology using the multi-step pin provides an effective way on obtaining a heterogeneous lap joint of metal to polymer with the excellent formation and high strength.

关键词： Friction stir lap welding Metal to polymer Multi-step pin Material flow Tensile shear strength

Multi-scale analyses of phase transformation mechanisms and hardness in linear friction welded Ti17(a+β)/Ti17(β)dissimilar titanium alloy joint

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Chinese Journal of Aeronautics 2024年第1期37卷 312-324页

作者： Zhenguo GUO Tiejun MA Xiawei YANG Ju LI Wenya LI Achilles VAIRIS state key laboratory of Solidification Processing Shaanxi Key Laboratory of Friction Welding TechnologiesNorthwestern Polytechnical UniversityXi’an 710072China Aeronautical key laboratory for welding and Joining Technologies AVIC Manufacturing Technology InstituteBeijing 100024China Mechanical Engineering Department University of West AtticaAthens 12241Greece

The Ti17(a+β)-Ti17(β)dual alloy-dual property blisk produced using Linear Friction welding(LFW)is considered as high-performance component in advanced ***,up to now,microstructure evolution and relationship between microstructure and micro mechanical properties of LFWed Ti17(a+β)/Ti17(β)dissimilar joint have not been thoroughly *** this work,complex analyses of the phase transformation mechanisms of the joint are conducted,and phase transformations in individual zones are correlated to their microhardness and *** reveal that a dissolution occurs under high temperatures encountered during LFW,which reduces microhardness of the joint to that of Ti17(a+β)and Ti17(β).In ThermoMechanically Affected Zone of Ti17(a+β)(TMAZ-(a+β))side joint,a large number of nanocrystalline a phases form with different *** microstructure strengthens significantly by fine grains which balances partial softening effect of a dissolution,and increases nanohardness of a phase and microhardness of TMAZ-(a+β).Superlattice metastableβphase precipitates from metastableβin Weld Zone(WZ)during quick cooling following welding,because of short-range diffusion migration of solute atoms,especiallyβstabilizing elements Mo and *** precipitation of the superlattice metastableβphase results in precipitation strengthening,which in turn increases nanohardness of metastableβand microhardness in WZ.

关键词： Linear friction welding Ti17 titanium alloy Phase transformation Microhardness Nanohardness

In-situ isothermal aging TEM analysis of a micro Cu/ENIG/Sn solder joint for flexible interconnects

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Journal of Materials Science & Technology 2024年第2期169卷 42-52页

作者： Jinhong Liu Jianhao Xu Kyung-Wook Paik Peng He Shuye Zhang state key laboratory of advanced welding and Joining Harbin Institute of TechnologyHarbin150001China Department of materials science and engineering KAIST291 Daehak-roYuseong-guDaejeon305-338Republic of Korea

Sn/ENIG has recently been used in flexible interconnects to form a more stable micron-sized metallurgical joint,due to high power capability which causes solder joints to heat up to 200℃.However,Cu_(6)Sn_(5)which is critical for a microelectronic interconnection,will go through a phase transition at temperatures between 186 and 189℃.This research conducted an in-situ TEM study of a micro Cu/ENIG/Sn solder joint under isothermal aging test and proposed a model to illustrate the mechanism of the microstructural *** results showed that part of the Sn solder reacted with Cu diffused from the electrode to formη´-Cu_(6)Sn_(5)during the ultrasonic bonding process,while the rest of Sn was left and enriched in a region in the solder *** the enriched Sn quickly diffused to both sides when the temperature reached 100℃,reacting with the ENIG coating and Cu to form(Ni_(x)Cu_(1-x))_(3)Sn_(4),AuSn_(4),and Cu_(6)Sn_(5)*** entering the heat preservation process,the diffusion of Cu from the electrode to the joint became more intense,resulting in the formation of Cu_(3)*** scallop-type Cu_(6)Sn_(5)and the seahorse-type Cu_(3)Sn constituted a typical two-layered structure in the solder *** importantly,the transition betweenηandη’was captured near the phase transition temperature for Cu_(6)Sn_(5)during both the heating and cooling process,which was accompanied by a volume shifting,and the transition process was further *** research is expected to serve as a reference for the service of micro Cu/ENIG/Sn solder joints in the electronic industry.

关键词： In-situ TEM observation Isothermal aging Micro Cu/ENIG/Sn solder joint Cu_(6)Sn_(5)phase transition

A review of linear friction welding of Ni -based superalloys

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International Journal of Minerals,Metallurgy and Materials 2024年第6期31卷 1382-1391页

作者： Xiawei Yang Tingxi Meng Qiang Chu Yu Su Zhenguo Guo Rui Xu Wenlong Fan Tiejun Ma Wenya Li state key laboratory of Solidification Processing Shaanxi Key Laboratory of Friction Welding TechnologiesNorthwestern Polytechnical UniversityXi’an 710072China Xi’an Aerospace Engine Co.Ltd. Xi’an 710100China

Ni-based superalloys are one of the most important materials employed in high-temperature applications within the aerospace and nuclear energy industries and in gas turbines due to their excellent corrosion,radiation,fatigue resistance,and high-temperature *** friction welding(LFW)is a new joining technology with near-net-forming characteristics that can be used for the manu-facture and repair of a wide range of aerospace *** paper reviews published works on LFW of Ni-based superalloys with the aim of understanding the characteristics of frictional heat generation and extrusion deformation,microstructures,mechanical proper-ties,flash morphology,residual stresses,creep,and fatigue of Ni-based superalloy weldments produced with LFW to enable future optim-um utilization of the LFW process.

关键词： Ni-based superalloys linear friction welding microstructures mechanical properties flash morphology

Hot deformation behavior and microstructure evolution of GH3536-TiB_(2) composites fabricated by powder metallurgy

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Science China(Technological Sciences) 2024年第7期67卷 2107-2124页

作者： ZHOU ShiPeng WANG Shuai HUANG LuJun ZHANG Rui CHEN Xin MENG FanChao CHEN Run SUN FengBo WANG CunYu GENG Lin School of Materials Science and Engineering Harbin Institute of TechnologyHarbin 150001China Waikato Centre for advanced Materials and Manufacturing School of EngineeringUniversity of WaikatoHamilton 3240New Zealand state key laboratory of advanced welding and Joining Harbin Institute of TechnologyHarbin 150001China

The hot deformation behavior and microstructure evolution of GH3536-TiB2composites fabricated by powder metallurgy(PM)were examined in the temperature range of 950–1150℃ and strain rate range of 0.001–1 s^(-1). The hot compression stress-strain curves and the constitutive equation were obtained. In addition, the hot processing map was drawn, which indicated that the appropriate hot working window was 950–1050℃/0.001–0.1 s^(-1)and 1050–1100℃/0.001–0.01 s^(-1). The microstructure analysis showed that the splitting and spheroidization of M3B2led to a decrease in size and volume fraction at 950–1100℃. At 1150℃,the eutectic microstructure of M_(3)B_(2)+ γ was formed due to the dissolution of M_(3)B_(2), which caused macroscopic cracking of the deformed sample. Additionally, the deformation temperature and the strain rate had little effect on the size and volume fraction of M_(3)B_(2). Besides, discontinuous dynamic recrystallization(DDRX) and continuous dynamic recrystallization(CDRX) were found in the deformed microstructure, while the former was dominant. Within the test range of this work, the dynamic recrystallization(DRX) fraction of the deformed composites was high due to the bulging nucleation of numerous interfaces. The DRX grain size increased with increasing deformation temperature or decreasing strain rate. Texture analysis showed that the deformation texture of //compression direction RD existed in the matrix when the deformation temperature was below 1100℃, and the texture type became //RD at 1100℃. Additionally, it was also found that the //RD texture was formed in M3B2under the strain rates of 0.1 and 0.01 s^(-1).

关键词： GH3536 alloy matrix composites powder metallurgy hot deformation behavior microstructure evolution

Fatigue Crack Initiation and Propagation Dominated by Crystallographic Factors in TiB/near α-Ti Composite

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Acta Metallurgica Sinica(English Letters) 2024年第5期37卷 763-776页

作者： Fanchao Meng Rui Zhang Shuai Wang Fengbo Sun Run Chen Lujun Huang Lin Geng School of Materials Science and Engineering Harbin Institute of TechnologyHarbin 150001China Waikato Centre for advanced Materials and Manufacturing School of EngineeringUniversity of WaikatoHamilton 3240New Zealand state key laboratory of advanced welding and Joining Harbin Institute of TechnologyHarbin 150001China

Discontinuously reinforced titanium matrix composites(DRTMCs)with a network structure have been extensively researched due to their superior combination of strength and ***,their fatigue performance has remained *** order to elucidate the fatigue behavior of DRTMCs,a tension-tension fatigue test was performed on a TiB/nearα-Ti composite with network *** results showed that the variability of fatigue lifetime increased as the stress level *** analysis indicated that fatigue crack initiation was associated with facet formation,while the subsequent propagation was hindered by the network structure comprising TiB whiskers and *** characterization further revealed that facets formed due to a combination of shear and normal *** reduction in fatigue lifetime was attributed to an increase in the effective slip length,which was influenced by the orientation of grains near the crack-initiation sites toward basal slip in the life-limiting *** in situ observation suggested that the crack initiation was facilitated by both basal and prismatic slip ofα-Ti as well as fracture of *** propagation was found to be associated with basal and prismatic slip systems with high Schmid factors,regardless of whether the crack was intergranular or intragranular.

关键词： Titanium matrix composite TiBw Fatigue lifetime variability Crack initiation Crack propagation

Fast strength-ductility synergistically adjusting of cold spray additive manufactured Cu deposits via electric pulse processing

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Chinese Journal of Aeronautics 2024年第5期37卷 558-569页

作者： Dong WU Yaxin XU Wenya LI Xiawei YANG Yu SU state key laboratory of Solidification Processing School of Materials Science and EngineeringNorthwestern Polytechnical UniversityXi’an 710072China Shaanxi key laboratory of Friction welding Technologies School of Materials Science and EngineeringNorthwestern Polytechnical UniversityXi’an 710072China

Electric Pulse Processing(EPP)treatment was innovatively introduced to optimize the strength and ductility of the CSAMed Cu *** results show that EPP is an efficient and fast post-treatment to improve the strength and ductility(within tens of seconds).The larger the pulse current and number of pulses,the better the mechanical ***,this research found that when the heat input determined by pulse current and number of pulses exceeds a certain threshold(pulse current intensity is 2000 A,number of pulses is 10),increasing the number of repeat time could also effectively improve the mechanical properties.A tensile strength of 210 MPa and a ductility of 14.0%could be obtained with reasonable EPP parameters(pulse current intensity is 2000 A,number of pulses is 10,and repeat number is 2),which is similar to those of conventional annealing(e.g.,tensile strength is 272 MPa,elongation is 28.3%).The microstructure evolution analysis shows that EPP can effectively improve the bonding quality between the deposited particles by recrystallization,promote grain growth and the formation of twins,which is the main reason for the improvement of mechanical properties.

关键词： Cold spray additive manufacturing Copper deposit Mechanical property Electric pulse processing Post treatment