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Progress in preparation of AlN-reinforced magnesium matrix composites:A review

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China Foundry 2024年第1期21卷 1-10页

作者： Lu Chen Shu-lin Lü Di-jia Zhao Wei Guo Jian-yu Li Shu-sen Wu state key lab of materials processing and Die&mould technology School of Materials Science and EngineeringHuazhong University of Science and TechnologyWuhan 430074China

As a ceramic material,AlN has very good thermophysical and mechanical *** addition,AlN is an effective refining agent for Mg alloys because it has a lattice constant similar to that of ***,AlN is an ideal reinforcement for magnesium matrix composites(MMCs),and is attracting increasing *** review addresses the development of preparation technologies for AlN-reinforced Mg matrix *** mainstream preparation techniques include stir casting,melt infiltration,powder metallurgy,and in-situ *** addition,the advantages and disadvantages of these techniques are analyzed in depth,and it is pointed out that the next direction for the preparation of high-performance AlN-reinforced MMCs is less aluminization and multiple technologies integration.

关键词： AlN MMCs preparation thermophysical property mechanical property

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Chinese Chemical Letters 2024年第8期35卷 25-35页

作者： Yatian Deng Dao Wang Jinglan Cheng Yunkun Zhao Zongbao Li Chunyan Zang Jian Li Lichao Jia School of materials Science and Engineering State Key Lab of Material Processing and Die&Mould TechnologyHuazhong University of Science and TechnologyWuhan 430074China College of Science Qiongtai Normal UniversityHaikou 571127China Kunming Sino-Platinum Metals Catalyst Co. Ltd.Kunming 650106China state key laboratory of Advanced Electromagnetic technology Huazhong University of Science and TechnologyWuhan 430074China

Catalyst with high performance has drawn increasing attention recently due to its significant advantages in chemical reactions such as speeding up the reaction,lowering the reaction temperature or pressure,and proceeding without itself being *** the superior catalytic performance of precious metal catalysts,transition metal oxides offer a promising route for substitution of precious metals in catalysis arising from their low cost,intrinsic activity and sufficient ***-type oxide SmMn_(2)O_(5) exhibits a unique crystal structure containing double crystalline fields,and nowadays is used widely as the catalyst in different chemical reactions,including the reactions of vehicle emissions reduction and oxygen evolution reaction,gas sensors,and metal-air batteries,promoting attention in catalytic perfor-mance *** our knowledge,there is no review article covering the comprehensive informa-tion of SmMn2 O 5 and its *** we review the recent progress in understanding of the crys-tal structure of SmMn_(2)O_(5) and its basic physical *** then summarize the catalytic sources of SmMn_(2)O_(5) and reaction mechanisms,while the strategies to improve catalytic performance of SmMn_(2)O_(5) are further ***,we provide a perspective on how to make further progress in catalytic applications.

关键词： Catalyst SmMn_(2)O_(5) Mullite-type oxide Catalytic oxidation Oxygen reduction reaction Oxygen evolution reaction Reaction mechanisms

Targeted regeneration and upcycling of spent graphite by defect‐driven tin nucleation

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Carbon Energy 2024年第4期6卷 91-103页

作者： Zhiheng Cheng Zhiling Luo Hao Zhang Wuxing Zhang Wang Gao Yang Zhang Long Qie Yonggang Yao Yunhui Huang Kun Kelvin Fu state key laboratory of materials processing and Die&mould technology School of Materials Science and EngineeringHuazhong University of Science and TechnologyWuhanChina key laboratory of Automobile materials(Jilin University) Ministry of EducationDepartment of Materials Science and EngineeringJilin UniversityChangchunChina Electronic materials Research laboratory(key lab of Education Ministry) School of Electronic and Information Engineeringand Instrumental Analysis CenterXi'an Jiaotong UniversityXi'anChina Department of Mechanical Engineering University of DelawareNewarkUSA

The recycling of spent batteries has become increasingly important owing to their wide applications,abundant raw material supply,and sustainable *** with the degraded cathode,spent anode graphite often has a relatively intact structure with few defects after long ***,most spent graphite is simply burned or discarded due to its limited value and inferior performance on using conventional recycling methods that are complex,have low efficiency,and fail in performance ***,we propose a fast,efficient,and“intelligent”strategy to regenerate and upcycle spent graphite based on defect‐driven targeted *** Sn as a nanoscale healant,we used rapid heating(~50 ms)to enable dynamic Sn droplets to automatically nucleate around the surface defects on the graphite upon cooling owing to strong binding to the defects(~5.84 eV/atom),thus simultaneously achieving Sn dispersion and graphite *** a result,the regenerated graphite showed enhanced capacity and cycle stability(458.9 mAh g^(−1) at 0.2 A g^(−1) after 100 cycles),superior to those of commercial *** from the self‐adaption of Sn dispersion,spent graphite with different degrees of defects can be regenerated to similar structures and *** analysis indicates that targeted regeneration and upcycling have significantly lower energy consumption(~99%reduction)and near‐zero CO_(2) emission,and yield much higher profit than hydrometallurgy,which opens a new avenue for direct upcycling of spend graphite in an efficient,green,and profitable manner for sustainable battery manufacture.

关键词： battery recycling spent graphite targeted regeneration upcycling graphite

Recent development of ductile cast iron production technology in China

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China Foundry 2008年第2期5卷 82-91页

作者： Cai Qizhou Wei Bokang state key lab of material processing and dies ＆ mould technology Huazhong University of Science and Technology Wuhan 430074 China

Recent progress in the production and technology of ductile cast iron castings in China is reviewed. The manufacture and process control of as-cast ductile iron are discussed. The microstructure, properties and application of partial austenitization normalizing ductile iron and austempered ductile iron (ADI) are briefly depicted. The new development of ductile iron production techniques, such as cored-wire injection (wire-feeding nodularization) process, tundish cover ladle nodularizing process, horizontal continuous casting, and EPC process (lost foam) for ductile iron castings, etc., are summarized.

关键词： ductile cast iron production technology recent development

Progress in MXene-based catalysts for oxygen evolution reaction

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Electron 2024年第1期2卷 48-67页

作者： Jieli Chen Xiaohong Gao Jing Li Zhenye Kang Juan Bai Tianjiao Wang Yuliang Yuan Chenghang You Yu Chen Bao Yu Xia Xinlong Tian School of Marine Science and Engineering Hainan Provincial Key Lab of Fine ChemistrySchool of Chemistry and Chemical EngineeringHainan UniversityHaikouChina School of Chemistry and Physics Queensland University of TechnologyBrisbaneQueenslandAustralia key laboratory of Macromolecular Science of Shaanxi Province School of Materials Science and EngineeringShaanxi Normal UniversityXi'anChina School of Chemistry and Chemical Engineering State Key Laboratory of Materials Processing and Die&Mould TechnologyKey Laboratory of Material Chemistry for Energy Conversion and Storage(Ministry of Education)Hubei Key Laboratory of Material Chemistry and Service FailureWuhan National Laboratory for OptoelectronicsHuazhong University of Science and Technology(HUST)WuhanChina

Electrochemical water splitting for hydrogen generation is considered one of the most promising strategies for reducing the use of fossil fuels and storing renewable electricity in hydrogen ***,the anodic oxygen evolution process remains a bottleneck due to the remarkably high overpotential of about 300 mV to achieve a current density of 10 mA cm^(−2).The key to solving this dilemma is the development of highly efficient catalysts with minimized overpotential,long-term stability,and low *** a new 2D material,MXene has emerged as an intriguing material for future energy conversion technology due to its benefits,including superior conductivity,excellent hydrophilic properties,high surface area,versatile chemical composition,and ease of processing,which make it a potential constituent of the oxygen evolution catalyst *** review aims to summarize and discuss the recent development of oxygen evolution catalysts using MXene as a component,emphasizing the synthesis and synergistic effect of MXene-based composite *** on the discussions summarized in this review,we also provide future research directions regarding electronic interaction,stability,and structural evolution of MXene-based oxygen evolution *** believe that a broader and deeper research in this area could accelerate the discovery of efficient catalysts for electrochemical oxygen evolution.

关键词： MXene-based catalysts oxygen evolution reaction water splitting

Preparation of Electrically Conductive Filler for Anisotropic Conductive Adhesive

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上海交通大学学报 2007年第S2期41卷 127-130,138页

作者：华丽安兵吴懿平吴丰顺王佳何敬强 state key lab.of material processing and Die & mould technology Huazhong Univ.of Science & Technology

The preparation process of electrically conductive filler for anisotropic conductive adhesive was performed and *** spherical filler contains tri-layer structures: resin core,Ni-P intermediate coating layer,Au outer coating *** 4 μm resin spherical cores were synthesized by monodispersion polymerization *** they were contributed to electrical conductivity by electrolessly plating Ni-P layer and gold *** particles have good corrosion resistance,high stability,and enough mechanical *** mixed with thermosetting epoxy resin to produce anisotropic conductive adhesive(ACA),it can realize a good conductive bonding between bumps on dies and pads on *** environmentally friendly conductive material offers numerous advantages over conventional solder technology and is an ideal substitute for the lead-contained solder in electronics packaging.

关键词： anisotropic conductive adhesive(ACA) monodispersion polymerization microsphere electroless plating

Structure and Properties of TiB_2 Thin Films Deposited at Low Temperatures Using RF Magnetron Sputtering

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Journal of Wuhan University of technology(materials Science) 2008年第5期23卷 666-669页

作者：戴伟张同俊 state key lab of material processing and Die & mould technology Huazhong University of Science and Technology

The TiB2 thin films were deposited on steel substrates using RF magnetron sputtering technique with the low normalized substrate temperature （0.1〈Ts/Tm〈0.2）. Microstructure of these films was obtained by field emission scanning electron microscope （FESEM） and the grazing incidence X-ray diffraction （GIXRD） characterization, while the composition of films was obtained using Auger emission spectroscopy （AES） analysis. It was found that the TiB2 thin films were overstoichiometric with the B/Ti ratio at 2.33 and the diffusion of Ti and B atoms on the substrate surface was greatly improved at 350 ℃. Moreover, a new dense structure, named ＂equiaxed＂ grain structure was observed by FESEM at this substrate temperature, Combined with FESEM and AES analysis, it was suggested that the ＂equiaxed＂ grain structure was located in Zone 2 at the normalized substrate temperature as low as 0.18.

关键词： TiB2 thin films structure zones 1,2,T equiaxed structure superhard coating auger electron spectroscopy

Investigation into the tribological behaviors of press hardening steels on the tailored conditions

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Science China(Technological Sciences) 2015年第1期58卷 97-106页

作者： WANG ZiJian LUO XiaoYu HE WenTing ZHANG YiSheng state key laboratory of material processing and Die and mould technology College of Materials Science and Engineering Huazhong University of Science & Technology

There has been a growing demand for safety parts with tailored properties in automobile ***,the understanding of tribological behavior of press hardening steels(PHS)on the tailored conditions is highly *** present work aims at creating new knowledge about the tribological characteristics of PHS on the tailored conditions and bridging this existing *** paper proposes an improved hot drawing tribo-simulator to simulate the realistic experimental conditions *** were carried out on the condition of different initial heating temperatures,tool temperatures,austenitizing temperatures,cooling rates and *** presented results show that the whole frictional process is divided into three stages for both coated and uncoated *** frictional factor changes a lot and the peak value of frictional factor occurs for serious adhesive *** frictional factor rises as the tool temperature and austenitizing temperature *** surface morphology of tools indicates that the coating adhering to tool gets thicker as the tool temperature *** the increase of cooling rate,the frictional factor declines firstly and then rises to some *** dies with different temperatures are used to form specimens with different microstructures,which also affects the frictional factor and wear.

关键词： frictional factor press hardening steel(PHS) adhesive wear tribological behavior

Preparation of narrow band gap V_2O_5/TiO_2 composite films by micro-arc oxidation

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International Journal of Minerals,Metallurgy and materials 2012年第11期19卷 1045-1051页

作者： Qiang Luo Xin-wei Li Qi-zhou Cai Qing-song Yan Zhen-hua Pan state key lab of material processing and dies & mould technology Huazhong University of Science and Technology Wuhan 430074 China National Defense key Disciplines laboratory of Light Alloy processing Science and technology Nanchang Hangkong University Nanchang 330063 China

V2Os/TiO2 composite films were prepared on pure titanium substmtes via micro-arc oxidation （MAO） in electrolytes consisting of NaVO3. Their morphology and dements were characterized by scanning electron microscopy （SEM） and energy-dispersive X-ray （EDX） analysis. Phase composition and valence states of species in the films were characterized by X-ray diffraction （XRD） and X-ray photoelec- tron spectroscopy （XPS）. Ultraviolet-visible diffuse reflectance spectra （UV-Vis DRS） were also employed to evaluate the photophysical property of the films. The VEOs/TiO2 composite films show a sheet-like morphology. Not only V205 phase appears in the films when the NaVO3 concentration of the electrolyte is higher than 6,10 g/L and is loaded at the surface of anatase, but also V4＋ is incorporated into the crystal lattice of anatase. In comparison with pure TiO2 films the V2Os/TiO2 composite films exhibit significantly narrow band gap energy. The film prepared in an electrolyte consisting of NaVO3 with a concentration of 8.54 g/L exhibits the narrowest band gap energy, which is approximately 1.89 eV. The V2Os/TiO2 composite films also have the significantly enhanced visible light photocatalytic activity. The film prepared in an electrolyte consisting of NaVO3 with a concentration of 8.54 g/L exhibits the best photocatalytic activity and about 93% of rhodamine is degraded after 14 h visible light radiation.

关键词： composite films titanium dioxide vanadium pentoxide micro-arc oxidation sodium metavanadate rhodamine photocatalysis