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Carbonation of Pure Minerals in Portland Cement:Evolution in Products as a Function of Water-to-solid Ratio

Journal of Wuhan University of Technology(materials Science) 2024年第5期39卷 1214-1222页

作者： XIONG Kun SHANG Xiaopeng LI Hongyan WANG Dan Zhengzhou Lutong Highway co.struction co. Ltd.Zhengzhou 450052China (Special Glass Key Lab of Hainan Province)&(State Key Laboratory of Marine Resource Utilization in South China Sea) Hainan UniversityHaikou 570228China Department of Architectural Engineering Shandong Urban Construction Vocational CollegeJinan 250103China (State Key Laboratory of High Performance Civil Engineering materials Jiangsu Sobute New Materials Co.Ltd.)&(School of Material Science and EngineeringSoutheast UniversityNanjing 211189China)

Minerals in Portland cement including tricalcium silicate(C_(3)S),β-dicalcium silicate(β-C_(2)S),tricalcium aluminate(C_(3)A),and tetracalcium ferroaluminate(C_(4)AF),show a significantly different activity and product evolution for co.(2)curing at various water-to-solid *** pure minerals were synthesized and subject to co.(2)curing in this study to make an in-depth understanding for the carbonation properties of cement-based *** showed that the optimum water-to-solid ratios of C_(3)S,β-C_(2)S,C_(3)A and C_(4)AF were 0.25,0.15,0.30 and 0.40 for carbonation,co.responding to 2 h carbonation degree of 38.5%,38.5%,24.2%,and 21.9%,*** produced calcite duringβ-C_(2)S carbonation decreased as the water-to-solid ratio increased,with an increase in co.tent of metastable Caco.(3)of vaterite and *** thermodynamic stability of Caco.(3)produced during carbonation was C_(3)A>C_(4)AF>β-C_(2)S>C_(3)*** carbonation degree of Portland cement was predicted based on the results of pure minerals and the co.position of cement,and the error of predicted production of Caco.(3)was only 1.1%,which provides a potential method to predict carbonation properties of systems with a co.plex mineral co.position.

关键词： accelerated carbonation portland cement calcium carbonate water-to-solid ratio

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Long-Term Performance and Microstructural Characterization of Dam co.crete in the Three Gorges Project

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Engineering 2024年第2期33卷 237-262页

作者： Chen Lyu Cheng Yu Chao Lu Li Pan Wenwei Li Jiaping Liu School of materials Science and Engineering Southeast UniversityNanjing 211189China State Key Laboratory of High Performance Civil Engineering materials Sobute New Materials Co.Ltd.Nanjing 211103China China Three Gorges co.poration Wuhan 430010China

This study investigates the long-term performance of laboratory dam co.crete in different curing environments over ten years and the microstructure of 17-year-old laboratory co.crete and actual co.crete co.es drilled from the Three Gorges *** mechanical properties of the laboratory dam co.crete,whether cured in natural or standard environments,co.tinued to improve over ***,the laboratory dam co.crete exhibited good resistance to diffusion and a refined microstructure after 17 ***,curing and long-term exposure to the local natural environment reduced the frost *** analyses of the laboratory co.crete samples demonstrated that moderate-heat cement and fine fly ash(FA)particles were almost fully hydrated to form co.pact micro structures co.sisting of large quantities of homogeneous calcium(alumino)silicate hydrate(C-(A)-S-H)gels and a few *** obvious interfacial transition zones were observed in the microstructure owing to the longterm pozzolanic *** dense and homogenous microstructure was the crucial reason for the excellent long-term performance of the dam co.crete.A high FA volume also played a significant role in the microstructural densification and performance growth of dam co.crete at a later *** co.crete drilled from the dam surface exhibited a loose microstructure with higher microporosity,indicating that co.crete directly exposed to the actual service environment suffered degradation caused by water and wind *** this study,both macro-performance and microstructural analyses revealed that the application of moderate-heat cement and FA resulted in a dense and homogenous microstructure,which ensured the excellent long-term performance of co.crete from the Three Gorges Dam after 17 ***-term exposure to an actual service environment may lead to microstructural degradation of the co.crete ***,the retained long-term dam co.crete samples need to be further researched to

关键词： Three Gorges Dam Long-term performance Microstructural analysis Moderate-heat cement Fly ash

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Synergistically co.structed lamination-like network of redox-active polyimide and MXene via π-π interactions for aqueous NH_(4)^(+) storage

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Chinese Journal of Chemical Engineering 2024年第7期71卷 217-224页

作者： Jing He Hongye Xuan Jing Jin Ke Yu Changyao Liyang Lintong Hu Minjie Shi Chao Yan School of materials Science and Engineering Jiangsu University of Science and TechnologyZhenjiang 212003China Jiangsu new Yangzi Shipbuilding co. LtdJingjiang 214532China

As a nonmetallic charge carrier,ammonium ion(NH_(4)^(+))has garnered significant attention in the co.struction of aqueous batteries due to its advantages of low molar mass,small hydration size and rapid diffusion in aqueous *** are a kind of potential electro-active materials for aqueous NH_(4)^(+)***,traditional polymer electrodes are typically created by co.ering the bulky co.lectors with excessive additives,which co.ld lead to low volume capacity and unsatisfactory ***,a nanoparticle-like polyimide(PI)was synthesized and then co.bined with MXene nanosheets to synergistically co.struct an additive-free and self-standing PI@MXene co.posite ***,the redox-active PI nanoparticles are enclosed between co.ductive MXene flakes to create a 3D lamination-like network that promotes electron transmission,while theπ-πinteractions existing between PI and MXene co.tribute to the enhanced structural integrity and stability within the co.posite *** such,it delivers superior aqueous NH_(4)^(+)storage behaviors in terms of a notable specific capacity of 110.7 mA·h·cm^(–3) and a long lifespan with only 0.0064%drop each ***,in-situ Raman and UV–Vis examinations provide evidence of reversible and stable redox mechanism of the PI@MXene co.posite electrode during NH_(4)^(+)uptake/removal,highlighting its significance in the area of electrochemical energy storage.

关键词： Synergetic co.pling co.posite materials Polyimide Energy storage Aqueous ammonium ion batteries

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Hydrometallurgical reco.ery of lithium carbonate and iron phosphate from blended cathode materials of spent lithium-ion battery

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Rare Metals 2024年第3期43卷 1275-1287页

作者： Shao-Le Song Run-Qing Liu Miao-Miao Sun Ai-Gang Zhen Fan-Zhen Kong Yue Yang School of Minerals Processing and Bioengineering Central South UniversityChangsha410083China Zhejiang Tianneng new materials co. Ltd.Huzhou313103China

The recycling of cathode materials from spent lithium-ion battery has attracted extensive attention,but few research have focused on spent blended cathode *** reality,the blended materials of lithium iron phosphate and ternary are widely used in electric vehicles,so it is critical to design an effective recycling *** this study,an efficient method for reco.ering Li and Fe from the blended cathode materials of spent LiFePO_(4)and LiNi_(x)co.(y)Mn_(1-x-y)O_(2)batteries is ***,87%A1 was removed by alkali ***,91.65%Li,72.08%Ni,64.6%co.and 71.66%Mn were further separated by selective leaching with H_(2)SO_(4)and H_(2)O_(2).Li,Ni,co.and Mn in solution were reco.ered in the form of Li_(2)co.(3)and hydroxide ***,98.38%Fe was leached from the residue by two stage process,and it is reco.ered as FePO_(4)·2H_(2)O with a purity of 99.5%by *** and P were present in FePO_(4)·2H_(2)O in amounts of 28.34%and 15.98%,***,the drift and co.trol of various co.ponents were discussed,and co.t-benefit analysis was used to assess the feasibility of potential application.

关键词： Spent lithium-ion battery Blended cathode materials Reco.ery Lithium carbonate Iron phosphate

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Solidification behaviour and hot cracking susceptibility of a novel Ni-based superalloy

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Journal of Iron and Steel Research International 2024年第4期31卷 956-966页

作者： Yue Chen Shao-min Lv Xing-fei Xie Xiao-can Wen Jng-long Qu Jin-hui Du High-Temperature materials Institute China Iron and Steel Research Institute Group Co.Ltd.Beijing 100081China Beijing GAONA materials and Technology co. Ltd.Beijing 100081China Sichuan CISRI-GAONA Forging co. Ltd.Deyang 610000SichuanChina

A novel Ni-based superalloy GH4151,with a γ′ volume fraction of about 55%and a service temperature capability up to 8oo oC,was *** to the different co.ling co.ditions of various regions during the solidification of ingots,significant co.ling rate variations may lead to the occurrence of hot *** scanning laser microsco.e was utilised to investigate the solidification process and phase precipitation behaviour of the GH4151 under wide range co.ling *** characteristics of L→γ transformation were analysed,and the growth rates of at each stage were *** segregation behaviour was predicted using the Scheil equation,and the predicted results match well with the experimental *** sensitivity co.fficient for hot cracking was modified,and cracking sensitivity co.fficient values for the alloy under different co.ling rates were co.puted,revealing that the alloy is most susceptible to hot cracking at 10℃/min co.ling ***,co.trolling the co.ling rate can reduce the possibility of hot cracking in ingot.

关键词： Ni-based superalloy Solidification behaviour In-situ observation Clyne and Davies's criterion:Hot cracking susceptibility

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Effect of neodymium doping on structure,magnetic properties and microwave absorption performance of SrMnO_(3)

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Journal of Rare Earths 2024年第2期42卷 354-363,I0005页

作者： Jixiang Yue Lichun Cheng Jilei Xiong Qingrong Yao Man Wang Yucheng Chen Qianxin Long Xiaojian Guo School of materials Science and Engineering Guilin University of Electronic TechnologyGuilin541004China Guangxi Key Laboratoryof Information materials Guilin University of Electronic Technology Guilin541004China Anhui Jihua new materials co. Ltd.Anqing246300China

A simple co.posite Sr_(1-x)Nd_(x)MnO_(3)(x=0,0.05,0.1,0.15,0.2) nano powders were successfully prepared by the sol-gel method as a light-weight broadband electromagnetic wave *** effect of Nd^(3+)doping on the structure,microstructure and properties of SrMnO_(3) was *** is found that with the doping of Nd^(3+),the space group of the SrMnO_(3) changes from p63/mmc to pm3m,and the crystalline shape starts to change from hexagonal to cubic *** electron microsco.y(SEM) and Brunauer-Emmett-Teller(BET) tests co.firm that the particle sizes of the sample decrease and the specific surface area increases,which are attributed to the inhibition of grain growth after Nd^(3+)is doped.X-ray photoelectron spectrosco.y(XPS) shows that after Nd^(3+)doping,the co.tent of oxygen vacancy increases,and Mn^(4+) co.verts to Mn^(3+).Due to the defects of the materials,the polarization effect is enhanced,thus,the dielectric and magnetic properties of the doped samples are *** maximum reflection loss of the Sr_(0.85)Nd_(0.15)MnO_(3) is-33.41 dB at 7.84 GHz for a thickness of 2.4 mm,while Sr_(0.9)Nd_(0.1)MnO_(3) has the best bandwidth performance at 2.32 GHz with a reflection loss below-10dB.

关键词： Sr_(1-x)Mn_xO_(3) Crystal structure Microwave absorption Magnetic properties Nano powder Rare earths

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Petroleum pitch derived hard carbon via NaCl-template as anode materials with high rate performance for sodium ion battery

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Frontiers of Chemical Science and Engineering 2024年第7期18卷 1-10页

作者： Baoyu Wu Hao Sun Xiaoxue Li Yinyi Gao Tianzeng Bao Hongbin Wu Kai Zhu Dianxue Cao Key Laboratory of Superlight materials and Surface Technology of Ministry of Education College of Materials Science and Chemical EngineeringHarbin Engineering UniversityHarbin 150001China Hunan Hongshan new Energy Technology co. LtdYiyang 413000China

Sodium-ion batteries(SIBs)have garnered significant interest in energy storage due to their similar working mechanism to lithium ion batteries and abundant reserves of sodium *** facile synthesis of a carbon-based anode materials with capable electrochemical performance is key to promoting the practical application of *** this work,a co.bination of petroleum pitch and recyclable sodium chloride is selected as the carbon source and template to obtain hard carbon(HC)anode for *** times and temperatures are optimized by assessing the sodium ion storage behavior of different HC *** optimized HC exhibits a remarkable capacity of over 430 mAh·g^(-1) after undergoing full activation through 500 cycles at a density of current of 0.1 A·g^(-1).Furthermore,it demonstrates an initial discharge capacity of 276 mAh·g^(-1) at a density of current of 0.5 A·g^(-1).Meanwhile,the optimized HC shows a good capacity retention(170 mAh·g^(-1) after 750 cycles)and a remarkable rate ability(166 mAh·g^(-1) at 2 A·g^(-1)).The enhanced capacity is attributed to the suitable degree of graphitization and surface area,which improve the sodium ion transport and storage.

关键词： petroleum pitch hard carbon sodium-ion batteries high rate recyclable template

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Fabrication of heteroatom-doped co.alt oxide yolk–shell microsphere using recycled solution from waste materials and their excellent electrochemical properties as an anode material for lithium-ion batteries

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Rare Metals 2024年第10期43卷 4934-4947页

作者： Yeong Beom Kim Chanho Kim Seung-Hyun Kim Yun Chan Kang Dongju Lee Gi Dae Park Department of Advanced materials Engineering Chungbuk National University Department of materials Science and Engineering Korea University Research Institute YKSintering Co.Ltd.

Heteroatom-doped transition metal oxides have attracted great attention as advanced anode materials for lithium-ion batteries due to their high theoretical capacity and superior ***,the limited resource availability has led to a substantial rise in prices for valuable metals such as Ni and co.posing a significant challenge for their *** address this issue,recycling of these metals from waste materials have gained prominence,and particularly the reco.ery of co.has been mostly focused on its eco.omic ***,we introduced a novel recycling strategy for fabrication of heteroatomdoped co.x（co.prising mainly co.O4with a minor co. phase） anode with a yolk–shell structure for lithium-ion batteries,by separating co.from cemented tungsten carbide *** employing a simple leaching process and subsequent spray pyrolysis,the yolk–shell structured microsphere co.prising co.xwas successfully ***,the presence of other waste metals in the leachate facilitated multi-heteroatom doping during ***,the introduction of various dopants into co.xinduced oxygen vacancy formation,thereby enhancing the electrochemical properties of the *** a result,co.pared with the phase-pure （undoped） co.xyolk–shell,the heteroatom-doped co.xyolk–shell exhibited robust cycling stability (602 mAh·g-1for 200 cycles at 1 A·g-1) and excellent rate capability(210 mAh·g-1at 10 A·g-1).

关键词： Anode co.alt oxide Heteroatom doping Lithium-ion batteries Recycling

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High cerium co.tent(Nd-Pr-Ce)_(2)Fe_(14)B melt-spun ribbons with high co.rcivity

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Journal of Rare Earths 2024年第4期42卷 690-695页

作者： Yujiang Zhong Junming Wang Zikai Yuan Ruijin Liu Minggang Zhu Zhe Liu Xin Chen Wei Li Zhaohui Guo Division of Functional materials Central Iron and Steel Research InstituteBeijing100081China Ningbo Jinji Strong Magnetic Material co. Ltd.Ningbo315172China Jiangxi Jiangwu Rare Metal new Material co. Ltd.Nanchang330013China

The effects of wheel speeds on the magnetic properties and microstructures of[(Nd,Pr)_(1-x)Ce_(x)]-Fe-B meltspun ribbons were *** to melt-spun ribbons with low cerium(Ce)co.tent(x=0.2),amorphous formation can be suppressed at high wheel speed in the ribbons with a relatively high Ce co.tent(x=0.8),and with the increase of the wheel speed,the magnetic properties of the ribbons with high Ce co.tent raise *** high wheel speed,the co.rcivity mechanism of melt-spun ribbons is mainly pinning field,and the high wheel speed introduces a large number of defects into the matrix as pinning ***,ribbons with high Ce co.tent form a fine and uniform grain structure,so the grain boundary area enlarges,which further hinders the movement of domain *** co.bined effects of the above factors enable ribbons with high Ce co.tent to have excellent magnetic properties(Hcj=0.977 T,Mr=64 m^(2) A/kg)at the wheel speed of 35 m/s.

关键词： Wheel speed Ceco.tent Microstructure Magnetic properties Rare earths

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Purification performance on molten steel of novel Al_(2)O_(3)-based ceramic filter prepared from microporous powder and nano-Al_(2)O_(3) powder

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Journal of Iron and Steel Research International 2024年第6期31卷 1535-1546页

作者： Zhe Chen Wen Yan Ying Liu Guang-qiang Li Shao-song Hong Nan Li The State Key Laboratory of Refractories and Metallurgy Wuhan University of Science and TechnologyWuhan 430081HubeiChina Jiangsu Shengnai new materials co. Ltd.Taizhou 225534JiangsuChina

Reticulated ceramic foam filters provide an effective way to purify molten steel by removing non-metallic *** proposed a novel strategy to improve the purification performance of Al_(2)O_(3)-based ceramic filters by using microporous co.undum-spinel raw materials to replace dense raw *** kinds of Al_(2)O_(3)-based ceramic filters fabricated from dense α-Al_(2)O_(3) micro-powder or microporous co.undum-spinel powder were selected to carry out the immersion tests with molten *** the one hand,the higher surface roughness of the filter skeleton prepared from microporous raw materials increased the adsorption capacity of skeleton surface on inclusions in molten *** the other hand,the higher apparent porosity and larger pore size of the filter skeleton were more beneficial to the penetration of molten steel in the micropores of *** reaction process at the solid-liquid interface also improved the wettability of the interface between skeleton and molten steel,resulting in a larger penetration depth and a better adsorption effect on the *** summary,the novel Al_(2)O_(3)-based ceramic filter prepared with microporous co.undum-spinel powder and addition of 5 wt.% nano-Al_(2)O_(3) powder reduced the total oxygen co.tent of the steel from 40.2×10^(-4) to 12.7×10^(-4) wt.% by 68.4% and the Al co.tent from 0.46 to 0.18 wt.% by 60.9% after immersion test,presenting the most excellent purification performance on molten steel.

关键词： Al_(2)O_(3)-based ceramic filter Microporous co.undum-spinel powder Non-metallic inclusion-Microstructure Molten steel purification

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