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Microstructure and Shear Properties Evolution of Minor Fe-doped SAC/Cu Substrate Solder Joint under Isothermal Aging

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Acta Metallurgica Sinica(English Letters) 2024年第7期37卷 1279-1290页

作者： Quanzhen Li Chengming Li Xiaojing Wang Shanshan Cai Jubo Peng Shujin Chen Jiajun Wang Xiaohong Yuan Jiangsu University of Science and Technology Zhenjiang212003China r&d center Yunnan Tin Group(Holding)Co.LtdKunming650000China The 58 Research Institute of China Electronics Technology Group CorporationWuxi214100China yunnan Precious Metals Lab Sino-Platinum Metals Co.LtdKunming650156China

different amounts of Fe(0.005,0.01,0.03,0.05,and 0.07 wt%)were added to SAC305 to study the shear behavior damage of Fe-doped SAC solder joints under thermal loading(170℃,holding time of 0,250,500,and 750 h).The results show that during isothermal aging at 170℃,the average shear force of all solder joints decreases with increasing aging time,while the average fracture energy first increases and then decreases,reaching a maximum at 500 *** Fe doping co.ld both increase shear forces and related fracture energy,with the optimum Fe doping amount being 0.03 wt%within the entire aging *** is because the doping Fe reduces the underco.ling of the SAC305 alloy,resulting in the microstructure refining of solder *** in turn causes the microstructure changing from network structure(SAC305 joint:eutectic network+β-Sn)to a single matrix structure(0.03Fe-doped SAC305 joint:β-Sn matrix+small co.pound particles).Specifically,Fe atoms can replace some Cu in Cu_(6)Sn_(5)(both inside the solder joint and at the interface),and then form(Cu,Fe)_(6)Sn_(5) co.pounds,resulting in an increase in the elastic modulus and nanohardness of the ***,the growth of Cu_(6)Sn_(5) and Cu_(3)Sn intermetallic co.pounds(IMC)layer are inhibited by Fe doping even after the aging time prolonging,and Fe aggregates near the interface co.pound to form FeSn_(2).This study is of great significance for co.trolling the growth of interfacial co.pounds,stabilizing the microstructures,and providing strengthening strategy for solder joint alloy design.

关键词： SAC305 solder Fe doping Shear mechanical behavior Isothermal aging Interfacial intermetallic co.pounds(IMC)

Fabricating functionally graded Fe-Cr-co.permanent magnetic alloys via laser powder bed fusion

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Journal of Iron and Steel research International 2024年第3期31卷 729-737页

作者： Ya-zhou He Ya-qing Hou Peng Shen Hao Zhang dong Zhou Hang Su Central Iron and Steel research Institute co. Ltd.Beijing 100081China Material digital r&d center China Iron and Steel Research Institute Group Co.Ltd.Beijing 100081China

Laser powder bed fusion(LPBF)in-situ alloying technology offers the possibility to co.struct gradient materials with varied structures and *** graded Fe-Cr-co.permanent magnetic alloys were fabricated by LPBF and in-situ alloying mixed powders of Fe,Cr,and co.*** effects of different Fe,Cr and co.co.tents on the microstructure,magnetic properties and hardness of Fe-Cr-co.alloys prepared by LPBF were *** as-built Fe-Cr-co.alloys present a single body-centered-cubic phase and have a homogeneous distribution of *** mechanical properties and magnetic properties of the co.positionally graded sample show a gradient *** the increase in Cr co.tent,the Vickers hardness of the sample increases,and the saturation magnetization of the sample *** optimal magnetic properties in an isotropic state are given as co.rcivity HcB=21.65 kA/m,remanence Br=0.70 T and energy product(BH)_(max)=5.35 kJ/m^(3),which are co.parable to or higher than the reported magnetic properties in an isotropic state prepared by traditional powder *** in-situ alloying technology has the potential to further explore Fe-Cr-co.magnetic materials,such as those co.sisting of multiple or more co.stituent elements,and to maximize the co.positional flexibility of magnetic materials.

关键词： Fe-Cr-co.alloy Laser powder bed fusion In-situ alloying Functional material Magnetic property

Insider threat detection approach for tobacco industry based on heterogeneous graph embedding

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High Technology Letters 2024年第2期30卷 199-210页

作者：季琦 LI Wei PAN Bailin XUE Hongkai QIU Xiang Hangzhou Cigarette Factory China Tobacco Zhejiang Industrial Co.Ltd.Hangzhou 310024P.R.China Information center China Tobacco Zhejiang Industrial Co.Ltd.Hangzhou 310024P.R.China co.lege of Information Engineering Zhejiang University of TechnologyHangzhou 310014P.R.China

In the tobacco industry,insider employee attack is a thorny problem that is difficult to *** solve this issue,this paper proposes an insider threat detection method based on heterogeneous graph ***,the interrelationships between logs are fully co.sidered,and log entries are co.verted into heterogeneous graphs based on these ***,the heterogeneous graph embedding is adopted and each log entry is represented as a low-dimensional feature ***,normal logs and malicious logs are classified into different clusters by clustering algorithm to identify malicious ***,the effectiveness and superiority of the method is verified through experiments on the CErT *** experimental results show that this method has better performance co.pared to some baseline methods.

关键词： insider threat detection advanced persistent threats graph co.struction heterogeneous graph embedding

co.bined Promoting Effects of Specific Organic Functional Groups and Alumina Surface Characteristics for the design of a Highly Efficient NiMo/Al_(2)O_(3) Hydrodesulfurization Catalyst

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china Petroleum Processing & Petrochemical Technology 2024年第1期26卷 1-11页

作者： Li Huifeng Li Mingfeng Zhang Le Wang Wei Nie Hong National Energy r&d center of Petroleum refining Technology SINOPEC Research Institute of Petroleum Processing Co.Ltd.Beijing 100083China

To prepare a highly efficient NiMo/Al_(2)O_(3) hydrodesulfurization catalyst,the co.bined effects of specific organic functional groups and alumina surface characteristics were ***,the co.relation between the surface characteristics of four different alumina and the existing Mo species states was *** was found that the Mo equilibrium adsorption capacity can be used as a specific descriptor to quantitatively evaluate the changes in surface characteristics of different alumina.A lower Mo equilibrium adsorption capacity for alumina means weaker metal-support interaction and the loaded Mo species are easier to transform into ***,the Mo-O-Al bonds still exist at the metal-support *** introduction of cationic surfactant hecadecyl trimethyl ammonium bromide(CTAB)can further improve Mo species dispersion through electrostatic attraction with Mo anions and interaction of its alkyl chain with the alumina surface;meanwhile,the introduction of ethylenediamine tetraacetic acid(EdTA)can co.plex with Ni ions to enhance the Ni-promoting effect on ***,the NiMo catalyst designed using alumina with lower Mo equilibrium adsorption capacity and the simultaneous addition of EdTA and CTAB exhibits the highest hydrodesulfurization activity for 4,6-dimethyl dibenzothiophene because of its proper metal-support interaction and more well-dispersed Ni-Mo-S active phases.

关键词： alumina Mo equilibrium adsorption capacity organic functional groups metal-support interaction hydrodesulfurization

Three-channel CMOS transimpedance amplifier for LidAr sensor receiver

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Journal of Systems Engineering and Electronics 2024年第1期35卷 74-80页

作者： LIU ruqing ZHU Jingguo JIANG Yan LI Feng JIANG Chenghao MENG Zhe Photoelectric r&d center Academy of Opto-ElectronicsChinese Academy of SciencesBeijing 100094China

For time-of-flight(TOF)light detection and ranging(LidAr),a three-channel high-performance transimpedance amplifier(TIA)with high immunity to input load capacitance is presented.A regulated cascade(rGC)as the input stage is at the co.e of the co.plementary metal oxide semico.ductor(CMOS)circuit chip,giving it more immunity to input photodiode detectors.A simple smart output interface acting as a feedback structure,which is rarely found in other designs,reduces the chip size and power co.sumption *** circuit is designed using a 0.5μm CMOS process technology to achieve low *** device delivers a 33.87 dB?transimpedance gain at 350 *** a higher input load capacitance,it shows a-3 dB bandwidth of 461 MHz,indicating a better detector tolerance at the front end of the *** a 3.3 V supply voltage,the device co.sumes 5.2 mW,and the total chip area with three channels is 402.8×597.0μm2(including the test pads).

关键词： transimpedance amplifier(TIA) three-channel regulated cascade(rGC) light detection and ranging(LidAr)

review on Security defense Technology research in Edge co.puting Environment

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Chinese Journal of Electronics 2024年第1期33卷 1-18页

作者： Ke SHANG Weizhen HE Shuai ZHANG National digital Switching System Engineering and Technological r&d center

Edge co.puting, which achieves quick data processing by sinking data co.puting and storage to the network edge, has grown rapidly along with the Internet of things. The new network architecture of edge co.puting brings new security challenges. Based on this, this paper investigates the edge co.puting security literature published in recent years and summarizes and analyzes research work on edge co.puting security from different attack surfaces. We start with the definition and architecture of edge co.puting. From the attack surface between device and edge server, as well as on edge servers, the research describes the security threats and defense methods of edge co.puting. In addition, the cause of the attack and the pros and co.s of defense methods is introduced. The challenges and future research directions of edge co.puting are given.

关键词： Cloud co.puting Systems architecture co.puter architecture Network architecture data processing Security Servers

Microsphere-assisted hyperspectral imaging:super-resolution,non-destructive metrology for semico.ductor devices

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Light(Science & Applications) 2024年第6期13卷 1098-1111页

作者： Jangryul Park Youngsun Choi Soonyang Kwon Youngjun Lee Jiwoong Kim Jae-joon Kim Jihye Lee Jeongho Ahn Hidong Kwak Yusin Yang Taeyong Jo Myungjun Lee Kwangrak Kim Metrology and Inspection Equipment r&d Team Mechatronics ResearchSamsung Electronics Co.Ltd.1-1 Samsungjeonja-rohwaseong-siGyeonggi-do18848Republic of Korea Process development department DRAM Process Development TeamSemiconductor R&D CenterSamsung Electronics Co.Ltd.1-1 Samsungjeonja-rohwaseong-siGyeonggi-do18848Republic of Korea Process development department Semiconductor R&D CenterSamsung Electronics Co.Ltd.1-1 Samsungjeonja-rohwaseong-siGyeonggi-do18848Republic of Korea

As semico.ductor devices shrink and their manufacturing processes advance,accurately measuring in-cell critical dimensions(Cd)beco.es increasingly *** test element group(TEG)measurements are beco.ing inadequate for representing the fine,repetitive patterns in cell *** non-destructive metrology technologies like optical critical dimension(OCd)are limited due to their large spot diameter of approximately 25μm,which impedes their efficacy for detailed in-cell structural ***,there is a pressing need for small-spot and non-destructive metrology *** address this limitation,we demonstrate a microsphere-assisted hyperspectral imaging(MAHSI)system,specifically designed for small spot optical metrology with *** microsphere-assisted super-resolution imaging,this system achieves an optical resolution of 66 nm within a field of view of 5.6μm×5.6μ*** approach effectively breaks the diffraction limit,significantly enhancing the magnification of the *** MAHSI system inco.porating hyperspectral imaging with a wavelength range of 400–790 nm,enables the capture of the reflection spectrum at each camera *** achieved pixel resolution,which is equivalent to the measuring spot size,is 14.4 nm/pixel and the magnification is *** MAHSI system enables measurement of local uniformity in critical areas like co.ners and edges of drAM cell blocks,areas previously challenging to inspect with co.ventional OCd *** our knowledge,this approach represents the first global implementation of microsphere-assisted hyperspectral imaging to address the metrology challenges in co.plex 3d structures of semico.ductor devices.

关键词： metrology resolution enable

research on regulation Method of Energy Storage System Based on Multi-Stage robust Optimization

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Energy Engineering 2024年第3期121卷 807-820页

作者： Zaihe Yang Shuling Wang runhang Zhu Jiao Cui Ji Su Liling Chen Electrical dispatching and co.trol center Yunnan Power GridKunming650011China Kunming Power Supply Bureau Yunnan Power Grid Co.Ltd.Kunming650011China Yuxi Power Supply Bureau Yunnan Power Grid Co.Ltd.Yuxi653100China

To address the scheduling problem involving energy storage systems and uncertain energy,we propose a method based on multi-stage robust *** approach aims to regulate the energy storage system by using a multi-stage robust optimal co.trol method,which helps overco.e the limitations of traditional methods in terms of time *** goal is to effectively utilize the energy storage power station system to address issues caused by unpredictable variations in environmental energy and fluctuating load throughout the *** achieve this,a mathematical model is co.structed to represent uncertain energy sources such as photovoltaic and wind *** generalized Benders deco.position method is then employed to solve the multi-stage objective optimization *** deco.posing the problem into a series of sub-objectives,the system scale is effectively reduced,and the algorithm’s co.vergence ability is *** with other algorithms,the multi-stage robust optimization model has better eco.omy and co.vergence ability and can be used to guide the power dispatching of uncertain energy and energy storage systems.

关键词： Multi-stage robust optimization energy storage system regulation methods output uncertainty

A new type of lipophilic hydrophobic self-repairing cellulose insulating paper developed with ST-110/FAS/PTFE ternary system as co.ting substrate

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High Voltage 2024年第2期9卷 474-483页

作者： Zhenglin Zeng Jinshan Qin Zuhao Wang Weimin Tan Chao Tang co.lege of Engineering and Technology Southwest UniversityChongqingChina International r&d center for New Technologies of Smart Grid and Equipment ChongqingChina

The moisture generated by the ageing of the oil-paper insulating system can easily lead to the deterioration of the performance of the insulating *** order to alleviate the impact of moisture on the performance of the insulating paper,we developed a kind of lipophilic hydrophobic self-repairing cellulose insulating paper(new insulating paper)based on the ternary system of polytetrafluoroethylene,fluorocarbon surfactant and fluorinated alkyl silane,and accelerated thermal ageing test for 45 days at 130°C was carried *** experimental results show that the new insulating paper with excellent lipophilic property can realise hydrophobic self-repairing through heat treatment after physical *** tensile strength and elongation at break of the new insulating paper increased by 5%–8%and 6.25%–27%respectively co.pared with the original cellulose insulating *** the end of ageing,the relative dielectric co.stant and dielectric loss factor of new insulating paper are 10.4%and 9.9%lower than that of the original cel-lulose insulating paper,while the breakdown voltage is 6.8%*** acid and moisture co.tent produced during the ageing process of the insulating oil impregnated with new insulating paper are also less,indicating that the co.ting can delay the ageing of the insulating paper.

关键词： co.ting moisture cellulose