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Journal of Energy Chemistry 2024年第8期95卷 241-249,I0006页

作者： Lin Su Ruining Fu Shuangying Lei Yuchen Pan Chongyang Zhu Pengcheng Liu Feng Xu SEU-FEI Nano-pico center Key Laboratory of MEMS of the Ministry of EducationSoutheast UniversityNanjing210096China

Alloy-typed anode materials,endowed innately with high theoretical specific capacity,hold great promise as an alternative to intercalation-typed counterparts for alkali-ion *** tremendous efforts devoted to addressing drastic volume change and severe pulverization issues of such anodes,the underlying mechanisms involving dynamic phase evolutions and reaction kinetics have not yet been fully ***,taking antimony(Sb)anode as a representative paradigm,its microscopic operating mechanisms down to the atomic scale during live(de)potassiation cycling are systematically unraveled using in situ transmission electron *** reversible phase transformations at single-particle level,that are Sb←→KSb_(2)←→KSb←→K_5Sb_(4)←→K_(3)Sb,were revealed during ***,multiple phase interfaces associated with different reaction kinetics coexisted and this phenomenon was properly elucidated in the context of density functional theory ***,previously unexplored unidirectional circulation of reaction interfaces within individual Sb particle is confirmed for both potassiation and *** on the empirical results,the surface diffusion-mediated potassiation-depotassiation pathways at single-particle level are *** work affords new insights into energy storage mechanisms of Sb anode and valuable guidance for targeted optimization of alloy-typed anodes(not limited to Sb)toward advanced potassium-ion batteries.

关键词： Alloy-typed anode Potassium storage mechanism In situ transmission electron microscopy Reaction interface

Visualizing the crystallization of sodium chloride under supersaturated condition

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Nano Research 2024年第8期17卷 7786-7792页

作者： Mao Ye Tao Xu Yuwei Xiong Yatong Zhu Mingrui Zhou Longxiang Han Jinyi Sun Ming Qin Litao Sun SEU-FEI Nano-pico center Key Laboratory of MEMS of Ministry of EducationSchool of Integrated CircuitsSoutheast UniversityNanjing 210096China

Crystallization in supersaturated solution plays a fundamental role in a variety of natural and industrial ***,a thorough understanding of crystallization phenomena in supersaturated solution is still difficult because the real-time visualization of crystallization processes under supersaturated condition is a great ***,an electron beam-induced crystallization method was carried out in in situ liquid cell transmission electron microscopy(TEM)to visualize the crystallization of NaCl under supersaturated condition in real *** steps and behaviors in the crystallization of NaCl were captured and clarified,including the growth of NaCl nanocrystals with different morphologies,the formation of initial crystalline seeds from amorphous ion clusters,and the non-equilibrium growth behaviors caused by uneven distribution of precursor *** study provides the real-time visualization of detailed nucleation and growth behaviors in NaCl crystallization and brings an ideal strategy for investigating crystallization phenomena under supersaturated condition.

关键词： crystallization in situ liquid cell transmission electron microscopy(TEM) electron-water interaction sodium chloride

Etching of quartz crystals in liquid phase environment:A review

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Nanotechnology and Precision Engineering 2024年第2期7卷 87-109页

作者： Yide Dong Yike Zhou Haizhou Huang Bosong Zhang Xihan Li Kaiwen Chen Litao Sun Guangbin Dou SEU-FEI Nano-pico center Key Laboratory of MEMS of Ministry of EducationSoutheast UniversityNanjing 210096People’s Republic of China Nanjing Jingxin Optoelectronics Research Institute Nanjing 210096People’s Republic of China

Quartz crystals are the most widely used material in resonant sensors,owing to their excellent piezoelectric and mechanical *** the development of portable and wearable devices,higher processing efficiency and geometrical precision are *** etching has been proven to be the most efficient etching method for large-scale production of quartz devices,and many wet etching approaches have been developed over the ***,until now,there has been no systematic review of quartz crystal etching in liquid phase ***,this article provides a comprehensive review of the development of wet etching processes and the achievements of the latest research in thisfield,covering conventional wet etching,additive etching,laser-induced backside wet etching,electrochemical etching,and electrochemical discharge *** each technique,a brief overview of its characteristics is provided,associated problems are described,and possible solutions are *** review should provide an essential reference and guidance for the future development of processing strategies for the manufacture of quartz crystal devices.

关键词： Quartz crystal Materials processing Wet etching Microfabrication Quartz MEMS

Anisotropic metal–insulator transition in strained VO_(2)(B) single crystal

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Chinese Physics B 2024年第6期33卷 56-61页

作者：马泽成闫胜楠刘增霖徐涛陈繁强陈思成曹天俊孙立涛程斌梁世军缪峰 Institute of Brain-Inspired Intelligence National Laboratory of Solid State MicrostructuresSchool of PhysicsCollaborative Innovation Center of Advanced MicrostructuresNanjing UniversityNanjing 210093China SEU-FEI Nano-pico center Key Laboratory of MEMS of Ministry of EducationSoutheast UniversityNanjing 210096China Institute of Interdisciplinary of Physical Sciences School of ScienceNanjing University of Science and TechnologyNanjing 210094China

Mechanical strain can induce noteworthy structural and electronic changes in vanadium dioxide, imparting substantial scientific importance to both the exploration of phase transitions and the development of potential technological applications. Unlike the traditional rutile(R) phase, bronze-phase vanadium dioxide [VO_(2)(B)] exhibits an in-plane anisotropic structure. When subjected to stretching along distinct crystallographic axes, VO_(2)(B) may further manifest the axial dependence in lattice–electron interactions, which is beneficial for gaining insights into the anisotropy of electronic ***, we report an anisotropic room-temperature metal–insulator transition in single-crystal VO_(2)(B) by applying in-situ uniaxial tensile strain. This material exhibits significantly different electromechanical responses along two anisotropic *** reveal that such an anisotropic electromechanical response mainly arises from the preferential arrangement of a straininduced unidirectional stripe state in the conductive channel. This insulating stripe state could be attributed to the in-plane dimerization within the distorted zigzag chains of vanadium atoms, evidenced by strain-modulated Raman spectra. Our work may open up a promising avenue for exploiting the anisotropy of metal–insulator transition in vanadium dioxide for potential technological applications.

关键词： vanadium dioxide strain anisotropy electrical transport

From Digital Human Modeling to Human Digital Twin: Framework and Perspectives in Human Factors

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Chinese Journal of Mechanical Engineering 2024年第1期37卷 1-14页

作者： Qiqi He Li Li Dai Li Tao Peng Xiangying Zhang Yincheng Cai Xujun Zhang Renzhong Tang State Key Laboratory of Fluid Power Components and Mechatronic Systems Zhejiang UniversityHangzhou 310027China ZJU-Sunon Joint Research center for Smart Furniture Zhejiang UniversityHangzhou 310027China pico-Lab Bytedance Inc.Shanghai 200233China Sunon Technology Co. Ltd.Hangzhou 311215China

The human digital twin(HDT)emerges as a promising human-centric technology in Industry 5.0,but challenges remain in human modeling and *** human modeling(DHM)provides solutions for modeling and simulating human physical and cognitive aspects to support ergonomic ***,it has limitations in real-time data usage,personalized services,and timely *** emerging HDT concept offers new possibilities by integrating multi-source data and artificial intelligence for continuous monitoring and ***,this paper reviews the evolution from DHM to HDT and proposes a unified HDT framework from a human factors *** framework comprises the physical twin,the virtual twin,and the linkage between these *** virtual twin integrates human modeling and AI engines to enable model-data-hybrid-enabled *** can potentially upgrade traditional ergonomic methods to intelligent services through real-time analysis,timely feedback,and bidirectional ***,the future perspectives of HDT for industrial applications as well as technical and social challenges are *** general,this study outlines a human factors perspective on HDT for the first time,which is useful for cross-disciplinary research and human factors innovation to enhance the development of HDT in industry.

关键词： Human digital twin Digital human modeling Human factors Human-centric technology

Ultrasensitive Mechanical Sensor Using Tunable Ordered Array of Metallic and Insulating States in Vanadium Dioxide

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Chinese Physics Letters 2024年第7期41卷 74-86页

作者：马泽成闫胜楠陈繁强戴玉頔刘增霖徐康徐涛童湛钦陈墨雨王利铮王鹏飞孙立涛程斌梁世军缪峰 Institute of Brain-Inspired Intelligence National Laboratory of Solid State MicrostructuresSchool of PhysicsCollaborative Innovation Center of Advanced MicrostructuresNanjing UniversityNanjing 210093China SEU-FEI Nano-pico center Key Laboratory of MEMS of Ministry of EducationSoutheast UniversityNanjing 210096China Institute of Interdisciplinary of Physical Sciences School of ScienceNanjing University of Science and TechnologyNanjing 210094China

Detecting tiny deformations or vibrations, particularly those associated with strains below 1%, is essential in various technological applications. Traditional intrinsic materials, including metals and semiconductors, face challenges in simultaneously achieving initial metallic state and strain-induced insulating state, hindering the development of highly sensitive mechanical sensors. Here we report an ultrasensitive mechanical sensor based on a strain-induced tunable ordered array of metallic and insulating states in the single-crystal bronze-phase vanadium dioxide [VO_(2)(B)] quantum material. It is shown that the initial metallic state in the VO_(2)(B) flake can be tuned to the insulating state by applying a weak uniaxial tensile strain. Such a unique property gives rise to a record-high gauge factor of above 607970, surpassing previous values by an order of magnitude, with excellent linearity and mechanical resilience as well as durability. As a proof-of-concept application, we use our proposed mechanical sensor to demonstrate precise sensing of the micro piece, gentle airflows and water droplets. We attribute the superior performance of the sensor to the strain-induced continuous metal-insulator transition in the single-crystal VO_(2)(B) flake, evidenced by experimental and simulation results. Our findings highlight the potential of exploiting correlated quantum materials for next-generation ultrasensitive flexible mechanical sensors, addressing critical limitations in traditional materials.

关键词： metallic durability hinder

Flexible printed three dimensional(3D) integrated carbon nanotube complementary metal oxide semiconductor(CMOS) thin film transistors and circuits

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Science China(Information Sciences) 2024年第09期67卷 280-293页

作者： Zhaofeng CHEN Jiaqi LI Min LI Hongxuan GUO Jianwen ZHAO SEU-FEI Nano-pico center Key Laboratory of MEMS of Ministry of Education Southeast University Printable Electronics Research center Division of Nanodevices and Related NanomaterialsSuzhou Institute of Nano-Tech and Nano-Bionics Chinese Academy of Sciences School of Nano Technology and Nano Bionics University of Science and Technology of China

The threshold voltage modulation of carbon nanotube thin-film transistors（TFTs） and flexible three-dimensional（3D） integration circuits has become hot research topics for carbon-based electronics. In this paper, a doping-free gate electrode technology is introduced to significantly modulate the threshold voltage of polymer-sorted semiconducting single-walled carbon nanotube（sc-SWCNT） TFTs in combination with the highly effective gate-controlling ability of solid-state electrolyte thin films as the dielectrics. A systematic investigation was conducted on the impact of printed silver, evaporated silver, and evaporated aluminum（Al） gate electrodes on the threshold voltage of flexible printed bottom-gate and top-gate SWCNT TFTs. The results indicate that the SWCNT TFTs with Al gate electrodes exhibit enhancement-mode characteristics with excellent electrical properties, such as the negative threshold voltages（-0.6 V）, high Ion/Ioff（up to 10～6）, low subthreshold swing(61.4 mV · dec-1), and small hysteresis. It is attributed to either the formation of lower work function thin films（Al2O3） at the electrode/dielectric layer interfaces through the natural oxidation of the Al bottom-gate electrodes or the dipole reaction of the Al top-gate electrodes from X-ray photoelectron spectroscopy（XPS） and ultraviolet photoelectron spectroscopy（UPS） data. In addition, 3D complementary metal-oxide-semiconductor（CMOS） inverters with common gate electrodes were constructed using the resulting enhancement-mode P-type SWCNT TFTs and matched N-type SWCNT TFTs, which shows high voltage gain（34）, rail-to-rail output and high noise margins(80.04%, VDD=-1 V)as well good mechanical flexibility at low operation voltages. It demonstrates that SWCNT TFTs have great advantages for building large-scale 3D flexible integrated circuits.

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通过激光/分散系耦合增强氧化石墨烯的还原效果:实现大规模、低缺陷的石墨烯用于无折痕散热膜在先进柔性电子器件中的应用

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Science Bulletin 2024年第11期69卷 1716-1727页

作者：孙佳惟熊雨薇贾海洋韩龙祥叶雯孙立涛 College of Electronic and Information Engineering Suzhou University of Science and TechnologySuzhou 215009China SEU-FEI Nano-pico center Key Laboratory of MEMS of Ministry of EducationSoutheast UniversityNanjing 210096China School of Physics and New Energy Xuzhou University of TechnologyXuzhou 221018China Jiangsu Industrial Intelligent and Low-carbon Technology Engineering center Suzhou 215000China Suzhou Key Laboratory of Intelligent Low-carbon Technology Application Suzhou 215000China College of Chemistry and Life Sciences Suzhou University of Science and TechnologySuzhou 215009China

The advancement of flexible electronics demands improved components,necessitating heat dissipation membranes(HDMs)to exhibit high thermal conductivity while maintaining structural integrity and performance stability even after extensive ***,we have devised a laser-modulated reduction technique for graphene oxide(GO),enabling the fabrication of high-quality,large-scale,lowdefect graphene,which yields high-performance HDMs after orderly *** work underscores the crucial role of the laser wavelength and dispersion liquid's coupling intensity in influencing the morphology and properties of *** coupling effect and energy conversion are realized when a laser of 1064 nm wavelength irradiates a triethylene glycol(TEG)/N,N-Dimethylformamide(DMF)*** unique synergy generates high transient energy,which facilitates the deprotonation process and ensures a swift,comprehensive GO *** contrast to conventional water-based laser reduction methods,the accelerated reaction magnifies the size of the graphene sheets by mitigating the ablation *** membrane construction with an ordered structure,the corresponding membrane exhibits a high thermal conductivity of 1632 W m^(-1)K^(-1),requiring only~1/10 of the total preparation time required by other reported ***,the resulting HDM demonstrates superior resilience against creasing and folding,maintaining excellent smoothness and negligible reduction in thermal conductivity after violent *** combination of exceptional flexibility and thermal conductivity in HDMs paves the way for long-term practical use in the flexible electronics industry.

关键词： Laser-irradiation technology System coupling Graphene-based Heat dissipation membranes Crease-free

Two-dimensional materials for future information technology: status and prospects

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Science China(Information Sciences) 2024年第6期67卷 1-147页

作者： Hao QIU Zhihao YU Tiange ZHAO Qi ZHANG Mingsheng XU Peifeng LI Taotao LI Wenzhong BAO Yang CHAI Shula CHEN Yiqi CHEN Hui-Ming CHENG Daoxin DAI Zengfeng DI Zhuo DONG Xidong DUAN Yuhan FENG Yu FU Jingshu GUO Pengwen GUO Yue HAO Jun HE Xiao HE Jingyi HU Weida HU Zehua HU Xinyue HUANG Ziyang HUANG Ali IMRAN Ziqiang KONG Jia LI Qian LI Weisheng LI Lei LIAO Bilu LIU Can LIU Chunsen LIU Guanyu LIU Kaihui LIU Liwei LIU Sheng LIU Yuan LIU Donglin LU Likuan MA Feng MIAO Zhenhua NI Jing NING Anlian PAN Tian-Ling REN Haowen SHU Litao SUN Yue SUN Quanyang TAO Zi-Ao TIAN Dong WANG Hao WANG Haomin WANG Jialong WANG Junyong WANG Wenhui WANG Xingjun WANG Yeliang WANG Yuwei WANG Zhenyu WANG Yao WE Department of Applied Physics The Hong Kong Polytechnic University Key Laboratory for Micro-Nano Physics and Technology of Hunan Province College of Materials Science and EngineeringHunan University College of Integrated Circuits Zhejiang University Shenzhen Geim Graphene center Shenzhen Key Laboratory of Layered Materials for Value-Added ApplicationsTsinghua-Berkeley Shenzhen Institute & Institute of Materials ResearchTsinghua Shenzhen International Graduate SchoolTsinghua University State Key Laboratory of Extreme Photonics and Instrumentation College of Optical Science and EngineeringInternational Research Center for Advanced PhotonicsZijingang CampusZhejiang University National Key Laboratory of Materials for Integrated Circuits Shanghai Institute of Microsystem and Information TechnologyChinese Academy of Sciences CAS Key Laboratory of Nanophotonic Materials and Devices & Key Laboratory of Nanodevices and Applications i-LabSuzhou Institute of Nano-Tech and Nano-Bionics (SINANO)Chinese Academy of Sciences College of Chemistry and Chemical Engineering Hunan University Key Laboratory of Quantum State Construction and Manipulation (Ministry of Education) Department of PhysicsRenmin University of China School of Integrated Circuits Beijing National Research Center for Information Science and Technology (BNRist)Tsinghua University School of Electronic Science and Engineering Nanjing University The State Key Discipline Laboratory of Wide Band Gap Semiconductor Technology Shaanxi Joint Key Laboratory of GrapheneSchool of MicroelectronicsXidian University Key Laboratory of Artificial Micro- and Nano-Structures of Ministry of Education School of Physics and TechnologyWuhan University School of Integrated Circuits Huazhong University of Science and Technology center for Nanochemistry (CNC) Beijing Science and Engineering Center for NanocarbonsBeijing National Laboratory for Molecular SciencesCollege of Chemistry and Molecular EngineeringPeking University State Key Laboratory for Artificial Microstruct

Over the past 70 years, the semiconductor industry has undergone transformative changes,largely driven by the miniaturization of devices and the integration of innovative structures and materials. Two-dimensional(2D) materials like transition metal dichalcogenides(TMDs) and graphene are pivotal in overcoming the limitations of silicon-based technologies, offering innovative approaches in transistor design and functionality, enabling atomic-thin channel transistors and monolithic 3D integration. We review the important progress in the application of 2D materials in future information technology, focusing in particular on microelectronics and optoelectronics. We comprehensively summarize the key advancements across material production, characterization metrology, electronic devices, optoelectronic devices, and heterogeneous integration on silicon. A strategic roadmap and key challenges for the transition of 2D materials from basic research to industrial development are outlined. To facilitate such a transition, key technologies and tools dedicated to 2D materials must be developed to meet industrial standards, and the employment of AI in material growth, characterizations, and circuit design will be essential. It is time for academia to actively engage with industry to drive the next 10 years of 2D material research.

关键词： two-dimensional (2D) materials information technology production technology standardization of characterization microelectronicdevices optoelectronic devices multi-functional integration

Combining in-situ TEM observations and theoretical calculation for revealing the thermal stability of CeO_(2) nanoflowers

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Nano Research 2022年第2期15卷 1319-1326页

作者： Mingyun Zhu Kuibo Yin Yifeng Wen Shugui Song Yuwei Xiong Yunqian Dai Litao Sun SEU-FEI Nano-pico center Key Laboratory of MEMS of Ministry of EducationSoutheast UniversityNanjing 210096China School of Chemistry and Chemical Engineering Southeast UniversityNanjing 211189China

The thermal stability of Ce_(2) nanomaterials can directly impact both the uniformity of the supported catalysts and the catalytic behavior of Ce_(2) ***,knowledge about the thermal stability of Ce_(2) is still ***,we conduct in-situ transmission electron microscopy experiments and theoretical calculations to elucidate the thermal stability of Ce_(2) nanomaterials under different environments.A sinter(700℃)are observed within Ce_(2) nanoflowers under O_(2).The sinter firstly occurs among the nanoflowers’monomers and then the sintered nanoparticles structurally decompose to tiny nanoparticles from the strain *** a vacuum environment,the Ce_(2) nanoflowers firstly undergo a transition from cubic fluorite Ce_(2) to hexagonal Ce_(2)O_(3),accompanied by the oxygen *** Ce_(2)O_(3) nanoparticles further atomically sublimate from the edges to the center under high *** calculation results reveal a considerably lower energy barrier for the structural decomposition under O_(2) and for the sublimation under *** work provides a perspective on the structural design and performance optimization of Ce_(2)-based catalysts.

关键词： CeO_(2) in-situ transmission electron microscopy structural evolution thermal stability theoretical calculation