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Adsorption behavior of CO2/H2S mixtures in calcite slit nanopores for CO2 storage:An insight from molecular perspective

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petroleum Science 2024年第4期21卷 2444-2456页

作者： Cheng Qian Zhen-Hua Rui Yue-Liang Liu Kai Du Chen Liu Yang Zhao Xiao-Min Ma State Key Laboratory of petroleum Resources and engineering China University of Petroleum College of petroleum engineering China University of Petroleum College of Carbon Neutrality Future Technology China University of Petroleum College of petroleum China University of Petroleum-Beijing at Karamay College of Mining engineering Taiyuan University of Technology

It is acknowledged that injecting CO2into oil reservoirs and saline aquifers for storage is a practical and affordable method for *** CO2produced from industrial exhaust contains impurity gases such as H2S that might impact CO2sequestration due to competitive *** study makes a commendable effort to explore the adsorption behavior of CO2/H2S mixtures in calcite slit *** Canonical Monte Carlo（GCMC） simulation is employed to reveal the adsorption of CO2,H2S as well as their binary mixtures in calcite *** show that the increase in pressure and temperature can promote and inhibit the adsorption capacity of CO2and H2S in calcite nanopores,***2exhibits stronger adsorption on calcite surface than *** energy plays the dominating role in the adsorption *** energy accounts for 97.11% of the CO2-calcite interaction energy and 56.33% of the H2S-calcite interaction energy at 10 MPa and 323.15 *** presence of H2S inhibits the CO2adsorption in calcite nanopores due to competitive adsorption,and a higher mole fraction of H2S leads to less *** quantity of CO2adsorbed is lessened by approximately 33% when the mole fraction of H2S reaches ***2molecules preferentially occupy the regions near the po re wall and H2S molecules tend to reside at the center of nanopore even when the molar ratio of CO2is low,indicating that CO2has an adsorption priority on the calcite surface over *** addition,moisture can weaken the adsorption of both CO2and H2S,while CO2is more *** interestingly,we find that pure CO2is more suitable to be sequestrated in the shallower formations,i.e.,500-1500 m,whereas CO2with H2S impurity should be settled in the deeper reservoirs.

关键词： Adsorption behavior CO 2 /H 2 S binary mixtures Molecular perspective Calcite slit nanopores CO 2 sequestration

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Auto-tuning PVT data using multi-objective optimization: Application of NSGA-Ⅱ algorithm

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petroleum 2024年第1期10卷 135-149页

作者： Abdolhadi Zarifi Mohammad Madani Mohammad Jafarzadegan Reservoir engineering Systems Petroleum Engineering Department Main Office Building of National Iranian South Oil Company (NISOC) Combined Planning Management National Iranian Oil Company (NIOC) Reservoir engineering Division Petroleum Engineering Department Petroleum Engineering and Development Company (PEDEC)

Reservoir simulation is known as perhaps the most widely used, accurate, and reliable method for field development in the petroleum industry. An integral part of a reliable reservoir simulation process is to consider robust and rigorous tuned EOS models. Traditionally, EOS models are tuned iteratively through arduous workflows against experimental PVT data. However, this comes with a number of drawbacks such as forcingly using weight factors, which upon alteration adversely affects the optimization *** objective of the current work is thus to introduce an auto-tune PVT matching tool using NSGA-II multi-objective optimization. In order to illustrate the robustness of the presented technique, three different PVT samples are used, including two black-oil and one gas condensate sample. We utilize PengRobinson EOS during all the manual and auto-tuning processes. Comparison of auto-tuned EOS-generated results with those of experimental and computed statistical error values for these samples clearly show that the proposed method is robust. In addition, the proposed method, contrary to the manual matching process, provides the engineer with several matched solutions, which allows them to select a match based on the engineering background to be best amenable to the problem at hand. In addition, the proposed technique is fast, and can output several solutions within less time compared to the traditional manual matching method.

关键词： Auto-tuning PVT Equation of state NSGA-II Multi-objective optimization

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Hole cleaning evaluation and installation spacing optimization of cuttings bed remover in extended-reach drilling

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petroleum Science 2024年第3期21卷 2005-2022页

作者： Shuo Peng Wen-Jun Huang De-Li Gao MOE Key Laboratory of petroleum engineering China University of Petroleum-BeijingBeijing102249China State Key Laboratory of petroleum Resources and engineering China University of Petroleum-BeijingBeijing102249China

In extended-reach or long-horizontal drilling,cuttings usually deposit at the bottom of the *** cuttings accumulate to a certain thickness,complex problems such as excessive torque and drag,tubing buckling,and pipe stuck probably occur,which results in a lot of non-productive time and remedial *** bed remover can efficiently destroy deposited cuttings in time through hydraulic and mechanical stirring *** paper aims to build a method for hole cleaning evaluation and installation spacing optimization of cuttings bed remover to improve the wellbore cleaning ***,a Computational Fluid Dynamics approach with Eulerian—Eulerian multiphase model was utilized to investigate the mechanism of cuttings transportation,and a new type of cuttings bed remover was ***,an evaluation method of hole cleaning effect of remover was *** that,the effects of several drilling parameters on hole cleaning including flow rate of drilling fluid,rotational speed of drillpipe,rate of penetration,wellbore size,rheological property of drilling fluid,and remover eccentricity on the performance of cuttings bed remover were *** results demonstrate that the new type of remover with streamline blade performs better than conventional *** efficiency of hole cleaning is greatly improved by increasing the rotational speed of drillpipe,flow rate of drilling fluid,remover eccentricity,and 6 rpm Fann dial reading for drilling *** higher rate of penetration and large wellbore size result in worse hole *** findings can serve as an important guide for the structure optimization design of cuttings bed remover and installation spacing of removers.

关键词： Extended-reach drlling Drilling hydraulics Cuttings transport Hole cleaning Cuttings bed remover

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Experimental investigation into effects of the natural polymer and nanoclay particles on the EOR performance of chemical flooding in carbonate reservoirs

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petroleum Science 2024年第2期21卷 951-961页

作者： Amir Mohammad Zamani Ashkan Moslemi Kamran Hassani department of petroleum engineering Islamic Azad University Science and Research BranchTehranIran Institute of petroleum engineering University of TehranTehranIran

This paper aims to investigate the tragacanth gum potential as a natural polymer combined with natural clay mineral(montmorillonite,kaolinite,and illite)nanoparticles(NPs)to form NP-polymer suspension for enhanced oil recovery(EOR)in carbonate *** gravimetric analysis(TGA)tests were conducted initially in order to evaluate the properties of tragacanth ***,scanning electron microscopy(SEM)and energy-dispersive X-ray(EDX)tests were used to detect the structure of clay *** various scenarios,the effects of natural NPs and polymer on the wettability alteration,interfacial tension(IFT)reduction,viscosity improvement,and oil recovery were investigated through contact angle system,ring method,Anton Paar viscometer,and core flooding tests,*** entire experiment was conducted at 25,50,and 75℃,*** to the experimental results,the clay minerals alone did not have a significant effect on viscosity,but the addition of minerals to the polymer solution leads to the viscosity enhancement remarkably,resulting mobility ratio *** clay NPs,the combination of natural polymer and kaolinite results in increased viscosity at all *** wettability alteration was also observed in the case of natural polymer and illite *** in combination with natural polymer showed an ability in reducing ***,the results of displacement experiments revealed that the combination of natural polymer and kaolinite could be the best option for EOR due to its substantial ability to improve the recovery factor.

关键词： Chemical flooding Tragacanth gum Clay nanoparticle Wettability IFT

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Studying the effect of surfactant assisted low-salinity water flooding on clay-rich sandstones

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petroleum 2024年第2期10卷 306-318页

作者： Saeed Khezerloo-ye Aghdam Alireza Kazemi Mohammad Ahmadi department of petroleum engineering Amirkabir University of Technology (AUT) department of petroleum and Chemical engineering College of Engineering Sultan Qaboos University

Sandstone reservoirs often contain clay particles that can cause damage and reduce permeability during low-salinity water flooding. In this study, the effect of surfactants on fine migration in clay-rich sandstones and its impact on oil recovery was ***, the impact of surfactants on interparticle forces in fine-matrix, fine-fine, and oil-matrix systems was modeled. The results showed that both CTAB(cetyltrimethyl ammonium bromide) and QS(quillaja saponin) cause EDL compaction, weakening the repulsive forces. However, SDS(sodium dodecyl sulfate)and TX(triton X-100) do not affect the EDL. Next, the effect of surfactants on IFT reduction and wettability alteration was experimentally investigated. All surfactants reduced IFT due to the surface excessive concentration mechanism. The wettability alteration experiment illustrated that although QS and CTAB compact EDL around oil and matrix particles leading to attraction force augmentation, they both alter wettability through adsorption on matrix and carboxylic groups present in crude oil, *** aqueous solutions were then injected into various clay-rich sandstone sanpacks, which resulted in increased oil recovery. However, the mechanisms leading to enhanced oil recovery variedby surfactant type. CTAB increased recovery by 10% through IFT reduction and wettability alteration, while SDS and TX increased recovery by 12% and 9%, respectively, through wettability alteration and extreme fine migration. In contrast, partial fine migration in the QS flooding experiment reached a recovery increase of 18%. Permeability trends through experiments were also recorded. During CTAB injection,permeability did not reduce, while QS aqueous solution reduced rock permeability to 5 m D. SDS and TX reduced the magnitude of permeability to 2 m *** conclusion, this study demonstrates that surfactants can effectively improve oil recovery in clay-rich sandstones by altering the interparticle forces, reducing IFT, a

关键词： Surfactant flooding Smart water Fine migration Recovery factor

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Fractures interaction and propagation mechanism of multi-cluster fracturing on laminated shale oil reservoir

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petroleum Science 2024年第4期21卷 2600-2613页

作者： Jia-Xin Lv Bing Hou Key Laboratory of petroleum engineering Ministry of Education China University of Petroleum (Beijing) State Key Laboratory of petroleum Resources and engineering China University of Petroleum (Beijing) department of petroleum engineering China University of Petroleum (Beijing) at Karamay

The continental shale reservoirs of Jurassic Lianggaoshan Formation in Sichuan Basin contain thin lamina, which is characterized by strong plasticity and developed longitudinal shell limestone *** improve the production efficiency of reservoirs by multi-cluster fracturing, it is necessary to consider the unbalanced propagation of hydraulic fractures and the penetration effect of fractures. This paper constructed a numerical model of multi-fracture propagation and penetration based on the finite element coupling cohesive zone method; considering the construction cluster spacing, pump rate,lamina strength and other parameters studied the influencing factors of multi-cluster fracture interaction propagation; combined with AE energy data and fracture mode reconstruction method, quantitatively characterized the comprehensive impact of the strength of thin interlayer rock interfaces on the initiation and propagation of fractures that penetrate layers, and accurately predicted the propagation pattern of hydraulic fractures through laminated shale oil reservoirs. Simulation results revealed that in the process of multi-cluster fracturing, the proportion of shear damage is low, and mainly occurs in bedding fractures activated by outer fractures. Reducing the cluster spacing enhances the fracture system's penetration ability, though it lowers the activation efficiency of lamina. The high plasticity of the limestone interlayer may impact the vertical propagation distance of the main fracture. Improving the interface strength is beneficial to the reconstruction of the fracture height, but the interface communication effect is limited. Reasonable selection of layers with moderate lamina strength for fracturing stimulation, increasing the pump rate during fracturing and setting the cluster spacing reasonably are beneficial to improve the effect of reservoir stimulation.

关键词： Laminated shale Multi-cluster fracturing Cross-layer Cohesive zone model Acoustic emission technique

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Pore-scale study of the effects of DTPA chelating agent flooding on oil recovery utilizing a clay-coated micromodel

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petroleum Research 2024年第2期9卷 228-237页

作者： Hojjat Mohammadzadeh Jamshid Moghadasi Khalil Shahbazi Shahin Kord department of petroleum engineering Ahwaz Faculty of Petroleum EngineeringPetroleum University of TechnologyAhwazIran

The use of diethylenetriaminepentaacetic acid(DTPA)chelating agent has shown promising results for enhanced oil recovery(EOR)in prior *** mechanisms,mainly resulting from rock-fluid interaction,have been proposed for chelating agent flooding;however,little attention has been paid to fluid-fluid interaction thus *** assessment of these mechanisms has primarily relied on macroscopic techniques such as core *** paper aims to investigate the injection of DTPA brine and its dominant mechanisms at the pore scale using a clay-coated *** micromodel tests were performed under oil-wet and water-wet *** a more precise examination of fluid/fluid interactions,the dynamic interfacial tension(IFT)and Zeta potential were *** was observed that the injection of DTPA brine in water-wet state changed the saturation distribution and increased oil *** on visual inspections,this change in saturation distribution could potentially be linked to the formation of micro-dispersions and viscoelastic interfacial ***-dispersions facilitate flow to unswept areas,and viscoelastic interface formation reshapes the interface between oil and brine,causing disconnected oil droplets to coalesce and thus increase *** the oil-wet state,the micro-dispersion formation and wettability alteration can be the dominant mechanisms,and the amount of recovered oil was higher than that observed in the water-wet ***,Zeta potential measurements at the interface between brine and oil showed a more negative value for DTPA brine,which is effective in wettability alteration and micro-dispersions *** results indicate that IFT reduction was not significant enough to be considered the dominant mechanism,although it assists in DTPA brine penetration into the crude oil and subsequent micro-dispersion formation.

关键词： Enhanced oil recovery technique Chelating agent Micromodel Fluid/fluid interaction Micro-dispersions Viscoelastic interface

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Rock physical characteristics of deep dolomite under complex geological conditions: A case study of 4th Member of Sinian Dengying Formation in the Sichuan Basin, China

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petroleum Science 2024年第4期21卷 2370-2382页

作者： Chuang Li Shu-Xin Pan Hong-Bin Wang Ji-Xin Deng Jian-Guo Zhao Zhi Li Yu Zhang Northwest Branch of Research Institute of petroleum Exploration & Development department of Geophysics and Exploration College of Geophysics Chengdu University of Technology State Key Laboratory of petroleum Resources and engineering China University of Petroleum (Beijing)

The deep-ultra deep carbonate reservoir in China, commonly subjected to modification of multi-stage diagenesis, has extremely high heterogeneity. Conventional rock physics analysis cannot accurately identify the elastic responses of reservoir. Here, the rock physics properties of the dolomite from the 4th Member of the Sinian Dengying Formation are experimentally measured, and the change law of rock physics characteristics is investigated within the framework of the diagenetic processes by the analysis of the elastic and petrologic characteristics, pore structure, and sedimentary environments. The results show that the differentiated diagenesis results in different pore structure characteristics and microtexture characteristics of the rock. The microbial dolomite of the algal mound-grain beach facies is subjected to the contemporaneous microbial dolomitization and seepage-reflux dolomitization, penecontemporaneous selective dissolution, burial dolomitization, and hydrothermal dolomitization. The resultant crystalline dolomite is found with one main type of the dolomite crystal contact boundaries,and the dissolution pore is extensive development. The siliceous, muddy, and limy dolomite of the interbeach sea environment mainly experiences the weak capillary concentration dolomitization, intensive mechanical compaction-induced densification, and burial dolomitization. Such crystalline dolomite is observed with four types of contact boundaries, namely the dolomite contact, clay contact, quartz contact, and calcite contact boundaries, and porosity mostly attributed to residual primary inter-granular or crystalline pores. The samples with the same crystal boundary condition have consistent correlations between the compressional-and shear-wave velocities, and between the compressional-wave velocity and the velocity ratio. Additionally, the variation of the acoustic velocity with effective pressure and the intensity of pore-scale fluid-related dispersion are controlled by t

关键词： Deep-ultra deep carbonate reservoirs Rock physics properties Dolomite Seismic elastic properties Micro-crack Pore structure types

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Study of deep transportation and plugging performance of deformable gel particles in porous media

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petroleum Science 2024年第2期21卷 962-973页

作者： Wen-Jing Zhao Jing Wang Zhong-Yang Qi Hui-Qing Liu National Key Laboratory of petroleum Resources and engineering China University of PetroleumBeijing102249China MOE Key Laboratory of petroleum engineering China University of PetroleumBeijing102249China

Deformable gel particles(DGPs) possess the capability of deep profile control and flooding. However, the deep migration behavior and plugging mechanism along their path remain unclear. Breakage, an inevitable phenomenon during particle migration, significantly impacts the deep plugging effect. Due to the complexity of the process, few studies have been conducted on this subject. In this paper, we conducted DGP flow experiments using a physical model of a multi-point sandpack under various injection rates and particle sizes. Particle size and concentration tests were performed at each measurement point to investigate the transportation behavior of particles in the deep part of the reservoir. The residual resistance coefficient and concentration changes along the porous media were combined to analyze the plugging performance of DGPs. Furthermore, the particle breakage along their path was revealed by analyzing the changes in particle size along the way. A mathematical model of breakage and concentration changes along the path was established. The results showed that the passage after breakage is a significant migration behavior of particles in porous media. The particles were reduced to less than half of their initial size at the front of the porous media. Breakage is an essential reason for the continuous decreases in particle concentration, size, and residual resistance coefficient. However, the particles can remain in porous media after breakage and play a significant role in deep plugging. Higher injection rates or larger particle sizes resulted in faster breakage along the injection direction, higher degrees of breakage, and faster decreases in residual resistance coefficient along the path. These conditions also led to a weaker deep plugging ability. Smaller particles were more evenly retained along the path, but more particles flowed out of the porous media, resulting in a poor deep plugging effect. The particle size is a function of particle size before inject

关键词： Physical simulation Deformable gel particle Breakage Particle size Residual resistance coefficient

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A contrasting analysis of CO_(2) and N_(2) foam flood for enhanced oil recovery and geological storage of CO_(2)

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petroleum Research 2024年第1期9卷 55-60页

作者： Alireza Roozbahani Farshad Soofivan Ali Sagban Hassoon Al-Tameemi Hadi Abdollahi Sogand Saatchi Abdolhamid Ansari petroleum engineering department Faculty of Chemical EngineeringTarbiat Modares UniversityTehranIran School of Chemical and petroleum engineering Shiraz UniversityShirazIran School of Chemical and petroleum engineering Shiraz BranchIslamic Azad UniversityShirazIran department of petroleum engineering Science and Research BranchAzad UniversityTehranIran department of Chemistry and Chemical engineering Rasht BranchIslamic Azad UniversityRashtIran department of petroleum engineering Lamerd BranchIslamic Azad UniversityLamerdIran

Foam flooding using CO_(2)has emerged as a promising method for both enhanced oil recovery(EOR)and the storage of CO_(2)in geological *** study conducts a thorough analysis of the behavior of CO_(2)and N_(2)foams in bulk and porous media,utilizing bubble-scale analyses and foam flooding *** study compares the foamability and longevity of CO_(2)and N_(2)foams,with findings indicating that N_(2)foam bubbles tend to be smaller and less varied in size than CO_(2)foam bubbles,leading to increased foam ***,the study compares the half-lives of CO_(2)and N_(2)foams generated through sparging and winding methods,showing that N_(2)foam has half-lives 22 and 10 times greater than CO_(2)foam when produced using the sparging and winding methods,***,CO_(2)foam generated through the sparging method had a lower foaming volume than N_(2)foam due to CO_(2)'s *** the foam flooding experiments,N_(2)foam proved more effective in recovering oil from porous media than CO_(2)foam,thus demonstrating the effectiveness of the foam injection *** results offer valuable insights into the differing performance of N_(2)and CO_(2)foam floods for EOR and CO_(2)geological storage.

关键词： CO_(2) storage Foam flood Enhanced oil recovery N_(2) foam CO_(2) foam

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