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Contact Resistance and Arc Erosion of Tungsten-copper Contacts in Direct Currents

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Journal of Wuhan University of technology(Materials Science) 2017年第4期32卷 816-822页

作者：马窦琴 XIE Jingpei LI Jiwen WANG Aiqin WANG Wenyan School of Materials Science and Engineering Henan University of Science and Technology Luoyang 471023 China non-ferrous metal generic technology collaborative innovation center of henan Province Luoyang 471023 China

The arc erosion under medium direct currents in the argon flow was tested on tungsten-copper（W-Cu） contacts which were processed by hot extrusion and heat treatment. The scanning electron microscopy（SEM） and transmission electron microscopy（TEM） were used to study the microstructure of the W-Cu powders and compacts. The contact resistance, arcing energy, and arcing time were continuously measured by JF04C contact materials test system. Changes in tungsten-copper contact surface were observed by SEM. The test results showed that the arcing time and arcing energy all increase with current and voltage, but the changes of average contact resistance are more complicated. For a short arcing time, the average contact resistance decreases with increasing current due to the vaporization of Cu. However, for a longer arcing time, it slightly increases due to the formation of high resistant films, compound copper tungsten. The formation of compound copper tungsten was confirmed by the increased Rc kept in the range from 1.1 to 1.6 mΩ. The compound copper tungsten is first exposed with a tungsten and copper-rich surface, and then totally exposed due to evaporation of copper from the surface. At last a stabilized surface is created and the crystals decrease from 8 μm to 2 μm caused by the arc erosion.

关键词： Tungsten-copper contacts arc erosion contact resistance surface analysis

Microstructure Evolution and Microhardness of Ultrafine-grained High Carbon Steel during Multiple Laser Shock Processing

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Journal of Iron and Steel Research International 2015年第1期22卷 55-59页

作者： Yi XIONG Tian-tian HE Feng-zhang REN Peng-yan LI Lu-fei CHEN Alex A.VOLINSKY School of Materials Science and Engineering Henan University of Science and Technology henan collaborative innovation center of non-ferrous metal generic technology Institute of metal Research Chinese Academy of Sciences Department of Mechanical Engineering University of South FloridaTampa FL 33620USA

Surface microstructure and microhardness of （ferrite＋ cementite） microduplex structure of the ultrafine- grained high carbon steel after laser shock processing （LSP） with different impact times were investigated by means of scanning electron microscopy （SEM）, transmission electron microscopy （TEM）, X-ray diffraction （XRD） and microhardness measurements. Equiaxed ferrite grains were refined from 400 to 150 nm, and the cementite lamellae were fully spheroidized, with a decrease of the particle diameter from 150 to 100 nm as the impact times increased. The cementite dissolution was enhanced significantly. Correspondingly, the lattice parameter of α-Fe and microhard- hess increased with the impact times.

关键词： ultrafine-grained high carbon steel laser shock processing impact times microstructure microhardness

In-situ polymerized PEO-based solid electrolytes contribute better Li metal batteries:Challenges,strategies,and perspectives

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Journal of Energy Chemistry 2024年第5期92卷 548-571页

作者： Zhihui Jia Yong Liu Haoming Li Yi Xiong Yingjie Miao Zhongxiu Liu Fengzhang Ren School of Materials Science and Engineering Henan Key Laboratory of Non-Ferrous Materials Science&Processing TechnologyHenan University of Science and TechnologyLuoyang 471023HenanChina Provincial and Ministerial Co-construction of collaborative innovation center for non-ferrous metal new Materials and Advanced Processing technology Henan University of Science and TechnologyLuoyang 471023HenanChina

Polyethylene oxide(PEO)-based solid polymer electrolytes(SPEs)with good electrochemical stability and excellent Li salt solubility are considered as one of the most promising SPEs for solid-state lithium metal batteries(SSLMBs).However,PEO-based SPEs suffer from low ionic conductivity at room temperature and high interfacial resistance with the electrodes due to poor interfacial contact,seriously hindering their practical *** an emerging technology,in-situ polymerization process has been widely used in PEO-based SPEs because it can effectively increase Li-ion transport at the interface and improve the interfacial contact between the electrolyte and ***,we review recent advances in design and fabrication of in-situ polymerized PEO-based SPEs to realize enhanced performance in *** merits and current challenges of various SPEs,as well as their stabilizing strategies are ***,various in-situ polymerization methods(such as free radical polymerization,cationic polymerization,anionic polymerization)for the preparation of PEO-based SPEs are *** addition,the application of in-situ polymerization technology in PEO-based SPEs for adjustment of the functional units and addition of different functional filler materials was systematically discussed to explore the design concepts,methods and working ***,the challenges and future prospects of in-situ polymerized PEO-based SPEs for SSLMBs are also proposed.

关键词： In-situ polymerization Polyethylene oxide Solid polymer electrolytes Lithium metal anodes

Structure and Optical Properties of ZnO Thin Films Prepared by the Czochralski Method

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Journal of Wuhan University of technology(Materials Science) 2022年第5期37卷 823-828页

作者： MA Zhanhong REN Fengzhang YANG Zhouya School of Materials Science and Engineering Henan University of Science and TechnologyLuoyang471023China Provincial and Ministerial Co-construction of collaborative innovation center for non-ferrous metal New Materials and Advanced Processing technology Luoyang471023China

The zinc oxide seed film was coated on conductive glass (FTO) substrate by the Czochralski method,Zinc acetate and hexamethylenetetramine were used as raw materials to prepare growth solution,and then ZnO film was prepared by a low-temperature solution *** effects of annealing temperature on the morphology,structure,stress and optical properties of ZnO films were *** thin films were characterized by X-ray diffraction (XRD),scanning electron microscopy (SEM),UV-visible absorption spectra (UV-vis),photoluminescence (PL) and X-ray photoelectron spectroscopy (XPS).The results show that the films are ZnO *** the increase of annealing temperature,the diameter of the rod increases,and the nanorods tend to be *** band gap of the sample obtained from the light absorption spectra first increases and then decreases with the increase of annealing *** the annealing temperature is 350 ℃,the crystallinity of zinc oxide film is the highest,the band gap is close to the theoretical value of pure ZnO.

关键词： Czochralski method ZnO film annealing temperature optical properties micro-morphology internal stress

Hot Compressive Deformation Characteristics of Al-9.3Zn-2.4Mg-1.1Cu Alloy

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Journal of Wuhan University of technology(Materials Science) 2024年第3期39卷 754-765页

作者：刘鹏茹郝世明 XIE Jingpei School of Physics and Engineering Henan University of Science and TechnologyLuoyang 471023China School of Materials Science and Engineering Henan University of Science and TechnologyLuoyang 471023China Provincial and Ministerial Co-Construction of collaborative innovation center for non-ferrous metal New Materials and Advanced Processing technology Luoyang 471023China

To understand the hot compression deformation characteristics of the self-developed Al-9.3Zn-2.4Mg^(-1).1Cu alloy,the hot compression tests of Al-9.3Zn-2.4Mg^(-1).1Cu alloy were investigated by Gleeble 1500 thermo-mechanical simulator to determine the best hot processing *** hot deformation temperatures were 300,350,400,and 450℃,and the strain rates were 1,0.1,0.01,and 0.003 s^(-1),*** on the experimental results,the constitutive equation and hot processing maps are established,and the corresponding strain rate and temperature-sensitive index are *** results show that Al-9.3Zn-2.4Mg^(-1).1Cu alloy has a dynamic softening trend and high strain rate sensitivity during the isothermal compression *** hot deformation behavior can be described by an Arrhenius-type equation after strain *** temperature has a negligible effect on the hot processing properties,while a low strain rate is favorable for the hot working of *** processing maps and microstructure show that the optimal processing conditions were in the temperature range of 400-450℃and strain rate range of 0.003-0.005 s^(-1).

关键词： Al-Zn-Mg-Cu alloy hot working hot deformation behavior constitutive equations processing maps

Effect of annealing time on microstructure and mechanical properties of cryorolled AISI 310S stainless steel

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Journal of Iron and Steel Research International 2023年第3期30卷 548-556页

作者： Xue-kui Lian Yong Li Yi Xiong Yong-li Wu Shun Han Tian-tian He Chun-xu Wang Feng-zhang Ren Central Iron and Steel Research Institute Co. Ltd.Beijing 100081China School of Materials Science and Engineering Henan University of Science and TechnologyLuoyang 471023HenanChina Provincial and Ministerial Co-construction of collaborative innovation center for non-ferrous metal New Materials and Advanced Processing technology Luoyang 471023HenanChina

AISI 310S stable austenitic stainless steel was subjected to 90%cryorolling and then annealed at 800 ℃ for 2-60 *** effect of annealing time on the microstructure and mechanical properties was studied by optical microscopy,scanning electron microscopy,transmission electron microscopy,microhardness and tensile *** results show that the grain size of AISI 310S stainless steel is refined to the nanometer level after 90%cryorolling,and the grain size is approximately 20 *** the increase in annealing time,the degree of grain recrystallization occurs more fully and completely,as the grain begins to grow and then tends to *** strength and hardness of the annealed specimens decrease with increasing annealing time,while elongation tends to *** the annealing time is 10 min,the yield strength increases by about 2 times compared to that of the original austenite(unrolled),and the elongation is also above 20%,which is the best preparation process for ultra-fine grain austenitic stainless steel under this experimental *** the annealing time treatment increases,the fracture morphology changes from mixed quasi-cleavage and ductile fracture(after cryorolling)to ductile fracture(after annealing).

关键词： Austenitic stainless steel Cryorolling Annealing time Microstructure Mechanical property

Novel synthesis of CuW composite reinforced with lamellar precipitates via aluminothermic reduction

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Rare metals 2022年第12期41卷 4047-4054页

作者： Chu Cheng Zi-Wei Song Ling-Feng Wang Ke-Xing Song Tao Huang Long Zhao Li-Sha Wang Zhi-He Dou Ting-An Zhang School of Materials Science and Engineering Henan University of Science and TechnologyLuoyang 471023China Provincial and Ministerial Co-Construction of collaborative innovation center for non-ferrous metal New Materials and Advanced Processing technology Luoyang 471023China henan Key Laboratory of non-ferrous Materials Science&Processing technology Henan University of Science and TechnologyLuoyang 471003China henan Academy of Sciences Zhengzhou 450002China Key Laboratory of Ecological Utilization of Multi-metal Intergrown Ores of Ministry of Education Northeastern UniversityShenyang 110819China

The in situ synthesized reinforced phases in the matrix have the advantages of uniform dispersion and good interfacial *** at in situ synthesizing reinforced phases in CuW composite,a novel methodology for direct synthetization of CuW composite reinforced with lamellar precipitates by aluminothermic reduction is proposed,and CuW composites and their slags were systematically *** results indicate that,at temperatures of above 1800 K,the mole percentage of Al,copper oxides,tungsten oxide,and CuO·Al_(2)O_(3)increased rapidly with temperature increasing,which was not conducive to CuO and W0_(3)thermite reduction.

关键词： composite composites synthesis

Enhanced magnetic properties of SmCo/FeCo nanocomposite magnets by doping eutectic Sm-Ni alloy

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Rare metals 2023年第6期42卷 1829-1835页

作者： Shi-Zhong An Xiao-Sen Li Wu-Hui Li Gui-Hong Lv Feng-Zhang Ren School of Materials Science and Engineering Henan University of Science and TechnologyLuoyang471023China henan Key Laboratory of nonferrous Materials Science and Processing technology Longmen LaboratoryProvincial and Ministerial Co-Construction of Collaborative Innovation Center for Non-Ferrous Metal New Materials and Advanced Processing TechnologyLuoyang471023China

In this work,we prepared SmCo/FeCo nanocomposite magnets with an enhanced magnetic performance by doping eutectic Sm-Ni *** magnets without Sm-Ni alloy,with a grain size of 5-12 nm and an average size of~ 9 nm,are composed of Sm_(2)Co_(17) phase and FeCo phase,leading to a relatively low remanence of 0.0365A·m^(2)·g^(-1) and coercivity of 0.15 T,*** doping 2.5 wt% Sm-Ni alloy,there is no obvious change on the grain size of SmCo/FeCo magnets.

关键词： magnets doping SmCo

Urea-induced interfacial engineering enabling highly reversible aqueous zinc-ion battery

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Rare metals 2024年第4期43卷 1599-1609页

作者： Bin-Rui Xu Quan-An Li Yong Liu Guang-Bin Wang Zi-He Zhang Feng-Zhang Ren School of Material Science and Engineering Henan University of Science and TechnologyLuoyang471023China School of Information Engineering Henan University of Science and TechnologyLuoyang471023China Longmen Laboratory Luoyang471023China Provincial and Ministerial Co-Construction of collaborative innovation center for non-ferrous metal New Materials and Advanced Processing technology Luoyang471023China

Aqueous zinc-ion batteries(AZIBs)have been regarded as prospective rechargeable energy storage devices because of the high theoretical capacity and low redox potential of Zn ***,the uncontrollable formation of dendrites and the water-induced side reactions at the Zn/electrolyte interface,and the poor reversibility under a high current density(>2 mA·cm^(-2))and large area capacity(>2 mAh·cm^(-2))still limit the practical applications of ***,a strategy that can overcome these difficulties is urgently ***,we introduce an environmentally friendly and low-cost additive,namely urea,to the electrolyte of AZIBs to induce uniform Zn deposition and suppress the side *** of the adsorption behavior,electrochemical characterization,and observations of the morphology revealed the interfacial modification induced by urea on the Zn/electrolyte interface,demonstrating its huge potential in ***,the long-term cycling stability(over2100 h)of a Zn/Zn symmetric cell under a high current density of 5 mA·cm^(-2)and a capacity of 5 mAh·cm^(-2)was achieved with a 1 mol·L^(-1)ZnSO_(4)electrolyte with the urea ***,the assembled Zn/NH_4V_4O_(10)full cell with urea exhibited excellent cycling performance and an outstanding average Coulombic efficiency of 99.98%.These results indicate that this is a low-cost and effective additive strategy for realizing highly reversible AZIBs.

关键词： Zn anode Urea additive Interface engineering Dendrite growth Side reaction