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Experimental study of the influencing factors and mechanisms of the pressure-reduction and augmented injection effect by nanoparticles in ultra-low permeability reservoirs

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Petroleum Science 2024年第3期21卷 1915-1927页

作者： Pan Wang Yu-Hang Hu Liao-Yuan Zhang Yong Meng Zhen-Fu Ma Tian-Ru Wang Zi-Lin Zhang Ji-Chao Fang Xiao-Qiang Liu Qing You Yan Zhang Beijing Key Laboratory of Unconventional Natural Gas Geological Evaluation and Development engineering China University of Geosciences (Beijing) School of Energy Resources China University of Geosciences (Beijing) Petroleum engineering technology Research Institute Sinopec Shengli Oilfield Company Hekou oil production plant Sinopec Shengli Oilfield Company Petroleum Exploration and production Research Institute SINOPEC CNPC engineering technology R&D Company Limited

Nanoparticles(NPs) have gained significant attention as a functional material due to their ability to effectively enhance pressure reduction in injection processes in ultra-low permeability reservoirs. NPs are typically studied in controlled laboratory conditions, and their behavior in real-world, complex environments such as ultra-low permeability reservoirs, is not well understood due to the limited scope of their applications. This study investigates the efficacy and underlying mechanisms of NPs in decreasing injection pressure under various injection conditions(25—85°C, 10—25 MPa). The results reveal that under optimal injection conditions, NPs effectively reduce injection pressure by a maximum of 22.77% in core experiment. The pressure reduction rate is found to be positively correlated with oil saturation and permeability, and negatively correlated with temperature and salinity. Furthermore, particle image velocimetry(PIV) experiments(25°C, atmospheric pressure) indicate that the pressure reduction is achieved by NPs through the reduction of wall shear resistance and wettability change. This work has important implications for the design of water injection strategies in ultra-low permeability reservoirs.

关键词： Nanoparticle Pressure reduction Augmented injection Ultra-low permeability reservoir

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Productivity Prediction Model of Perforated Horizontal Well Based on Permeability Calculation in Near-Well High Permeability Reservoir Area

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Energy engineering 2024年第1期121卷 59-75页

作者： Shuangshuang Zhang Kangliang Guo Xinchen Gao Haoran Yang Jinfeng Zhang Xing Han College of the Earth Science Yangtze UniversityWuhan430100China PetroChina Changqing oilfield Fifth oil production plant Xi’an710201China Sinopec Jianghan oilfield Information Center Wuhan430100China

To improve the productivity of oil wells,perforation technology is usually used to improve the productivity of horizontal wells in oilfield exploitation.After the perforation operation,the perforation channel around the wellbore will form a near-well high-permeability reservoir area with the penetration depth as the radius,that is,the formation has different permeability characteristics with the perforation depth as the dividing line.Generally,the permeability is measured by the permeability tester,but this approach has a high workload and limited application.In this paper,according to the reservoir characteristics of perforated horizontal wells,the reservoir is divided into two areas:the original reservoir area and the near-well high permeability reservoir area.Based on the theory of seepage mechanics and the formula of open hole productivity,the permeability calculation formula of near-well high permeability reservoir area with perforation parameters is deduced.According to the principle of seepage continuity,the seepage is regarded as the synthesis of two directions:the horizontal plane elliptic seepage field and the vertical plane radial seepage field,and the oil well productivity prediction model of the perforated horizontal well is established by partition.The model comparison demonstrates that the model is reasonable and feasible.To calculate and analyze the effect of oil well production and the law of influencing factors,actual production data of the oilfield are substituted into the oil well productivity formula.It can effectively guide the technical process design and effect prediction of perforated horizontal wells.

关键词： Perforated horizontal well permeability productivity model sensitivity analysis

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Factors Influencing Fracture Propagation in Collaborative Fracturing ofMultiple HorizontalWells

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Energy engineering 2024年第2期121卷 425-437页

作者： Diguang Gong Junbin Chen Cheng Cheng Yuanyuan Kou Shanxi Key Laboratory of Well Stability and Fluid&RockMechanics inoil andGas Reservoirs Xi’an Shiyou UniversityXi’an710065China The Second oil production plant Petro China Changqing Oilfield CompanyQingyang745100China

Horizontal well-stimulation is the key to unconventional resource exploration and development.The development mode of the well plant helps increase the stimulated reservoir volume.Nevertheless,fracture interference between wells reduces the fracturing effect.Here,a 2D hydro-mechanical coupling model describing hydraulic fracture(HF)propagation is established with the extended finite element method,and the effects of several factors on HF propagation during multiple wells fracturing are analyzed.The results show that with an increase in elastic modulus,horizontal principal stress difference and injection fluid displacement,the total fracture area and the reservoir stimulation efficiency are both improved in all three fracturing technologies.After a comparison of the three technologies,the method of improved zipper fracturing is proposed,which avoids mutual interference between HFs,and the reservoir stimulation effect is improved significantly.The study provides guidance for optimizing the fracturing technology of multiple horizontal wells.

关键词： Multi-well fracturing inter-fracture interference hydraulic fracturing hydro-mechanical coupling extended finite element horizontal well

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Effect of nanocomposite pour point depressant EVAL/CNT on flow properties of waxy crude oil

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Petroleum Science 2023年第6期20卷 3807-3818页

作者： Yang Liu Zheng-Nan Sun Sheng-Zhu Ji Yi-Hai Yang Jian-Qi Xu Guo-Lin Jing Provincial Key Laboratory of oil&Gas Chemical technology College of Chemistry&Chemical EngineeringNortheast Petroleum UniversityDaqing163318HeilongjiangChina no.8 oil production plant engineering technology brigade Daqing OilfieldDaqing163514HeilongjiangChina

The nanocomposite EVAL-CNT was produced by chemical grafting in the solution system through the esterification of ethylene-vinyl alcohol copolymer (EVAL) and carboxylated multi-walled carbon nanotubes (O-MWCNT), and its structural properties were characterized. The improvement of the rheological properties of the waxy oil system by the novel pour point depressant was investigated using macroscopic rheological measurements and microscopic observations. The results showed that EVAL-CNT nanocomposite pour point depressant (PPD) could significantly reduce the pour point and improve the low temperature fluidity of crude oil and had better performance than EVAL-GO at the same addition level. The best effect was achieved at the dosing concentration of 400 ppm, which reduced the pour point by 13 ℃ and the low-temperature viscosity by 85.4%. The nanocomposites dispersed in the oil phase influenced the precipitation and crystallization of wax molecules through heterogeneous crystallization templates, which led to the increase of wax crystal size and compact structure and changed the wax crystal morphology, which had a better effect on the rheological properties of waxy oil.

关键词： Pour point depressant Carbon nanotubes Nanocomposites Waxy crude oil Rheological behavior

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An Experimental Study on the Effect of a Nanofluid on oil-Water Relative Permeability

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Fluid Dynamics & Materials Processing 2024年第6期20卷 1265-1277页

作者： Hui Tian Dandan Zhao Yannan Wu Xingyu Yi Jun Ma Xiang Zhou Baikouquan oil production plant PetroChina Xinjiang Oilfield CompanyKaramay834000China Research Institute of Petroleum Exploration Development PetroChina Liaohe OilfieldPanjin124010China Petroleum engineering School Southwest Petroleum UniversityChengdu610500China oil and Gas Development Haosheng Xincheng Energy TechnologyLtd.of SicuanChengdu610213China

The low porosity and low permeability of tight oil reservoirs call for improvements in the current technologies for oil recovery.Traditional chemical solutions with large molecular size cannot effectively flow through the nanopores of the reservoir.In this study,the feasibility of Nanofluids has been investigated using a high pressure high temperature core-holder and nuclear magnetic resonance(NMR).The results of the experiments indicate that the specified Nanofluids can enhance the tight oil recovery significantly.The water and oil relative permeability curve shifts to the high water saturation side after Nanofluid flooding,thereby demonstrating an increase in the water wettability of the core.In the Nanofluid flooding process the oil recovery was enhanced by 15.1%,compared to waterflooding stage.The T2 spectra using the NMR show that after Nanofluid flooding,a 7.18%increment in oil recovery factor was gained in the small pores,a 4.9%increase in the middle pores,and a 0.29%increase in the large pores.These results confirm that the Nanofluids can improve the flow state in micro-sized pores inside the core and increase the ultimate oil recovery factor.

关键词： Tight oil reservoir nanofluid relative permeability nuclear magnetic resonance T2 spectrum

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A review of SAGD technology development and its possible application potential on thin-layer super-heavy oil reservoirs

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Geoscience Frontiers 2022年第4期13卷 1-10页

作者： Guodong Cui Ting Liu Jingyu Xie Guanghui Rong Lihong Yang Faculty of engineering China University of GeosciencesWuhan 430074China The 2th oil production plant of PetroChina Changqing oilfield Company Qingyang 710021China School of Resources and Geosciences China University of Mining and TechnologyXuzhou 221116China The 12th oil production plant of PetroChina Changqing oilfield Company Xi’an 710000China Sinopec Petroleum Exploration and production Research Institute Beijing 100083China

Super-heavy oil is a significant unconventional energy source,and more than 30 years of research have shown that steam-assisted gravity drainage(SAGD)technology is suitable for thick super-heavy oil reservoirs.Recently,more and more thin-layer super-heavy oil reservoirs have been discovered in China,while their deep buried depth and serous heterogeneity make the existing SAGD technology difficult to apply,so it is urgent to improve the existing SAGD technology for the thin-layer super-heavy oil.To this end,this paper focuses on the enlightenment of field application in SAGD technology.Firstly,based on typical SAGD field projects,the development history of SAGD technology in the world was reviewed,and the influence of reservoir physical properties on the application of SAGD technology in thin-layer superheavy oil reservoirs was analyzed.Secondly,the well pattern,wellbore structure,pre-heating,artificial lift,and monitor technique of SAGD were detailed described,and their adjustment direction was expounded for the development of thin-layer super-heavy oil reservoirs.Lastly,the gas-and solventassistant SAGD were comprehensively evaluated,and their application potential in thin-layer superheavy oil reservoirs was studied.The research results can provide theoretical guidance for the application of SAGD technology in thin-layer super-heavy oil reservoirs.

关键词： SAGD Thin-layer super-heavy oil Development technology Multimedia assisted SAGD

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Copper ions-me diate d dynamic re dox-responsive microgels synergize with silicone for efficient and sustainable antibacterial properties

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Journal of Materials Science & technology 2023年第12期143卷 253-267页

作者： Huali Li Liuqin Zhang Xiaohu Zhang Shuwen Luo Baoshan Yang Min Wu Wei-Hua Li Fa-Qian Liu School of Chemical engineering and technology Sun Yat-sen UniversityZhuhai 519082China School of Materials Science and engineering Sun Yat-sen UniversityGuangzhou 510275China Offshore oil production plant of Sinopec Shengli oilfield Company Dongying 257237China

The antifouling of marine facilities placed below the waterline is a key constraint to the development of the marine economy.Currently,commercial Cu_(2)O-based antifouling coatings still have defects such as agglomeration,oxidation,short duration and high dosage.For this reason,we developed for the first time a triple antifouling system consisting of Cu_(2)O@poly(NIPAM-co-DAm)(Cu_(2)O@PND)dynamic redox micro-gels triggered by copper ions and polydimethylsiloxane(PDMS).The catechol groups of PND nanogels can chelate Cu^(2+)and reduce it in situ to obtain Cu_(2)O@PND microgels,which guarantees the stable release of Cu^(+).Furthermore,Cu_(2)O remains stable and free from oxidation because of the electron transfer between PND and Cu^(2+).Finally,superior antifouling performance was achieved by combining the stable Cu^(+)re-leased from Cu_(2)O,in situ conversion of PND to hydrogel,and its oxidation to produce active substances and H_(2)O_(2),and PDMS coating with low surface energy.

关键词： Hydrogel Copper ions Dynamic redox Silicone Efficient-sustainable release Antibacterial

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Quantitative investigation of nanofluid imbibition in tight oil reservoirs based on NMR technique

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Petroleum Science 2022年第5期19卷 2185-2198页

作者： Tian-Tian Zhang Zhi-Ping Li Caspar Daniel Adenutsi Yong-Zhou Wei Zhen-Fu Ma Qing You School of Energy Resources China University of GeosciencesBeijing10083China Beijing Key Laboratory of Unconventional Natural Gas Geological Evaluation and Development engineering Beijing10083China Core and Rock Properties Laboratory Department of Petroleum EngineeringFaculty of Civil and Geo-EngineeringKwame Nkrumah University of Science and TechnologyKumasiGhana Binnan oil production plant Shengli Oilfield CompanySINOPECBinzhou256606ShandongChina Hekou oil production plant Shengli Oilfield CompanySINOPECDongying257200ShandongChina

Nanofluids have been effective chemical additives for enhanced oil recovery(EOR)in tight oil reservoirs due to their special properties.However,oil imbibition recoveries vary for different nanofluids.The oil/water distribution in rocks during imbibition using various nanofluids was less discussed in previous studies.In this study,we systematically examined the imbibition efficiencies of various nanofluids at60℃.Furthermore,the migration of nanofluids and oil distribution in the rock pores were monitored using nuclear magnetic resonance(NMR).The nanofluids were prepared by dispersing silica nanoparticles and five different types of surfactants i.e.,anionic-nonionic,anionic,nonionic,amphoteric and cationic surfactants in deionized(DI)water.Subsequently,interfacial tension(IFT)and contact angle measurements were conducted to reveal the underlying EOR mechanisms of various nanofluids.The experimental results showed that the EOR potential of the different types of nanofluids was in the order anionic-nonionic>anionic>nonionic>amphoteric>cationic>brine.Anionic-nonionic(sodium lauryl ether sulfate(SLES))and anionic(sodium dodecyl sulfonate(SDS))nanofluids exhibited excellent capability of wettability alteration,and increased oil recovery by 27.96%and 23.08%,respectively,compared to brine.The NMR results also showed that mesopores(0.1-1μm)were the dominant developed pores in the rocks,and contributed the most to imbibition efficiency.In addition,the imbibition of nanofluids initially took place in mesopores and micropores before moving into macropores.This study provides fundamental information on the selection of nanofluids for EOR in tight oil reservoirs.The study also improved the understanding of oil/water distribution during the imbibition of the proposed nanofluids.

关键词： Nanofluids Spontaneous imbibition Nuclear magnetic resonance(NMR) oil migration Tight oil reservoir

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Modular zonal fluid sampling and pressure testing technology for production well

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Petroleum Exploration and Development 2022年第2期49卷 438-447页

作者： XU Jianguo YANG Qinghai YI Peng HOU Ze JIA Weite FU Tao ZHANG Zonglin YUE Qingfeng Jilin oilfield oil&Gas engineering Research Institute Songyuan 138000China PetroChina Research Institute of Petroleum Exploration&Development Beijing 100083China Jilin oilfield Xinmu production plant Songyuan 138000China Daqing oilfield production engineering Research Institute Daqing 163453China

To accurately obtain development dynamic data such as zonal pressure and fluid parameters of each oil layer in the late development stage of a high water-cut old oilfield, a modular zonal sampling and testing technology with the characteristics of modularization, full electronic control and rapidity was proposed and developed. Lab testing and on-site testing was carried out. The modular zonal sampling and testing system is composed of 10 functional modules, namely ground control system, downhole power supply module, drainage pump, electronically controlled anchor, electronically controlled packer, electronically controlled sampler, magnetic positioning sub, terminal sub, adapter cable, and quick connector. Indoor tests have confirmed that the performance parameters of each module meet the design requirements. The downhole function modules of the system can withstand pressures up to 35 MPa and temperatures up to 85 ℃. The rubber cylinder of the electronically controlled packer can withstand a pressure difference of more than 10 MPa. The electronically controlled anchor has an anchoring force of greater than 6.9 t, and can be forcibly detached in the event of an accident. The discharge pump has a displacement of 0.8 m;/d and a head of 500 m. The electronically controlled sampler can meet the requirement of taking 500 mL of sample in each of the 3 chambers. Field tests in Jilin oilfield show that the system can realize rapid isolation and self-check of isolation of a certain production interval downhole, as well as layer-by layer pressure build-up test. The drainage pump can be used to discharge the mixed liquid between the upper and lower packers and near the wellbore to obtain real fluid samples of the tested formation interval. The data obtained give us better understanding on the pay zones in old oilfields, and provide important basis for development plan adjustment, reservoir stimulation, and EOR measures.

关键词： zonal sampling zonal testing modularization full electronic control rapidity enhanced oil recovery fluid sampling pressure testing

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Facile synthesis of chromium chloride/poly(methyl methacrylate) core/shell nanocapsules by inverse miniemulsion evaporation method and application as delayed crosslinker in secondary oil recovery

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Petroleum Science 2023年第1期20卷 396-406页

作者： Jing-Yang Pu Keith P.Johnston Ping-Keng Wu Muaaz Ahmad Ming-Liang Luo Na Zhang Ju-Tao He School of Petroleum engineering China University of Petroleum(East China)Qingdao266580ShandongChina Key Laboratory of Unconventional oil&Gas Development(China University of Petroleum(East China)) Ministry of EducationQingdao266580ShandongChina Mcketta Department of Chemical engineering The University of Texas at AustinAustinTX78712USA Department of Energy and Mining engineering Shandong University of Science and TechnologyQingdao266590ShandongChina No.7 oil production plant of PetroChina Changqing oilfield Branch Qingyang745100GansuChina

Cr(III)ehydrolyzed polyacrylamide(HPAM)gels have been extensively studied as a promising strategy controlling waste water production for mature oilfields.However,the gelation time of the current technologies is not long enough for in-depth placement.In this study,we report a novel synthesis method to obtain chromium chloride/poly(methyl methacrylate)(PMMA)nanocapsules which can significantly delay the gelation of HPAM through encapsulating the chromium chloride crosslinker.The chromium chloride-loaded nanocapsules(CreNC)are prepared via a facile inverse miniemulsion evaporation method during which the hydrophobic PMMA polymers,pre-dispersed in an organic solvent,were carefully controlled to precipitate onto stable aqueous miniemulsion droplets.The stable aqueous nanodroplets(W)containing Cr(III)are dispersed in a mixture of organic solvent(O1)with PMMA and nonsolvent medium(O2)to prepare an inverse miniemulsion.With the evaporation of the O1,PMMA forms CreNCs around the aqueous droplets.The CreNCs are readily transferred into water from the organic nonsolvent phase.The CreNCs exhibit the tunable size(358-983 nm),Cr loading(7.1%-19.1%),and Cr entrapment efficiency(11.7%-80.2%),with tunable zeta potentials in different PVA solutions.The CreNCs can delay release of Cr(III)and prolong the gelation time of HPAM up to 27 days.

关键词： Nanocapsules Inverse miniemulsion evaporation Chromium chloride crosslinker HPAM gelation Secondary oil recovery

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