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Sequential alkaline-organic acid leaching process to enhance the recovery of rare earth elements from Indonesian coal fly ash

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Journal of Rare Earths 2024年第7期42卷 1366-1374,I0006页

作者： Widya Rosita Indra Perdana I Made Bendiyasa Ferian Anggara Himawan Tri Bayu Murti Petrus Agus Prasetya Isyatun Rodliyah Department of Nuclear Engineering and Engineering Physics Faculty of EngineeringUniversitas Gadjah MadaJl Grafika No.2Yogyakarta55281Indonesia Department of Chemical Engineering Faculty of EngineeringUniversitas Gadjah MadaJl Grafika No.2Yogyakarta55281Indonesia Department of Geological Engineering Faculty of EngineeringUniversitas Gadjah MadaJl Grafika No.2Yogyakarta55281Indonesia Unconventional Geo-resources Research Group Faculty of EngineeringUniversitas Gadjah MadaJl Grafika No.2Yogyakarta55281Indonesia center for testing of Mineral and Coal Tekmira-Directorate General of Mineral and Coal-Ministry of Energy and Mineral Resources Jl.Jend.Sudirman No.623Wr.MuncangKec.Bandung KulonKota BandungJawa Barat40211Indonesia

In this decade,coal fly ash(CFA)is considered a potential secondary source of rare earth elements(REEs).However,most REEs in coal fly ash are encapsulated in aluminosilicate glass,making it challenging to recover them through acid *** this study,a sequential alkaline-organic acid leaching was developed for the recovery of REEs from *** effect of alkaline leaching using NaOH solution on the destructive ability of aluminosilicate glass,as well as the mineralogy and morphology changes of the resulting coal fly ash,was first ***,the effectiveness of alkaline leaching on the recovery ability of REEs through organic acid leaching was *** results show that the maximum leaching efficiency for Si and Al,which was obtained at the optimum alkaline leaching conditions,namely NaOH concentration of 10 mol/L,reaction temperature of 65℃,liquid/solid(L/S)ratio of 10 mL/g,and reaction time of 90 min,is 28%and 32%,*** digestion reaction with NaOH lixiviants also causes coal fly ash to become more porous,making it advantageous in the organic acid-leaching process at the REEs recovery *** utilization of the desilicated residue produced from the digestion process in acid leaching effectively increases the overall REEs recovery from 32.2%to 77.6%.

关键词： Rare earth elements Alkaline Organic acid Coal fly ash

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Multi-field Coupled Inverse Hall–Petch Relations for Ferroelectric Nanocrystals

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Acta Mechanica Solida Sinica 2024年第1期37卷 139-147页

作者： Xiaodong Zhang Wei Yan Xuhui Lou Yujun Chen Zhihong Zhou Qingyuan Wang Lianhua Ma Xiaobao Tian Non-Destructive testing Laboratory School of Quality and Technical SupervisionHebei UniversityBaoding 071002China AVIC Huiyang Aviation Propeller Co. LtdBaoding 071051China Department of Mechanics and Engineering Sichuan UniversityChengdu 610065China Yibin Institute of Industrial Technology Sichuan University Yibin ParkYibin 644000China Research Institute of Interdisciplinary Sciences(RISE) Dongguan University of TechnologyDongguan 523808China School of Materials Science and Engineering Dongguan University of TechnologyDongguan 523808China

Tailoring grain size can improve the strength of polycrystals by regulating the proportion of grains to grain boundaries and the interaction *** the grain size decreases to the nanoscale,the deformation mechanism in polycrystals shifts from being primarily mediated by dislocations to deformation occurring within the grains and grain ***,the mechanism responsible for fine-grain strengthening in ferroelectric materials remains unclear,primarily due to the complex multi-field coupling effect arising from spontaneous *** molecular dynamics simulations,we investigate the strengthening mechanism of barium titanate(BaTiO3),with extremely fine-grain *** material exhibits an inverse Hall–Petch relationship between grain size and strength,rooting in the inhomogeneous concentration of atomic strain and grain ***,we present a theoretical model to predict the transition from the inverse Hall–Petch stage to the Hall–Petch stage based on strength variations with size,which aligns well with the simulation *** has been found that the piezoelectric properties of the BaTiO3 are affected by polarization domain switching at various grain *** study enhances our understanding of the atomic-scale mechanisms that contribute to the performance evolution of fine-grain nano-ferroelectric *** also provides valuable insights into the design of extremely small-scale ferroelectric components.

关键词： Ferroelectrics Multi-field coupling Molecular dynamics Fine-grain reinforcement Inverse Hall-Petch effect

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A Local Tb Theorem for Square Functions and Parabolic Layer Potentials

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数学学报（英文版） 2024年第8期40卷 1941-1966页

作者： Zhi Dan WANG Guo Ming ZHANG School of Physical and Mathematical Sciences Nanjing Tech UniversityNanjing 211816P.R.China Frontiers Science center for Nonlinear Expectations Ministry of EductionResearch Center for Mathematics and Interdisciplinary SciencesShandong UniversityQingdao266237P.R.China

In this paper,we give a locally parabolic version of Tb theorem for a class of vector-valued operators with off-diagonal decay in L2 and certain quasi-orthogonality on a subspace of L2,in which the testing functions themselves are also *** an application,we establish the boundedness of layer potentials related to parabolic operators in divergence form,defined in the upper half-space Rn+2+:={(x,t,λ)∈ Rn+1 ×(0,∞)},with uniformly complex elliptic,L∞,t,λ-independent coefficients,and satisfying the De Giorgi/Nash estimates.

关键词： 35A99 Calderón-Littlewood-Paley family Carleson measure estimates Local Tb theorems Parabolic layer potentials

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Construction and Properties of Simvastatin and Calcium Phosphate Dual-Loaded Coaxial Fibrous Membranes with Osteogenic and Angiogenic Functions

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Journal of Bionic Engineering 2022年第6期19卷 1645-1657页

作者： Chang Liu Dan Deng Jing Gao Shue Jin Yi Zuo Yubao Li Jidong Li Research center for Nano-Biomaterials Analytical&Testing CenterSichuan UniversityChengdu610064China

The ideal Guided Bone Regeneration(GBR)membrane is required to have good biocompatibility,space maintenance ability,appropriate degradation rate,and preferably can guide the regeneration of vascularized bone *** this study,Simvastatin(SIM)and calcium Phosphate(CaP)were encapsulated in a Polycaprolactone(PCL)/Chitosan(CS)core-shell structural fibrous membranes via coaxial electrospinning *** results showed that loaded SIM in the core of the core-shell structure fibrous membranes could sustainably release the drug for more than two months and upregulate the angiogenic marker of Bone Mesenchymal Stem Cells(BMSCs).Adding a certain amount of CaP to the shell layer provided more sites for the mineralization and synergistic with SIM to promote osteogenic differentiation of BMSCs in *** intramuscular implantation experiments in rabbits suggested a normal early inflammation and enhanced vascularization induced by the SIM-loaded fibrous *** study proposed an effective strategy to prepare a dual-loaded core-shell fibrous membrane for guided vascularized bone tissue regeneration.

关键词： Simvastatin Calcium phosphate Coaxial electrospinning Vascularization Guided Bone Regeneration

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Reactivation of hepatitis B virus infection – an important aspect of multifaceted problem

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World Journal of Gastroenterology 2024年第26期30卷 3193-3197页

作者： Sergey Morozov Sergey Batskikh Department of Gastroenterology Hepatology and NutritionFederal Research Center of NutritionBiotechnology and Food SafetyMoscow 115446Russia Department of Hepatology Moscow Clinical Scientific Center N.A.A.S.LoginovMoscow 111123Russia

In this editorial we comment on the article published in the recent issue of the W orld Journal of *** focus specifically on the problem of occult hepatitis B virus(HBV)infection,that is a result of previous hepatitis B(PHB)and a source for reactivation of *** prevalence of PHB is underestimated due to the lack of population testing ***,this condition not only com-plicate anticancer treatment,but may be responsible for the development of other diseases,like cancer or autoimmune *** we unveil possible mecha-nisms responsible for realization of these processes and suggest practical approa-ches for diagnosis and treatment.

关键词： Occult hepatitis B virus infection Hepatitis B virus reactivation Previous hepatitis B Cancer Autoimmune disorders

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Evidence for distortion-induced local electric polarization in α-RuCl

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Science China(Physics,Mechanics & Astronomy) 2024年

作者： Xinrun Mi De Hou Xiao Wang Sabreen Hammouda Caixing Liu Zijian Xiong Han Li Yan Liu Guiwen Wang Aifeng Wang Yisheng Chai Yang Qi Wei Li Xiaoyuan Zhou Yixi Su D.I.Khomskii Mingquan He Zhigao Sheng Young Sun College of Physics Center of Quantum Materials and Devices Chongqing University Anhui Key Laboratory of Condensed Matter Physics at Extreme Conditions High Magnetic Field Laboratory Hefei Institutes of Physical Science Anhui Chinese Academy of Sciences University of Science and Technology of China Jülich Centre for Neutron Scienceat Heinz Maier-Leibnitz Zentrum (JCNS-MLZ) Forschungszentrum Jülich GmbH School of Physics Beihang University Analytical and testing center Chongqing University State Key Laboratory of Surface Physics Department of Physics Fudan University CAS Key Laboratory of Theoretical Physics Institute of Theoretical Physics Chinese Academy of Sciences II.Physikalisches Institut Universit?t zu K?ln

The spin-orbit assisted Mott insulator α-RuCl3is a prime candidate for material realization of the Kitaev quantum spin *** little attention has been paid to charge degrees of freedom, charge effects, such as electric polarization, may arise in this system. Here, we report distortion-induced local electric polarization in α-RuCl3as evidenced by single-crystal X-ray diffraction,second harmonic generation（SHG） and dielectric measurements. The SHG signal appears at room temperature and develops substantially in the Kitaev paramagnetic state when short-range spin correlations come into play. Despite sizable pyroelectric currents in the Kitaev paramagnetic state, the absence of hysteresis in the polarization-electric field（P-E） points to the shortrange nature of electric polarization. This localized electric polarization is likely the result of distortion-induced charge dimerization, achieved through virtual hopping-induced charge redistribution. In addition, the electric polarization is boosted by short-range spin correlations via spin-phonon coupling in the Kitaev paramagnetic state. Our results emphasize the importance of charge degrees of freedom in α-RuCl3, which establish a novel platform to investigate charge effects in Kitaev materials.

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Defects in phospholipase C zeta cause polyspermy and low fertilization after conventional IVF:not just ICSI failure

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Asian Journal of Andrology 2024年第2期26卷 175-182页

作者： Jian-Fang Che Hui-Xia Wu Si-Cong Zeng Yue-Ren Wu Jing Dai De-Hua Cheng Fei Gong Guang-Xiu Lu Ge Lin Can Dai School of Medicine Hunan Normal UniversityChangsha 410013China Reproductive and Genetic Hospital of CITIC-Xiangya Changsha 410008China Clinical Research center for Reproduction and Genetics in Hunan Province Changsha 410078China National Engineering and Research center of Human Stem Cell Changsha 410205China

Phospholipase C zeta(PLC)is a key sperm-borne oocyte-activating factor that triggers Ca^(2+)oscillations and the subsequent block to polyspermy following gamete *** in PLCZ1,the gene encoding PLCζ,cause male infertility and intracytoplasmic sperm injection(ICSI)fertilization failure;and PLCζ expression and localization patterns are significantly correlated with ICSI fertilization rate(FR).However,in conventional in vitro fertilization(cIVF),whether and how sperm PLCζ affects fertilization remain ***,we identified one previously reported and two novel PLCZ1 mutations associated with polyspermy in vitro that are characterized by excessive sperm-zona binding and a delay in pronuclei(PN)*** staining and oocyte activation testing revealed that virtually all spermatozoa from patients lacked functional PLCζ and were thus unable to evoke Ca^(2+) *** with an artificial oocyte activation treatment successfully rescued the polyspermic phenotype and resulted in a live ***,we analyzed PLCζ in an additional 58 males after cIVF treatment in the Reproductive and Genetic Hospital of CiTiC-Xiangya(Changsha,China)between February 2019 and January *** found that the proportion of spermatozoa that expressed PLCζ was positively correlated with both 2PN rate and total *** optimal cutoff value below which males were likely to experience low FR(total FR≤30%)after clVF was 56.7%for the proportion of spermatozoa expressing *** study expands the mutation and the phenotypic spectrum of PLCZ1 and further suggests that PLCζ constitutes a promising biomarker for identifying low FRs cases in cIVF due to sperm-related oocyte activation deficiency and that sperm PLCζ analysis may benefit the widermale population and not onlymen with IcsI failure.

关键词： conventional IVF gene variants PLCζ polyspermy

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Effect of Antibacterial Enoxacin on the Properties of Injectable Nano-hydroxyapatite/Polyurethane Cement for Bone Repairing

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Journal of Bionic Engineering 2022年第2期19卷 483-496页

作者： Jinzheng Zhang Xiaoyu Lei Jiajing Tang Jie Chen Qing Zhao Wei Fang Yinglong Zhang Yubao Li Yi Zuo Research center for Nano-Biomaterials Analytical and Testing CenterSichuan UniversityChengdu 610064People’s Republic of China

Biomaterial-associated infection(BAI)is a kind of serious post-operative complication in orthopaedic ***-loaded bone cement shines a light on BAI prevention for convenient manipulation and complex *** this aim,we designed an antibacterial bone cement based on Nano-hydroxyapatite/Polyurethane(PUHA)loading with antibiotic Enoxacin(EN).The distinct shear-thinning behavior of the prepolymers was observed,indicating a good *** PUHA bone cement possessed a suitable curing speed,and the addition of EN might slightly expedite the curing process and enhance the mechanical *** EN release profile indicated that the EN-loaded bone cement could reach the minimum inhibitory concentration in 2 h,and sustainedly released EN for almost 8 days,exhibiting an antibacterial delivery *** test further confirmed the antibacterial ability of EN-loaded bone cement is in a dose-dependent ***,the osteogenic performance of drug-loaded bone cement with high dosage is not as good as antibacterial *** the EN concentration of antibacterial cement was lower than 32μg·mL^(-1),the proliferation and osteogenic differentiation of rat mesenchymal stem cells could be significantly ***,this study verified the potential of the EN-loaded PUHA bone cement in anti-infection and osteogenesis for bone repairing.

关键词： Antibacterial bone cement Nano-hydroxyapatite/polyurethane Enoxacin Shear-thinning behavior Osteogenesis

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DNA framework signal amplification platform-based highthroughput systemic immune monitoring

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Signal Transduction and Targeted Therapy 2024年第3期9卷 1115-1131页

作者： Ye Chen Xingyu Chen Bowen Zhang Yuxin Zhang Songhang Li Zhiqiang Liu Yang Gao Yuxuan Zhao Lin Yan Yi Li Taoran Tian Yunfeng Lin State Key Laboratory of Oral Diseases National Center for StomatologyNational Clinical Research Center for Oral DiseasesWest China Hospital of StomatologySichuan UniversityChengdu 610041 SichuanPR China Department of Prosthodontics Tianjin Stomatological HospitalSchool of MedicineNankai UniversityTianjin 300041PR China Department of Laboratory Medicine West China HospitalSichuan UniversityChengdu 610041 SichuanPR China Sichuan Provincial Engineering Research center of Oral Biomaterials Chengdu 610041 SichuanChina

Systemic immune monitoring is a crucial clinical tool for disease early diagnosis,prognosis and treatment planning by quantitative analysis of immune ***,conventional immune monitoring using flow cytometry faces huge challenges in large-scale sample testing,especially in mass health screenings,because of time-consuming,technical-sensitive and high-cost ***,the lack of high-performance detection platforms hinders the development of high-throughput immune monitoring *** address this bottleneck,we constructed a generally applicable DNA framework signal amplification platform(DSAP)based on post-systematic evolution of ligands by exponential enrichment and DNA tetrahedral framework-structured probe design to achieve high-sensitive detection for diverse immune cells,including CD4+,CD8+T-lymphocytes,and monocytes(down to 1/100μl).Based on this advanced detection platform,we present a novel high-throughput immune-cell phenotyping system,DSAP,achieving 30-min one-step immune-cell phenotyping without cell washing and subset analysis and showing comparable accuracy with flow cytometry while significantly reducing detection time and *** a proof-of-concept,DSAP demonstrates excellent diagnostic accuracy in immunodeficiency staging for 107 HIV patients(AUC>0.97)within 30 min,which can be applied in HIV infection monitoring and ***,we initially introduced promising DSAP to achieve high-throughput immune monitoring and open robust routes for point-of-care device development.

关键词： diagnosis monitoring initially

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Application Strategies of Shotcrete Anchor Support Technology in Highway Bridge and Tunnel Engineering

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Journal of Architectural Research and Development 2024年第1期8卷 56-61页

作者： Ruiquan Liu China Merchants Chongqing Highway Engineering testing center Co. Ltd.Chongqing 400067China

This article analyzes the application strategies of shotcrete anchor support technology using a highway bridge-tunnel construction project as an *** article covers various strategies,including support plan formulation,mortar shotcrete anchor construction,grid steel frame construction,steel mesh construction,and concrete support *** analysis aims to provide a guideline for those interested in applying this technology and improving the quality and safety of highway bridges and tunnels construction.

关键词： Highway bridge engineering Tunnel construction Shotcrete support Support plan Support construction

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