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Experimental study on wax deposition of highly paraffinic oil in intermittent gas-oil flow in pipelines

Petroleum Science 2024年第3期21卷 2080-2088页

作者： Chuan-Shuo Wang Qian-Li Ma Xiao-Fang Lv Jie Zhang Yang Liu Shi-Dong Zhou Jiangsu Key Laboratory of oil and gas Storage and Transportation Technology Changzhou University Hade oil and gas Development Department Tarim Oilfield Branch

oil-gas two phase wax deposition is a fairly common and open-ended question in flow assurance of multiphase transportation pipelines. This paper investigated the two main aspects of oil-gas two phase wax deposition layer: apparent thickness and crystal structure characteristics. A typical highly paraffinic oil in Bohai Sea, China, was used as the experimental material to investigate the wax deposition thickness in oil-gas two phase under the influence of different oil temperatures, superficial gas/liquid phase velocities and gas-oil ratios by using multiphase flow loop experimental device. Just as in the classical theory of wax molecular diffusion, it showed that wax deposition thickness of oil-gas two phase increased with increasing oil temperature. Analysis of the impact of different superficial phase velocities found that the actual liquid flow heat transfer and shear stripping was the gas phase dominant mechanisms determining wax deposit thickness. In addition, the crystal structure of the wax deposition layer was characterized with the help of small-angle X-ray scattering(SAXS) for different circumferential positions, flow rates and gas-oil ratios. The bottom deposition layer had a complex crystal structure and high hardness, which were subject to change over flow rate variations. Furthermore, the SAXS results provided evidence that the indirect effect of the actual liquid velocity modified by the gas phase was the main mechanism. Our study of the effect of gas phase on the wax deposition of oil-gas two phase will help shed light onto the mechanism by which this important process occurs. Our findings address a very urgent need in the field of wax deposition of highly paraffinic oil to understand the flow security of oilgas two phase that occurs easily in multiphase field pipelines.

关键词： oil-gas two phase Highly paraffinic oil Wax deposition SAXS

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Insights into in-situ imbibition behavior of fracturing fluid in propped shale fractures based on nuclear magnetic resonance:A case study from Longmaxi Formation shale,Sichuan Basin,China

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Petroleum Science 2024年第1期21卷 410-429页

作者： Jing-Jing Guo Kai-Xiang Di Lie-Hui Zhang Yu-Long Zhao Hui-Ying Tang Rui-Han Zhang Ye Tian national Key Laboratory of oil and gas Reservoir Geology and Exploitation Southwest Petroleum UniversityChengdu610500SichuanChina

Shale gas is an important component of unconventional oil and gas *** the imbibition behavior is helpful to optimize flowback parameters and enhance gas *** imbibition studies have focused on shale matrix,and the pressure conditions discussed were mostly *** initial imbibition behavior begins from propped fractures to matrix,but there are few studies working on explaining the imbibition behavior in propped fractures or the phenomenon of many shale wells exhibit higher productivity after a“soaking”***,propped fracture samples were designed for imbibition and migration *** order to accurately study the mechanism and main influencing factors of fracturing fluid imbibition and migration in propped and unpropped shale fractures under high temperature and high pressure,a series of experiments based on nuclear magnetic resonance(NMR)were carried *** showed that NMR T_(2) spectra of all samples exhibited a bimodal *** final imbibition volume of fracturing fluid was positively related to pressure and fracture *** imbibition effect of fracturing fluid was more evident in matrix pores under high *** the migration during soaking stage,the fracturing fluid gradually migrated from large pores to small pores and gradually displaced the shale gas from the matrix,thus allowing the water blocking in propped fractures to self-unlock to some *** permeability decreased in the imbibition stage,while it recovered in the migration stage to some extent.

关键词： Forced imbibition Migration Soaking NMR T_(2)spectra Propped fracture Permeability recovery

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Probabilistic seismic inversion based on physics-guided deep mixture density network

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Petroleum Science 2024年第3期21卷 1611-1631页

作者： Qian-Hao Sun Zhao-Yun Zong Xin Li national Key Laboratory of Deep oil and gas China University of Petroleum(East China) Laoshan Laboratory CNOOC Research Institute Ltd.

Deterministic inversion based on deep learning has been widely utilized in model parameters *** by logging data, seismic data, wavelet and modeling operator, deterministic inversion based on deep learning can establish nonlinear relationships between seismic data and model ***, seismic data lacks low-frequency and contains noise, which increases the non-uniqueness of the solutions. The conventional inversion method based on deep learning can only establish the deterministic relationship between seismic data and parameters, and cannot quantify the uncertainty of inversion. In order to quickly quantify the uncertainty, a physics-guided deep mixture density network(PG-DMDN) is established by combining the mixture density network(MDN) with the deep neural network(DNN). Compared with Bayesian neural network(BNN) and network dropout, PG-DMDN has lower computing cost and shorter training time. A low-frequency model is introduced in the training process of the network to help the network learn the nonlinear relationship between narrowband seismic data and low-frequency impedance. In addition, the block constraints are added to the PG-DMDN framework to improve the horizontal continuity of the inversion results. To illustrate the benefits of proposed method, the PG-DMDN is compared with existing semi-supervised inversion method. Four synthetic data examples of Marmousi II model are utilized to quantify the influence of forward modeling part, low-frequency model, noise and the pseudo-wells number on inversion results, and prove the feasibility and stability of the proposed method. In addition, the robustness and generality of the proposed method are verified by the field seismic data.

关键词： Deep learning Probabilistic inversion Physics-guided Deep mixture density network

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Integrated numerical simulation of hydraulic fracturing and production in shale gas well considering gas-water two-phase flow

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Petroleum Exploration and Development 2024年第3期51卷 684-696页

作者： TANG Huiying LUO Shangui LIANG Haipeng ZENG Bo ZHANG Liehui ZHAO Yulong SONG Yi national Key Laboratory of oil and gas Reservoir Geology and Exploitation Southwest Petroleum UniversityChengdu 610500China Chengdu university of Technology Chengdu 610059China Shale gas Research Institute PetroChina Southwest Oil&Gas Field CompanyChengdu 610051China

Based on the displacement discontinuity method and the discrete fracture unified pipe network model,a sequential iterative numerical method was used to build a fracturing-production integrated numerical model of shale gas well considering the two-phase flow of gas and *** model accounts for the influence of natural fractures and matrix properties on the fracturing process and directly applies post-fracturing formation pressure and water saturation distribution to subsequent well shut-in and production simulation,allowing for a more accurate fracturing-production integrated *** results show that the reservoir physical properties have great impacts on fracture propagation,and the reasonable prediction of formation pressure and reservoir fluid distribution after the fracturing is critical to accurately predict the gas and fluid production of the shale gas *** with the conventional method,the proposed model can more accurately simulate the water and gas production by considering the impact of fracturing on both matrix pressure and water *** established model is applied to the integrated fracturing-production simulation of practical horizontal shale gas *** simulation results are in good agreement with the practical production data,thus verifying the accuracy of the model.

关键词： shale gas well hydraulic fracturing fracture propagation gas-water two-phase flow fracturing-production integrated numerical simulation

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Development review and the prospect of oil shale in-situ catalysis conversion technology

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Petroleum Science 2024年第2期21卷 1385-1395页

作者： Li Wang Chen-Hao Gao Rui-Ying Xiong Xiao-Jun Zhang Ji-Xiang Guo The Unconventional oil and gas Institute China University of Petroleum-BeijingBeijing102200China

As an unconventional resource, oil shale possesses abundant reserves and significant potential for industrial applications. The rational and efficient development of oil shale resources holds immense importance in reducing national energy demand. In-situ catalytic technology, characterized by its high efficiency, low pollution, and minimal energy consumption, represents a key direction for future oil shale development. This paper provides a comprehensive review of research progress in in-situ oil shale mining technology, oil shale pyrolysis catalysts, the pyrolysis mechanism of kerogen, and the compatibility of different heating processes and catalysts. Furthermore, the paper proposes future research directions and prospects for oil shale in-situ catalytic technology, including reservoir modification, highefficiency catalyst synthesis, injection processes, and high-efficiency heating technology. These insights serve as valuable technical references for the advancement of oil shale in-situ catalytic technology.

关键词： oil shale In-situ catalytic technology Pyrolysis catalyst Kerogen pyrolysis mechanism

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An integrated MINLP model for multi-party coordination in downstream oil supply chain

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Petroleum Science 2024年第3期21卷 2066-2079页

作者： Rui Qiu Bo Zhang Wei Zhao Ren-Fu Tu Man-Qiu He Qi Liao Yong-Tu Liang national Engineering Laboratory for Pipeline Safety/Beijing Key Laboratory of Urban oil and gas Distribution Technology China University of Petroleum-Beijing Strategy & Implementation Department PipeChina

Cooperation among enterprises can bring overall and individual performance improvement, and a smooth coordination method is indispensable. However, due to the lack of customized coordination methods, cooperation in the downstream oil supply chain cannot be carried out smoothly. This paper intends to propose a multi-party coordination method to promote cooperation between oil shippers and pipeline operator by optimizing oil transportation, oil substitution and pipeline pricing schemes. An integrated game-theoretic modeling and analysis approach is developed to characterize the operation behaviors of all stakeholders in the downstream oil supply chain. The proposed mixed integer nonlinear programming model constrains supply and demand capacity, transportation routes, oil substitution rules and pipeline freight levels. Logarithm transformation and price discretization are introduced for model linear approximation. Simulation experiments are carried out in the oil distribution system in South China. The results show that compared to the business-as-usual scheme, the new scheme saves transportation cost by 3.48%, increases pipeline turnover by 5.7%, and reduces energy consumption and emissions by 7.66% and 6.77%. It is proved that the proposed method improves the revenue of the whole system, achieves fair revenue distribution, and also improves the energy and environmental benefits of the oil supply chain.

关键词： Downstream oil supply chain Multi-party coordination Cooperative game Mixed integer nonlinear programming model Pipeline transportation Revenue distribution

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Rheological study of methane gas hydrates in the presence of micron-sized sand particle

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Chinese Journal of Chemical Engineering 2024年第6期70卷 149-161页

作者： Bohui Shi Shangfei Song Yuchuan Chen Shunkang Fu Lihao Liu Xinyao Yang Haihao Wu Guangjin Chen Jing Gong national Engineering Research Center of oil and gas Pipeline Transportation Safety MOE Key Laboratory of Petroleum EngineeringBeijing Key Laboratory of Urban Oil and Gas Distribution TechnologyChina University of Petroleum-BeijingBeijing 102249China China's oil and gas Exploration and Development Company(CNODC) Beijing 100034China China national Petroleum Corporation Mozambique LDA MaputoMozambique PipeChina West East Pipeline Company Shanghai 200122China

Natural gas hydrates,intricate crystalline structures formed by water molecules and small gas molecules,have emerged as a significant and globally impactful clean energy ***,their commercial exploitation faces challenges,particularly operational disruptions caused by sand-related *** the rheological properties of hydrate slurry,especially in the presence of micron-sized sand particles,is imperative for ensuring the flow assurance of subsea hydrate *** study extensively investigates the rheological properties of sand-containing hydrate *** findings reveal that these slurries exhibit non-Newtonian fluid characteristics,including yield stress,thixotropy,and shear-thinning ***-like elastic features are observed in sand-containing hydrate slurries before yielding,transitioning to viscous behavior after *** with a minimal amount of sand,both static yield stress and yield strain experience substantial changes,correlating with the increase in sand *** research conclusively establishes the thixotropic nature of sand-hydrate slurries,where the viscosity decay rate is directly influenced by the shear *** insights aim to contribute comprehensively to the development of effective flow assurance strategies,ensuring the safe and stable operation of subsea hydrate exploitation.

关键词： Natural gas hydrate production Sand-containing hydrate slurries Yield stress Thixotropy Shear-thinning behavior

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Combined use of fly ash and silica to prevent the long-term strength retrogression of oil well cement set and cured at HPHT conditions

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Petroleum Science 2024年第2期21卷 1122-1134页

作者： Guo-Dong Cheng Xue-Yu Pang Jin-Sheng Sun Zheng-Song Qiu Chuang-Chuang Wang Jian-Kun Qin Ning Li School of Petroleum Engineering China University of Petroleum(East China)Qingdao266580ShandongChina national Key Laboratory of Deep oil and gas China University of Petroleum(East China)Qingdao266580ShandongChina oil and gas Engineering Research Institute(Tarim oilfield Company) China National Petroleum CorporationTarim841000XinjiangChina

The long-term strength retrogression of silica-enriched oil well cement poses a significant threat to wellbore integrity in deep and ultra-deep wells, which is a major obstacle for deep petroleum and geothermal energy development. Previous attempts to address this problem has been unsatisfactory because they can only reduce the strength decline rate. This study presents a new solution to this problem by incorporating fly ash to the traditional silica-cement systems. The influences of fly ash and silica on the strength retrogression behavior of oil well cement systems directly set and cured under the condition of 200°C and 50 MPa are investigated. Test results indicate that the slurries containing only silica or fly ash experience severe strength retrogression from 2 to 30 d curing, while the slurries containing both fly ash and silica experience strength enhancement from 2 to 90 d. The strength test results are corroborated by further evidences from permeability tests as well as microstructure analysis of set cement. Composition of set cement evaluated by quantitative X-ray diffraction analyses with partial or no known crystal structure(PONKCS) method and thermogravimetry analyses revealed that the conversion of amorphous C-(A)-S-H to crystalline phases is the primary cause of long-term strength *** addition of fly ash can reduce the initial amount of C-(A)-S-H in the set cement, and its combined use with silica can prevent the crystallization of C-(A)-S-H, which is believed to be the working mechanism of this new admixture in improving long-term strength stability of oil well cement systems.

关键词： Fly ash Long-term strength retrogression High temperature Quantitative X-ray diffraction(QXRD) Partial or no known crystal structure(PONKCS)

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CO_(2)flooding in shale oil reservoir with radial borehole fracturing for CO_(2)storage and enhanced oil recovery

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Petroleum Science 2024年第1期21卷 519-534页

作者： Jia-Cheng Dai Tian-Yu Wang Jin-Tao Weng Kang-Jian Tian Li-Ying Zhu Gen-Sheng Li State Key Laboratory of Petroleum Resources and Prospecting China University of PetroleumBeijing102249China China national oil and gas Exploration and Development Company Limited Beijing100034China

This study introduces a novel method integrating CO_(2)flooding with radial borehole fracturing for enhanced oil recovery and CO_(2)underground storage,a solution to the limited vertical stimulation reservoir volume in horizontal well fracturing.A numerical model is established to investigate the production rate,reservoir pressure field,and CO_(2)saturation distribution corresponding to changing time of CO_(2)flooding with radial borehole fracturing.A sensitivity analysis on the influence of CO_(2)injection location,layer spacing,pressure difference,borehole number,and hydraulic fractures on oil production and CO_(2)storage is *** CO_(2)flooding process is divided into four *** in layer spacing will significantly improve oil production rate and gas storage ***,serious gas channeling can occur when the spacing is lower than 20 *** the pressure difference between the producer and injector,the borehole number,the hydraulic fracture height,and the fracture width can also increase the oil production rate and gas storage *** analysis shows that layer spacing and fracture height greatly influence gas storage and oil *** outcomes are expected to provide a theoretical basis for the efficient development of shale oil reservoirs in the vertical direction.

关键词： Shale oil Radial borehole fracturing Embedded discrete fracture model Enhanced oil recovery Carbon storage

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Quantitative evaluation of adsorbed and free water in deep shales:a case study on the Wufeng-Longmaxi Formations from the Luzhou area,southern Sichuan Basin,China

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Frontiers of Earth Science 2024年第2期18卷 336-346页

作者： Shengxian ZHAO Yongyang LIU Shuangfang LU Shuaihu LIU Wenbiao LI Zhiyan ZHOU Yashuo WANG Zhaojing SONG Key Laboratory of Deep oil and gas China University of Petroleum(East China)Qingdao 266580China School of Geosciences China University of Petroleum(East China)Qingdao 266580China Shale gas Research Institute of PetroChina Southwest oil&gasfield Company Chengdu 610051China Sanya Offshore oil&gas Research Institute Northeast Petroleum UniversitySanya 572025China

Deep shale gas reservoirs commonly contain connate water, which affects the enrichment and migration of shale gas and has attracted the attention of many scholars. It is significant to quantitatively estimate the amounts of adsorbed and free water in shale matrix pores, considering the different impacts of pore water (adsorbed water and free water) on shale gas. In this paper, pore water in six deep shale samples from the Wufeng-Longmaxi Formations in the Luzhou area, southern Sichuan Basin, China, was quantitatively evaluated by saturation-centrifugation experiments. Further, the impact of shale material composition and microstructure on the pore water occurrence was analyzed. The results show that amounts of adsorbed and free water are respectively 1.7967–9.8218 mg/g (mean 6.4501 mg/g) and 9.5511–19.802 mg/g (mean 13.9541 mg/g) under the experimental conditions (30°C, distilled water). The ratio of adsorbed water to total water is 15.83%–42.61% (mean 30.45%). The amounts of adsorbed and free water are related to the pore microstructure and material compositions of shale. The specific surface area of shale controls the amount of adsorbed water, and the pore volume controls the amount of free water;organic pores developed in shale solid asphalt contribute specific surface area and pore volume, and inorganic pores developed in clay mineral contribute pore volume. Therefore, the pores of shale solid asphalt accumulate the adsorbed water and free water, and the pores of clay minerals mainly accumulate the free water.

关键词： deep shales pore water adsorbed amount free amount

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