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Implications of electrode modifications in aqueous organic redox flow batteries

Journal of Energy Chemistry 2024年第8期95卷 499-510,I0011页

作者： Zahid Manzoor Bhat Mohammad Furquan Muhammad Aurang Zeb Gul Sial Umair Alam Atif Saeed Alzahrani Mohammad Qamar Interdisciplinary research center for Hydrogen Technologies and Carbon Management(IRC-HTCM) King Fahd University of Petroleum&Minerals(KFUPM)Dhahran 31261Saudi Arabia Department of Materials Science and Engineering King Fahd University of Petroleum and MineralsDhahran 31261Saudi Arabia Interdisciplinary research center for Sustainable Energy Systems(IRC-SES) King Fahd University of Petroleum and MineralsDhahran 31261Saudi Arabia

Aqueous organic redox flow batteries(RFBs)exhibit favorable characteristics,such as tunability,multielectron transfer capability,and stability of the redox active molecules utilized as anolytes and catholytes,making them very viable contenders for large-scale grid storage *** attention has been paid on the development of efficient redox-active molecules and their performance optimization through chemical substitutions at various places on the backbone as part of the pursuit for high-performance *** the fact that electrodes are vital to optimal performance,they have not garnered significant *** research has been conducted on the effects of electrode modifications to improve the performance of *** primary emphasis has been given on the impact of electrode engineering to augment the efficiency of aqueous organic *** overview of electron transfer at the electrode-electrolyte interface is *** implications of electrode modification on the performance of redox flow batteries,with a particular focus on the anodic and cathodic half-cells separately,are then *** each section,significant discrepancies surrounding the effects of electrode engineering are thoroughly examined and ***,we have presented a comprehensive assessment along with our perspectives on the future trajectory.

关键词： Redox flow batteries Electrode modification Organic redox molecules Outer sphere and inner sphere

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Design and Synthesis of NiO@Co_(3)O_(4)@ZSM-5 Heterogeneous Multitask Hollow Structures for Tandem Catalysis

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Chemical research in Chinese Universities 2024年第3期40卷 529-535页

作者： Muhammad Waqas Interdisciplinary research center for Refining and Advanced Chemicals King Fahd University of Petroleum&MineralsDhahran 31261Saudi Arabia

Precipitation and impregnation procedures unevenly distribute metals on zeolite,limiting chemical transformation in Lewis-acid,Brönsted-acid and metal-catalyzed tandem ***,heterogeneous multitask transition metals oxides@zeolites are promising catalysts for sustainable processes;nevertheless,synthesis is fascinating and ***,the construction of purposely designed multitask materials segregated in selective shells reveals the remarkable spatial organization of metals-zeolite,resulting in them being suitable for a wide range of tandem *** synthesis of multi-site catalysts begins with a universal wet chemistry approach that yields nickel oxide(NiO)***,the NiO crystals are stabilized using cationic dodecyltrimethylammonium bromide,followed by achieving cross-linking carbon growth by emulsion polymerization of glucose in hydrothermal treatment to yield uniformed NiO@carbon spheres(NiO@CSs).Next,sequential adsorption of cobalt cations and colloidal ZSM-5(1%in H_(2)O,mass fraction),followed by calcination in air,yielded NiO@cobalt oxide@zeolite denoted as NiO@Co_(3)O_(4)@ZEO hollow *** hollowing mechanism and materials segregation within shells are revealed by scanning and transmission electron microscopy,thermogravimetric analysis,and X-ray *** finding advances the rational synthesis of heterogenous core-shell hollow structures for various gas phase catalytic tandem reactions to yield valuable chemicals.

关键词： Multifunctional Core-shell hollow spheres Gas-phase reaction Valuable chemical

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A Novel Layered Double Hydroxide and Dodecyl Alcohol Assisted PCM Composite with High Latent Heat Storage Capacity and Thermal Conductivity

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Journal of Thermal Science 2024年第2期33卷 537-547页

作者： AL-AHMED Amir SARI Ahmet KHAN Firoz AL-RASHEIDI Masoud Hekimoğlu Gökhan AFZAAL Mohammad A.ALSULAMI Ahmed DAFALLA Hatim SALHI Billel A.ALSULAIMAN Fahad Interdisciplinary research center for Renewable Energy and Power Systems(IRC-REPS) King Fahd University of Petroleum&MineralsDhahran31261Saudi Arabia Department of Metallurgical and Material Engineering Karadeniz Technical UniversityTrabzon61080Turkey Maths and Natural Sciences Division Higher Colleges of TechnologyP.O.Box 7947SharjahUnited Arab Emirates Department of Mechanical Engineering King Fahd University of Petroleum&MineralsDhahran31261Saudi Arabia Core research Facilities King Fahd University of Petroleum&MineralsDhahran31261Saudi Arabia Interdisciplinary research center for Membranes and Water Security King Fahd University of Petroleum&MineralsDhahran31261Saudi Arabia

Dodecyl alcohol(DDA) is a promising solid-liquid phase change material(PCM) due to its favorable latent heat storage(LHS) ***,the leakage issue of PCM in a melted state during the heating period and low thermal conductivity restricts its utilization potential in thermal energy storage(TES) *** the same context,the present work aims to overcome the leakage issue and improve the thermal conductivity of the *** this in mind,a novel leak-proof layered double hydroxide(LDH)/DDA composite PCM is proposed through a solution-based impregnation *** leak-proof impregnation ratio of the DDA impregnated within the cavities of the synthesized Al/Fe-LDH was determined to be 60%.Detailed morphological,physicochemical,and thermal properties of the fabricated composite were studied by scanning electron microscopy(SEM),Fourier transforms infrared(FTIR) spectroscopy,X-ray diffraction(XRD)spectroscopy,differential scanning calorimetry(DSC),thermalgravimetric analysis(TGA),and thermal cycling *** results show that the LDH/DDA composite has a suitable phase change temperature(about 20℃) for passive solar thermal management of building *** composite PCM showed high LHS enthalpy(about136 J/g),good thermal stability,and cycling LHS *** also showed nearly 152% higher thermal conductivity compared to that of pure DDA,ultimately reducing the melting and solidification time of the pure DDA by 44.9% and 45.5%,respectively.

关键词： dodecyl alcohol layered double hydroxide composite PCM thermal conductivity thermal energy storage(TES)

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A Lightweight Intrusion Detection System Using Convolutional Neural Network and Long Short-Term Memory in Fog Computing

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Computers, Materials & Continua 2024年第9期80卷 4703-4728页

作者： Hawazen Alzahrani Tarek Sheltami Abdulaziz Barnawi Muhammad Imam Ansar Yaser Computer Engineering Department Interdisciplinary Research Center of Smart Mobility and LogisticsKing Fahd University of Petroleum and MineralsDhahran31261Saudi Arabia Computer Engineering Department Interdisciplinary Research Center for Intelligent Secure SystemsKing Fahd University of Petroleum and MineralsDhahran31261Saudi Arabia Transportation research Institute(IMOB) Hasselt UniversityHasselt3500Belgium

The Internet of Things(IoT)links various devices to digital services and significantly improves the quality of our ***,as IoT connectivity is growing rapidly,so do the risks of network vulnerabilities and *** interesting Intrusion Detection Systems(IDSs)are presented based on machine learning(ML)techniques to overcome this *** the resource limitations of fog computing environments,a lightweight IDS is *** paper introduces a hybrid deep learning(DL)method that combines convolutional neural networks(CNN)and long short-term memory(LSTM)to build an energy-aware,anomaly-based *** test this system on a recent dataset,focusing on reducing overhead while maintaining high accuracy and a low false alarm *** compare CICIoT2023,KDD-99 and NSL-KDD datasets to evaluate the performance of the proposed IDS model based on key metrics,including latency,energy consumption,false alarm rate and detection rate *** findings show an accuracy rate over 92%and a false alarm rate below 0.38%.These results demonstrate that our system provides strong security without excessive resource *** practicality of deploying IDS with limited resources is demonstrated by the successful implementation of IDS functionality on a Raspberry Pi acting as a Fog *** proposed lightweight model,with a maximum power consumption of 6.12 W,demonstrates its potential to operate effectively on energy-limited devices such as low-power fog nodes or edge *** prioritize energy efficiency whilemaintaining high accuracy,distinguishing our scheme fromexisting *** experiments demonstrate a significant reduction in false positives,ensuring accurate identification of genuine security threats while minimizing unnecessary alerts.

关键词： Intrusion detection fog computing CNN LSTM energy consumption

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Effective utilization of dolomitic lead-zinc waste rock by replacing dolomite as flux in iron ore sintering process

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Journal of Iron and Steel research International 2024年第8期31卷 1861-1872页

作者： Xin Wang Cong-cong Yang Jian Pan De-qing Zhu Zheng-qi Guo Guang-hui Xia Shi-juan Qu School of minerals Processing and Bioengineering Central South UniversityChangsha 410083HunanChina Low-Carbon and Hydrogen Metallurgy research center Central South UniversityChangsha 410083HunanChina

With increasingly stringent environmental protection policies,cost-effective and value-added treatment of massive lead-zinc waste rock(LZWR)generated from the preconcentration process has attracted substantial attention.A type of dolomitic LZWR with 18 wt.%MgO,27 wt.%CaO,0.29 wt.%Zn and 1.43 wt.%S was used as a replacement flux in the iron ore sintering *** sinter pot tests were carried out based on an industrial ore *** results show that replacing 0%-60%of dolomite with LZWR does not adversely affect the sintering productivity,fuel consumption rate,and the quality of the sinter products,while the Zn and S elements contained in LZWR can be effectively removed with the residual Zn and S contents of the resultant sinter products being less than 0.02 and 0.055 wt.%,***,substituting LZWR for dolomite as a flux inevitably increases the SO_(2) concentration in the sintering flue gas due to its high sulfur *** the processing capacity of the sintering flue gas desulfurization system,the replacement ratio of dolomite can reach 40%,equal to LZWR consumption of 24.3 kg per ton of *** SO_(2) in sintering flue gas can be recovered to produce(NH_(4))_(2)SO_(4) or HSO_(4),while the volatilized Zn collected into the zinc-containing dust can be subsequently recycled by the rotary hearth furnace ***,it is technologically and economically feasible to use the LZWR as a replacement flux in the iron ore sintering process,providing a new way for the safe,large-scale and low-cost treatment of LZWR.

关键词： Lead Zinc waste rock Dolomite Sintering Flue gas Sinter product

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Microalgae cultivation in photobioreactors: sustainable solutions for a greener future

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Green Chemical Engineering 2024年第4期5卷 418-439页

作者： Shaikh Abdur Razzak Khairul Bahar K.M.Oajedul Islam Abdul Khaleel Haniffa Mohammed Omar Faruque S.M.Zakir Hossain Mohammad M.Hossain Chemical Engineering Department King Fahd University of Petroleum and Minerals center for Refining and Advanced Chemicals King Fahd University of Petroleum & Minerals Department of Chemical Engineering University of Bahrain

Microalgae cultivation in photobioreactors（PBRs） has emerged as a promising and sustainable approach to address various environmental and energy challenges, offering a multitude of benefits across diverse *** developments in microalgae cultivation in photobioreactors have contributed substantially to the development and optimization of sustainable bioprocesses. This review presents a comprehensive analysis of recent innovations and breakthroughs in the field of microalgae cultivation, with a specific focus on their application in photobioreactors, aimed at paving the way for a greener future. This study in-depth examines the advantages of microalgae cultivation in photobioreactors, concentrating on its effectiveness in wastewater treatment, CO2bioremediation, and the production of biofuels and high-value products. The review evaluates the effects of light,solar irradiation, temperature, nitrogen and phosphorus concentrations in culture media, CO2concentrations, and pH on microalgae growth performance, including specific growth and biomass productivity. The study also examines open systems like unstirred ponds, raceway ponds, and circular ponds and closed systems like horizontal tubular, vertical bubble-column, airlift, flat panel, and plastic-bag photobioreactors, comparing their pros and cons. To optimize microalgae cultivation, key factors in photobioreactor design, including photosynthetic efficiencies, light/dark（L/D） cycles, CO2concentrations, mass transfer, hydrodynamics behavior, and p H, are extensively investigated. In addition, the review outlines recent developments in large-scale photobioreactors and highlights the challenges and opportunities associated with photobioreactor scale-up and design parameter optimization, including genetic engineering and economic feasibility. This article is a vital resource for researchers, engineers, and industry professionals seeking sustainable bioprocesses and the application of microalgae-based technol

关键词： Microalgae biomass CO 2 biofixation Wastewater treatment Biofuel Photobioreactors

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The utilization of spent palm cooking oil for formulating oil-based drilling muds with excellent H_(2)S scavenging capability

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Petroleum research 2024年第2期9卷 280-288页

作者： Sagheer A.Onaizi Department of Chemical Engineering and Interdisciplinary Research Center for Hydrogen and Energy StorageKing Fahd University of Petroleum&Minerals31261DhahranSaudi Arabia

In this study,a spent palm cooking oil-based mud with an excellent H_(2)S scavenging capability induced by the inclusion of a small quantity of potassium permanganate is formulated and tested for the first *** mud formulation,containing the spent palm oil as the continuous phase and water as the dispersed phase,respectively,was stabilized by Span 80 and rhamnolipid biosurfactant as primary and secondary emulsifiers,respectively,while hydrophobic zinc nanoparticles(NPs)were used as weighting *** results showed that H_(2)S scavenging capacity at the breakthrough time reached 182.4 g H_(2)S/barrel mud,which increased to 417.9 g H_(2)S/barrel mud at the saturation time,demonstrating the effective H_(2)S scavenging performance of the formulated *** spent palm oil-based mud(SPOBM)also showed a good flow behavior that could be well fitted using the Herschel-Bulkley and Casson *** effect of temperature on the apparent viscosity of the SPOBM has been investigated,and the fitting of the viscosity-temperature data provided an estimate of the activation energy as 23.53 kJ/*** findings reported in this article reveal the feasibility of transforming the spent/waste cooking oils into a valuable commodity for formulating greener drilling fluids with acceptable rheology and excellent H_(2)S scavenging performance.

关键词： Hydrogen sulfide(H_(2)S) Oil-based mud(OBM)drilling fluids Spent palm oil H_(2)S scavengers Rheology

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An Optimization Approach of IoD Deployment for Optimal Coverage Based on Radio Frequency Model

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Computer Modeling in Engineering & Sciences 2024年第6期139卷 2627-2647页

作者： Tarek Sheltami Gamil Ahmed Ansar Yasar Computer Engineering Department Interdisciplinary Research Center of Smart Mobility and LogisticsKing Fahd University of Petroleum and MineralsDhahran31261Saudi Arabia Transportation research Institute(IMOB) Hasselt UniversityHasselt3500Belgium

Recently,Internet of Drones(IoD)has garnered significant attention due to its widespread ***,deploying IoD for area coverage poses numerous limitations and *** include interference between neighboring drones,the need for directional antennas,and altitude restrictions for *** challenges necessitate the development of efficient *** research paper presents a cooperative decision-making approach for an efficient IoDdeployment to address these challenges *** primary objective of this study is to achieve an efficient IoDdeployment strategy thatmaximizes the coverage regionwhile minimizing interference between neighboring *** deployment problem,the interference increases as the number of deployed drones increases,resulting in bad quality of *** the other hand,deploying a few drones cannot satisfy the coverage *** accomplish this,an enhanced version of a concise population-based meta-heuristic algorithm,namely Improved Particle SwarmOptimization(IPSO),is *** objective function of IPSO is defined based on the coverage probability,which is primarily influenced by the characteristics of the antennas and drone altitude.A radio frequency(RF)model is derived to evaluate the coverage quality,considering both Line of Sight(LOS)and Non-Line of Sight(NLOS)down-link coverage probabilities for ground *** is assumed that each drone is equipped with a directional antenna to optimize coverage in a given *** simulations are conducted to assess the effectiveness of the proposed *** demonstrate that the proposed method achieves maximum coverage with minimum transmission ***,a comparison is made against Collaborative Visual Area Coverage Approach(CVACA),and a game-based approach in terms of coverage quality and convergence *** simulation results reveal that our approach outperforms both CVACA and the gamebased schemes in terms of coverage an

关键词： IoD line of sight optimal deployment IPSO RF model

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Layer-by-layer fabrication of montmorillonite coating immobilizing Cu_(2)O nanoparticles for continuously catalyzing glycerol to dihydroxyacetone

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Chinese Journal of Chemical Engineering 2024年第4期68卷 263-275页

作者： Kejin Li Jiahui Liu Dajian Li Xiaolan Chen Chunhui Zhou research Group for Advanced Materials&Sustainable Catalysis(AMSC) State Key Laboratory Breeding Base of Green Chemistry-Synthesis TechnologyCollege of Chemical EngineeringZhejiang University of TechnologyHangzhou 310032China Qing Yang Institute for Industrial minerals Qingyang 242804China Engineering research center of Non-metallic minerals of Zhejiang Province Zhejiang Institute of Geology and Mineral ResourcesHangzhou 310007China

Microreactors are increasingly used for green and safe chemical processes owing to their benefits of superior mass and heat transfer,increased yield,safety,and simplicity of ***,immobilizing catalysts in microreactors remains *** this investigation,a technique for creating Cu_(2)O/montmorillonite catalyst coating,using electrostatic attraction for layer-by-layer self-assembly,was *** montmorillonite film's morphology and thickness could be efficiently regulated by adjusting the degree of exfoliation and surface charge of montmorillonite,alongside layer-by-layer coating *** Cu_(2)O nanoparticles were immobilized using the flow deposition *** resulting Cu_(2)O@montmorillonite-film-coated capillary microreactor successfully transformed glycerol into *** conversion of glycerol and product selectivity could be controlled by adjusting the molar ratio of reactants,temperature,residence time,and Cu_(2)O *** maximum glycerol conversion observed was 47.6%,with a 27%selectivity toward *** study presents a technique for immobilizing montmorillonite-based catalyst coatings in capillary tubing,which can serve as a foundation for the future application of microreactors in glycerol conversion.

关键词： Microreactor Coating Montmorillonite Glycerol Cu_(2)O

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Mechanical behaviour of fiber-reinforced grout in rock bolt reinforcement

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Journal of Rock Mechanics and Geotechnical Engineering 2024年第2期16卷 437-453页

作者： Yingchun Li Ammar Ahmed Danqi Li Deep Underground Engineering research center Dalian University of TechnologyDalian116024China WA School of Mines:minerals Energy and Chemical Engineering Curtin UniversityKalgoorlieWA6430Australia

Grouted rock bolts subject to axial loading in the field exhibit various failure modes,among which the most predominant one is the bolt-grout interface ***,mechanical characterization of the grout is essential for understanding its performance in ground *** date,few studies have been conducted to characterize the mechanical behaviour of fiber-reinforced grout(FRG)in rock bolt *** we experimentally studied the mechanical behaviour of FRG under uniaxial compression,indirect tension,and direct shear loading *** also conducted a series of pullout tests of rebar bolt encapsulated with different grouts including conventional cementitious grout and *** was developed using 15%silica fume(SF)replacement of cement(by weight)and steel fiber to achieve highstrength and crack-resistance to overcome drawbacks of the conventional *** types of steel fibers including straight and wavy steel fibers were further added to enhance the grout *** effect of fiber shape and fiber volume proportion on the grout mechanical properties were *** experimental results showed that the addition of SF and steel fiber by 1.5%fiber volume proportion could lead to the highest compressive,tensile,and shear strengths of the *** minimum volume of fiber that could improve the mechanical properties of grout was found at 0.5%.The scanning electron microscopy(SEM)analysis demonstrated that steel fibers act as an excellent bridge to prevent the cracks from propagating at the interfacial region and hence to aid in maintaining the integrity of the cementitious *** laboratory pullout tests further confirmed that FRG could prevent the cylindrical grout annulus from radial crack and hence improve the rebar’s load carrying ***,FRG has a potential to be utilized in civil and mining applications where high-strength and crack-resistance support is required.

关键词： Fiber-reinforced grout(FRG) Steel fibers Mechanical properties Direct shear test Pullout test

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