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Evolution of inclusions in vacuum induction melting of superalloys containing 70%return material

Journal of Iron and Steel Research(International) 2024年第3期31卷 719-728页

作者： Jin-guo Gao Shu-lei Yang Shu-feng Yang Jing-she Li Wei Liu Meng-jing Zhao An-ren Wang School of metallurgical and Ecological Engineering University of Science and Technology BeijingBeijing 100083China State Key Laboratory of Advanced Metallurgy University of Science and Technology BeijingBeijing 100083China metallurgical and building materials business department China International Engineering Consulting CorporationBeijing 100048China

The variation law of inclusions type and size in the vacuum induction melting process and ingot of Ni-based superalloy containing 70%return material was studied by industrial test sampling,and the mechanism of inclusions formation was analyzed with thermodynamic *** results show that there are mainly two types of composite inclusions in the vacuum induction melting of Ni-based superalloys,which are nitride-and oxide-based composite inclusions,like Al_(2)O_(3)-SiO_(2)-Cr_(2)O_(3),TiN-(Mo,Nb)C,*** type and proportion of inclusions from the center to the edge of the vacuum induction ingot did not change *** number density of inclusions from the center to the edge of the ingot varied less,and the size of inclusions became smaller from the center to the *** addition,thermodynamic calculations show that oxides(M_(2)O_(3))are present in the liquid phase and mainly contain Al,Ti,Cr,Fe and O *** nitride consists mainly of Ti and N and contains small amounts of Cr,C,Nb,and Mo *** is consistent with the results of industrial *** the temperature decreases,the precipitation phases such as M_(2)O_(3),MN,γ,MC,δ,γ'andμphases are gradually precipitated,where oxides and nitrides are present in the liquid *** contents of O and N elements are the main influencing factors for the inclusions content and precipitation temperature;when the nitrogen content is reduced to below 0.0015%,it can make MN precipitate below the liquid-phase line.

关键词： Ni-based superalloy Vacuum induction melting Return material Inclusion Thermodynamic

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Synthesis of Long-Chain Oligomeric Donor and Acceptors via Direct Arylation for Organic Solar Cells

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Chinese Journal of Chemistry 2024年第5期42卷 523-532页

作者： Yu Wu Xin-Yu He Xu-Min Huang Ling-Jun Yang Peng Liu Na Chen Chang-Zhi Li Shi-Yong Liu Jiangxi Provincial Key Laboratory of Functional Molecular materials Chemistry College of MaterialsMetallurgical and ChemistryJiangxi University of Science and TechnologyGanzhouJiangxi341000 China department of Polymer Science and Engineering Zhejiang UniversityHangzhouZhejiang310027 China

The rapid synthesis of structurally complicated electron donors&acceptors still remains a major challenge in organic solar cells(OSC).In this work,we developed a highly efficient strategy to access long-chain oligomeric donor and acceptors for OSC applications.A series of cyclopentadithiophene(CPDT)and benzothiadiazole(BT)-basedπ-conjugated oligomers,i.e.,three oligomeric acceptors(BTDT)n-IC(n=1—3)and one long-chain oligomeric donor(BTDT)4-RD,are facilely synthesized by an atom-and step-economical,and labor-saving direct C—H arylation(DACH)reaction(i.e.,C—H/C—Br cross coupling).Note that(BTDT)4-RD involving five CPDT,four BT and two rhodamine(RD)building blocks is the longest oligomeric donor in the fullerene-free OSC devices ever *** dependence of the structure-property-performance correlation of(BTDT)n-IC(n=1—3)and(BTDT)4-RD on theπ-conjugation lengths is thoroughly investigated by opto-electrochemical measurements,bulk heterojunction(BHJ)OSC devices and ***(BTDT)1-IC:PBDB-T and(BTDT)4-RD:Y6 BHJs achieve power conversion efficiencies of 9.14%and 4.51%,*** findings demonstrate that DACH reaction is a powerful tool to tune the opto-electronic properties and device performances by regulating the lengths ofπ-conjugated oligomers with varied numbers of repeating units.

关键词： Long-chainπ-conjugated oligomer Organic solar cells Direct arylation Atom-economical synthesis Cyclopentadithiophene Benzothiadiazole C—H activation Conjugation Oligomers

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Developing Lexicons for Enhanced Sentiment Analysis in Software Engineering:An Innovative Multilingual Approach for Social Media Reviews

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Computers, materials & Continua 2024年第5期79卷 2771-2793页

作者： Zohaib Ahmad Khan Yuanqing Xia Ahmed Khan Muhammad Sadiq Mahmood Alam Fuad AAwwad Emad A.A.Ismail School of Automation Beijing Institute of TechnologyBeijing100081China department of Computer Science and Technology University of Science and Technology BannuKPKBannu28100Pakistan School of Computer Science and Engineering Central South UniversityChangsha410083China department of Quantitative Analysis College of Business AdministrationKing Saud UniversityP.O.Box 71115Riyadh11587Saudi Arabia

Sentiment analysis is becoming increasingly important in today’s digital age, with social media being a significantsource of user-generated content. The development of sentiment lexicons that can support languages other thanEnglish is a challenging task, especially for analyzing sentiment analysis in social media reviews. Most existingsentiment analysis systems focus on English, leaving a significant research gap in other languages due to limitedresources and tools. This research aims to address this gap by building a sentiment lexicon for local languages,which is then used with a machine learning algorithm for efficient sentiment analysis. In the first step, a lexiconis developed that includes five languages: Urdu, Roman Urdu, Pashto, Roman Pashto, and English. The sentimentscores from SentiWordNet are associated with each word in the lexicon to produce an effective sentiment score. Inthe second step, a naive Bayesian algorithm is applied to the developed lexicon for efficient sentiment analysis ofRoman Pashto. Both the sentiment lexicon and sentiment analysis steps were evaluated using information retrievalmetrics, with an accuracy score of 0.89 for the sentiment lexicon and 0.83 for the sentiment analysis. The resultsshowcase the potential for improving software engineering tasks related to user feedback analysis and productdevelopment.

关键词： Emotional assessment regional dialects SentiWordNet naive bayesian technique lexicons software engineering user feedback

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Hot Corrosion Behavior of Friction Welded AISI 4140 and AISI 304 in K_2SO-60% NaCl Mixture

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Journal of materials Science & Technology 2012年第10期28卷 895-904页

作者： N.Arivazhagan K.Senthilkumaran S.Narayanan K.Devendranath Ramkumar S.Surendra S.Prakash School of Mechanical and building Sciences VIT University department of metallurgical and materials Engineering Indian Institute of Technology Roorkee

Understanding the behavior of weldment at elevated temperatures and especially the corrosion behavior has become an object of scientific investigation recently. Investigation has been carried out on friction welded AISI 4140 and AISI 304 in molten salt of K2SO4-60% NaCI environment at 550, 600 and 650 ℃ under cyclic condition. The resulted oxide scales in the weldment have been characterized systematically by surface analytical techniques. From the results of the experiments~ it is observed that the scale thickness on low alloy steel side was higher than that on stainless steel side. Furthermore, weld interface has been found to be more susceptible to degradation than base metals due to inter diffusion of element across the interface and the formation of intermetallic compound. The influences of welding parameters and the temperature of exposure on the hot corrosion behavior of the weldment were discussed in this paper.

关键词： Friction Welding Dissimilar metals Hot corrosion

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Synchrotron Characterisation of Ultra-Fine Grain TiB_(2)/Al-Cu Composite Fabricated by Laser Powder Bed Fusion

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Acta Metallurgica Sinica(English Letters) 2022年第1期35卷 78-92页

作者： Sheng Li Biao Cai Ranxi Duan Lei Tang Zihan Song Dominic White Oxana V.Magdysyuk Moataz M.Attallah School of Metallurgy and materials University of BirminghamEdgbastonBirminghamB152TTUK department of materials Science and Engineering Southern University of Science and TechnologyShenzhen518055China ZEISS House Building 1030Cambourne Business ParkCambourneCambridgeCB236DWUK Diamond Light Source Ltd Harwell Science and Innovation CampusDidcotOX110DEOxfordshireUK

Isotropy in microstructure and mechanical properties remains a challenge for laser powder bed fusion(LPBF)processed materials due to the epitaxial growth and rapid cooling in *** this study,a high-strength TiB_(2)/Al-Cu composite with random texture was successfully fabricated by laser powder bed fusion(LPBF)using pre-doped TiB_(2)/Al-Cu composite powder.A series of advanced characterisation techniques,including synchrotron X-ray tomography,correlative focussed ion beam-scanning electron microscopy(FIB-SEM),scanning transmission electron microscopy(STEM),and synchrotron in situ X-ray diffraction,were applied to investigate the defects and microstructure of the as-fabricated TiB_(2)/Al-Cu composite across multiple length *** study showed ultra-fine grains with an average grain size of about 0.86μm,and a random texture was formed in the as-fabricated condition due to rapid solidification and the TiB_(2)particles promoting heterogeneous *** yield strength and total elongation of the as-fabricated composite were 317 MPa and 10%,*** contributions of fine grains,solid solutions,dislocations,particles,and Guinier-Preston(GP)zones were *** was found to be initiated from the largest lack-of-fusion pore,as revealed by in situ synchrotron tomography during tensile *** situ synchrotron diffraction was used to characterise the lattice strain evolution during tensile loading,providing important data for the development of crystal-plasticity models.

关键词： Aluminium metal matrix composite Laser powder bed fusion Heterogeneous nucleation Synchrotron characterisation

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GREEN SYNTHESIS OF ANTIBACTERIAL CHITOSAN FILMS LOADED WITH SILVER NANOPARTICLES

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Chinese Journal of Polymer Science 2013年第7期31卷 984-993页

作者： Neama A. Reiad Omar E. Abdel Salam Ehab F. Abadir Farid A. Harraz Sanitary & Environmental Engineering department Housing & Building National Research Center department of Chemical Engineering Faculty of EngineeringCairo University Advanced materials Technology department Central Metallurgical R & D Institute

An eco-friendly chemical reduction method was successfully used for the preparation of chitosan （CTS） composite films loaded with silver nanoparticles （AgNPs） by self assembly method using poly（ethylene glycol） as both reducing and stabilizing agent. UV-Vis spectra of the prepared chitosan loaded silver nanoparticles （CTSLAg） films reveal that full reduction of silver ions to silver nanoparticles takes place at 90 ℃. The effect of reaction conditions on the silver nanoparticles formation was investigated using UV-Vis spectrophotometer. The morphology of the films was tested by scanning electron microscopy （SEM）. The DSC curves showed that the CTSLAg film had a favorable compatibility and heat stability. AgNPs were confirmed by XRD and UV-Vis spectroscopy. The TEM findings revealed that the silver nanoparticles synthesized were spherical in shape with uniform dispersal, and by increasing CTS：PEG ratio larger silver nanoparticles could be obtained. The results of antibacterial study reveal that the prepared nanoeomposite films exhibited potential inhibition.

关键词： Chitosan Silver nanoparticles Antibacterial activity.

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Preparation and properties of silane coupling agent modified steel slag as functional filler for anti-corrosion coating

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Journal of Iron and Steel Research(International) 2023年第4期30卷 708-716页

作者： Wei-cheng Zheng Wei-cheng Xu Hao Zhang Hao-xuan Zheng Lin Wang Zheng-ming Cheng Yan-fei Ye Jun Lin Hong-ming Long School of metallurgical Engineering Anhui University of TechnologyMa’anshan 243032AnhuiChina Key Laboratory of metallurgical Emission Reduction and Resources Recycling(Anhui University of Technology) Ministry of EducationMa’anshan 243002AnhuiChina School of Civil Engineering and Architecture Anhui University of TechnologyMa’anshan 243032AnhuiChina department of Chemical and Biochemical Engineering Western UniversityLondonON N6A 3K7Canada Shanghai Baosteel New building materials Technology Co. Ltd.Shanghai 201900China Shougang Jingtang United Iron&Steel Co. Ltd.Tangshan 063200HebeiChina Zhanjiang Baosteel New building materials Technology Co. Ltd.Zhenjiang 524047GuangdongChina Guilin Hongcheng Mining Equipment Manufacture Co. Ltd.Guilin 541000GuangxiChina

The chemical composition and high wear resistance of steel slag(SS)make it a potential alternative to traditional inorganic fillers.3-Aminopropyltriethoxysilane(KH550)modified steel slag(MSS)was successfully prepared,and its application in epoxy(EP)anti-corrosion coating was *** to the grafting of silane coupling agent functional groups onto the surface of SS,MSS exhibited improved solubility in xylene organic solvent and reduced *** the MSS content was 15 wt.%,the contact angle of the MSS/EP composite coating was 101°,and the abrasion was only 0.07 g,compared with 56.2°and 0.13 g,respectively,for the pure EP *** corrosion resistance of coatings was investigated by performing the electrochemical test(impedance)after immersion in a 3.5 wt.%NaCl *** electrochemical test results showed that the impedance modulus of the 15 wt.%MSS/EP composite coating at low frequency(Z_(f)=0.01 Hz)was approximately 1.08×10^(7)Ωcm^(2),which was two orders of magnitude higher than that of the pure EP coating.

关键词： Steel slag Silane coupling agent Modification Epoxy coating Inorganic filler

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Chemical and Thermal Characterization of Cement Mortar Containing Ground Palm Oil Fuel Ash as a Partial Cement Replacement

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Journal of Wuhan University of Technology(materials Science) 2023年第3期38卷 575-581页

作者： SUMRA Yousuf PAYAM Shafigh IFTIKHAR Ahmed Channa M Rizwan TANVEER Ahmed Khan BELAL Alsubari MUSTABSHIRHA Gul l.department of building and Architectural Engineering Faculty of Engineering&TechnologyBahauddin Zakariya University60000 MultanPakistan Centre for building Construction&Tropical Architecture(BuCTA)Faculty of Built EnvironmentUniversity of Malaya50603 Kuala LumpurMalaysia department of metallurgical Engineering NED University of Engineering and Technology74200 KarachiPakistan department of Civil Engineering Faculty of EngineeringMiami College of Henan UniversityKaifeng475001China department of Mechanical Engineering University of Malaya50603 Kuala LumpurMalaysia department of Mechanical Engineering Faculty of Engineering&TechnologyBahauddin Zakariya University60000 MultanPakistan

This study investigates the influence of using ground palm oil fuel ash(G-POFA) from 10%-30% as cement replacement(by weight) on the cement mortar's pH under various curing conditions. These findings were supplemented by thermal gravimetric analysis(TGA). Moreover, the resistance of G-POFA blended cement mortars to water absorption and sorptivity was determined. Further, the k-value test was carried out to explain the pozzolanic and filler behavior of G-POFA and to support the results obtained from TGA. It was found that there was no significant impact of several curing conditions on the pH of mortars. The mortar with 10% G-POFA in replacement of cement(G-POFA-10) exhibited the best resistance against water absorption and sorptivity.

关键词： curing condition Ca(OH)_(2)content k-value pH palm oil fuel ash

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Adsorptive removal of iron and manganese ions from aqueous solutions with microporous chitosan/polyethylene glycol blend membrane

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Journal of Environmental Sciences 2012年第8期24卷 1425-1432页

作者： Neama A.Reiad Omar E.Abdel Salam Ehab F.Abadir Farid A.Harraz Sanitary&Environmental department Housing&Building National Research Center87 el Tahrir st.DokkiEgypt department of Chemical Engineering Faculty of EngineeringCairo UniversityGizaEgypt Advanced materials Technology department Central Metallurgical R&D InstituteHelwanEgypt

Microporous chitosan （CS） membranes were directly prepared by extraction of poly（ethylene glycol）（PEG） from CS/PEG blend membrane and were examined for iron and manganese ions removal from aqueous solutions. The different variables affecting the adsorption capacity of the membranes such as contact time, pH of the sorption medium, and initial metal ion concentration in the feed solution were investigated on a batch adsorption basis. The affinity of CS/PEG blend membrane to adsorb Fe（II） ions is higher than that of Mn（II） ions, with adsorption equilibrium achieved after 60 min for Fe（II） and Mn（II） ions. By increasing CS]PEG ratio in the blend membrane the adsorption capacity of metal ions increased. Among all parameters, pH has the most significant effect on the adsorption capacity, particularly in the range of 2.9-5.9. The increase in CS/PEG ratio was found to enhance the adsorption capacity of the membranes. The effects of initial concentration of metal ions on the extent of metal ions removal were investigated in detail. The experimental data were better fitted to Freundlich equation than Langmuir. In addition, it was found that the iron and manganese ions adsorbed on the membranes can be effectively desorbed in 0.1 mol/L HCl solution （up to 98% desorption efficiency） and the blend membranes can be reused almost without loss of the adsorption capacity for iron and manganese ions.

关键词： chitosan blend membrane iron and manganese ions adsorption

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Enhanced strength in novel nanocomposites prepared by reinforcing graphene in red soil and fly ash bricks

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International Journal of Minerals,Metallurgy and materials 2019年第10期26卷 1322-1328页

作者： Jit Sarkar D.K.Das department of metallurgical and materials Engineering Indian Institute of TechnologyKharagpur 721302West BengalIndia department of Mechanical Engineering Indian Institute of Technology(Indian School of Mines)Dhanbad 826004JharkhandIndia

Low-dimensional nanomaterials such as graphene can be used as a reinforcing agent in building materials to enhance the strength and durability. Common building materials burnt red soil bricks and fly ash bricks were reinforced with various amounts of graphene, and the effect of graphene on the strength of these newly developed nanocomposites was studied. The fly ash brick nanocomposite samples were cured as per their standard curing time, and the burnt red soil brick nanocomposite samples were merely dried in the sun instead of being subjected to the traditional heat treatment for days to achieve sufficient strength. The water absorption ability of the fly ash bricks was also discussed. The compressive strength of all of the graphene-reinforced nanocomposite samples was tested, along with that of some standard (without graphene) composite samples with the same dimensions, to evaluate the effects of the addition of various amounts of graphene on the compressive strength of the bricks.

关键词： graphene burnt red soil brick fly ash brick nanocomposites compressive strength

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