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Advanced Electro-active Dry Adhesive Actuated by an Artificial Muscle Constructed from an Ionic Polymer Metal Composite Reinforced with Nitrogen-doped Carbon Nanocages

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Journal of bionic Engineering 2017年第3期14卷 567-578页

作者： Qingsong He Xu Yang Zhongyuan Wang Jin Zhao Min Yu Zhen Hu Zhendong Dai Institute of bio-inspired Structure and Surface Engineering Jiangsu Provincial Key Laboratory of Bionic Functional Materials Col- lege of Astronautics Nanjing University of Aeronautics & Astronautics Nanjing 210016 China College of Mechanical and Electrical Engineering Nanjing University of Aeronautics & Astronautics Nanjing 210016 China Key laboratory of Mesoscopic Chemistry of MOE Jiangsu Provincial Lab for Nanotechnology School of Chemistry and Chemical Engineering Nanjing University Nanjing 210093 China

An advanced electro-active dry adhesive, which was composed of a mushroom-shaped tibrillar dry adhesive array actuated by an Ionic Polymer Metal Composite （IPMC） artificial muscle reinforced with nitrogen-doped carbon nanocages （NCNCs）, was developed to imitate the actuation of a gecko＇s toe. The properties of the NCNC-reinforced Nation membrane, the electro- mechanical properties of the NCNC-reinforced IPMC, and the related electro-active adhesion ability were investigated. The NCNCs were uniformly dispersed in the 0.1 wt% NCNC/Nafion membrane, and there was a seamless connection with no clear interface between the dry adhesive and the IPMC. Our 0.1 wt% NCNC/Nation-IPMC actuator shows a displacement and force that are 1.6 - 2 times higher than those of the recast Nafion-IPMC. This is due to the increased water uptake （25.39%） and tensile strength （24.5 MPa） of the specific 3D hollow NCNC-reinforced Nation membrane, as well as interactions between the NCNCs and the sulfonated groups of the Nation. The NCNC/Nation-IPMC was used to effectively actuate the mushroom-shaped dry adhesive. The normal adhesion forces were 7.85 raN, 12.1 mN, and 51.7 mN at sinusoidal voltages of 1.5 V, 2.5 V, and 3.5 V, respectively, at 0.1 Hz. Under the bionic leg trail, the normal and shear forces were approximately 713.5 mN （159 mN·cm^-2） and 1256.6 mN （279 mN·cm^-2）, respectively, which satisfy the required adhesion. This new electro-active dry adhesive can be applied for active, distributed actuation and flexible grip in robots.

关键词： electro-active dry adhesive bionic ionic polymer metal composite Nation membrane carbon nanocage

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Highly Transparent and Adhesive Poly(vinylidene difluoride)Films for Self-Powered Piezoelectric Touch Sensors

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Chinese Journal of Polymer Science 2022年第7期40卷 726-737页

作者： Qing-Qing Li Guang-Kuo Wang Zi-Xu Liang Zhi-Jun Hu School of Optoelectronic Science and Engineering&Collaborative Innovation Center of Suzhou Nano Science and Technology Soochow UniversitySuzhou215006China Center for Soft Condensed Matter Physics and Interdisciplinary Research Soochow UniversitySuzhou215006China Soochow University Key Lab of Advanced Optical Manufacturing Technologies of Jiangsu Province&Key Lab of Modern Optical Technologies of Education Ministry of ChinaSuzhou215006China

With the rapid development of internet of things,self-powered touch sensors made of piezoelectric fluorinated polymers have attracted significant interest because they can constantly convert mechanical energy into electrical energy without external power ***,it is still challenging to fabricate fluorinated polymer films with good adhesion and high output performance with a large-scale and low-cost method while maintaining high transparency,which are extremely important for simultaneous optical detection and electromechanical *** this work,we demonstrate that the incorporation of a molecular ferroelectric-dabcoHReO_(4)(DH)into poly(vinylidene difluoride)(PVDF)solution enables high-throughput and low-temperature processing of flexible and transparent piezoelectric films by scalable processing *** effects of multiaxial DH are ***,DH can trigger the phase transition of PVDF fromα-toβ-phase and realize the orderly orientation of PVDF,which guarantees higher piezoelectric performance without any additional electrical poling ***,the hydrophilic nature of DH can improve the adhesion properties of PVDF,which in turn improve the stability and durability of the *** optimizing the fabrication processes,the transmittance of the piezoelectric touch sensors based on PVDF films and Ag nanowires coated poly(ethylene terephthalate)electrodes can be higher than 94%.The piezoelectric voltage constant g;of the transparent films can reach to 1.2 V·m·N;,which is at least three times higher than the commercially available PVDF films obtained by *** results indicate that the flexible piezoelectric sensors have potential applications in transparent electronic devices for mechanical sensing and energy harvesting.

关键词： PVDF Transparent Adhesive Large scale Piezoelectric sensor

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Formation of Nanotubular Structures with Petal Effect by Soft-Template Electropolymerization of Benzotrithiophene with Hydrophilic Carboxyl Group

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Journal of bionic Engineering 2022年第4期19卷 1054-1063页

作者： Maroua Khodja Imen Bousrih Mejda El Kateb Mohammed Beji Frederic Guittard Thierry Darmanin laboratory of Structural Organic Chemistry Faculty of Sciences of Tunis University of Tunis El Manar2092 TunisTunisia NICE lab Universite Cote d’Azur06100 NiceFrance

The bioinspiration is one of the best ways to make a breakthrough in a field,and particularly in the wetting *** by natural species,such as rose petals and gecko foot,and previous researches,nanotubular structures are prepared here by soft-template electropolymerization in organic solvent and using an original benzotrithiophene with a hydrophilic carboxyl group,as the *** best results are obtained by cyclic voltammetry because of a much higher amount of gas bubbles released with this deposition *** nanoparticles and nanotubes are observed while the water content has an influence on the number of *** if the monomer has hydrophilic carboxyl group,the best films have both high hydrophobicity(apparent water contact angle up to 130.7°)and strong water adhesion(petal effect).These surfaces could be used in future in applications such as water harvesting systems.

关键词： bioinspired Electropolymerization Hydrophobicity Nanostructures Nanotubes Wettability

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High power impulse magnetron sputtering and its applications

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Plasma Science and Technology 2018年第6期20卷 52-68页

作者：袁燕杨丽珍刘忠伟陈强 lab.of Plasma Physics and Materials Beijing Institute of Graphic Communication

High power impulse magnetron sputtering（HiPIMS） has attracted a great deal of attention because the sputtered material is highly ionized during the coating process,which has been demonstrated to be advantageous for better quality ***,the mechanism of the HiPIMS technique has recently been *** this paper,the current knowledge of HiPIMS is *** focus on the mechanical properties of the deposited thin film in the latest applications,including hard coatings,adhesion enhancement,tribological performance,and corrosion protection layers.A description of the electrical,optical,photocatalytic,and functional coating applications are *** prospects for HiPIMS are also discussed in this work.

关键词： HiPIMS basic knowledge applications review

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Tough adhesion and antifouling poly(vinyl alcohol)hydrogel coating on the arch wire for antibacterial adhesion

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Science China(Technological Sciences) 2023年第10期66卷 2786-2796页

作者： LI MingWen TANG Chen YU XiXi SHI XinLei YU Hui YIN HaiYan YOU Min CHEN Qiang DING Xi Department of Stomatology The First Affiliated Hospital of Wenzhou Medical UniversityWenzhou 325000China Wenzhou Institute University of Chinese Academy of SciencesWenzhou 325001China Oujiang laboratory(Zhejiang lab for Regenerative Medicine Vision and Brain Health)Wenzhou 325000China

The arch wire(AW)plays an important role in providing continuous force,aligning the teeth,and excellent dental arch stability for orthodontic ***,the high friction performance of the AW surface can increase bacterial adhesion and colonization,leading to oral hygiene ***,a simple method is developed to modify the surface of the orthodontic wire with a poly(vinyl alcohol)(PVA)hydrogel coating,which can improve the lubricity and antibacterial adhesion of the AW and prevent the oral hygiene problems caused by *** PVA hydrogel coating can toughly adhere to the surface of the AW and remarkably reduce the friction performance of the AW,and then its friction coefficient in water can reach *** the action of brushing and bending,the PVA hydrogel coating possesses superior ultralubrication and hardly affects the mechanical properties of the stainless-steel ***,the PVA hydrogel coating can significantly inhibit bacterial adhesion on the surface of the AW,thereby reducing bacterial colonization and maintaining oral hygiene while correcting the shape of the mouth and ***,the PVA hydrogel coating exhibits tough adhesion and good antibacterial adhesion while maintaining the mechanical properties of the AW,and it is a promising antifouling coating for improving the performance of the AW.

关键词： orthodontic treatment arch wire hydrogel coating tough adhesion antifouling

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Thermodynamic prediction and experimental investigation of short-term dynamic membrane formation in dynamic membrane bioreactors:Effects of sludge properties

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Journal of Environmental Sciences 2019年第3期31卷 85-96页

作者： Zhenzhen Yu Yisong Hu Mawuli Dzakpasu Xiaochang C.Wang Key lab.of Northwest Water Resource Environment and Ecology MOE Xi'an University of Architecture and Technology International Science & Technology Cooperation Center for Urban Alternative Water Resources Development Key lab.of Environmental Engineering Shaanxi Province

In dynamic membrane bioreactors(DMBRs), a dynamic membrane(DM) forms on a support material to act as the separation membrane for solids and liquids. In this study, batch filtration tests were carried out in a DMBR using nylon mesh(25 μm) as support material to filtrate sludge suspensions of variable properties from three different sources to evaluate the effects on the short-term DM formation process(within 240 min). Furthermore, the extended Derjaguin–Landau–Verwey–Overbeek(XDLVO) theory was applied to analyze the sludge adhesion and cohesion behaviors on the mesh surface to predict quantitative parameters of the short-term DM formation process(including initial formation and maturation stage). The filtration results showed that the order of the initial DM formation time(permeate turbidity lability. Moreover, normal sludge(regarding settleability, dewaterability,flocculability, and extracellular polymeric substance) showed a more acceptable DM formation performance(short DM formation time, low permeate turbidity, and high permeate flux) than sludge with poor settleability, dewaterability and flocculability. The influence of sludge properties on the initial DM formation time corroborates the prediction of sludge adhesion behaviors by XDLVO theory. Additionally, the XDLVO calculation results showed that acid–based interaction, energy barrier, and secondary energy minimum were important determinants of the sludge adhesion and cohesion behaviors. Therefore, short-term DM formation process may be enhanced to achieve stable long-term DMBR operation through positive modification of the sludge properties.

关键词： Dynamic membrane bioreactor Dynamic membrane formation XDLVO theory Sludge properties Wastewater treatment

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Investigation on Viscoelasticity of Waterborne Polyurethane with Azobenzene-containing Pendant Groups under Ultraviolet and Visible-light Irradiation

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Chinese Journal of Polymer Science 2019年第12期37卷 1267-1272,I0007页

作者： Yi-Jun Liu Dong Liu Si-Han Li Hua-Qing Liang Fang-Ming Zhu GDHPPC lab School of ChemistrySun Yat-sen UniversityGuangzhou 510275China Key lab for Polymer Composite and Functional Materials of Ministry of Education School of ChemistrySun Yat-sen UniversityGuangzhou 510275China

In this study,a novel waterborne polyurethane(WPU)with azobenzene-containing(azo-containing)pendant groups was synthesized by isophorone diisocyanate,long-chain diol of polycaprolactone,2-ethyl-2-methyl-butanoic acid(2,2-dimethylolpropionic acid),10-(4-(phenyldiazenyl)phenoxy)decyl-3-hydroxy-2-(hydroxymethyl)-2-methylpropanoate,and N,N-diethyl-ethanamine(triethylamine).Moreover,the influence of ultraviolet and visible(UV-Vis)light irradiation on the viscoelasticity of azo-containing WPU film in terms of the reversible trans-cis photoisomerization of azo-containing pendant groups was investigated by UV-Vis light spectroscopy,atomic force microscopy,and dynamic thermomechanical *** results revealed that the adhesion of azo-containing WPU with single crystal silicon atomic force microscope probe was about 13 n N when irradiated by 450 nm Vis light for 60 s at 25°***,the adhesion increased to 82 n N after irradiation with 365 nm UV light for 60 s at 25°*** addition,the azo-containing WPU presented a photo-induced reversible transition of tensile modulus and tanδin the range from about 2 MPa to 22 MPa and 6000 to 0.35 with UV-Vis light cyclic irradiation for 120 s at 25°C,respectively.

关键词： Waterborne polyurethane Viscoelasticity Photoisomerization Azobenzene

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Regulation of substrate surface topography on differentiation of mesenchymal stem cells

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Acta Mechanica Sinica 2020年第5期36卷 1158-1169,I0004页

作者： Bo Huo Yang Zhao Xue Bai Qing Sun Fei Jiao biomechanics lab Department of MechanicsSchool of Aerospace EngineeringBeijing Institute of TechnologyBeijing 100081China

Mesenchymal stem pells(MSCs)have been extensively used in the field of tissue engineering and regenerative *** effect of surface properties on the differentiation of MSCs is a very important issue for the design and fabrication of scaffolds or *** review is mainly focused on the morphological or topographic characteristics of cell adhesion substrate,*** area and shape for individual cell,cell density and cell-cell contact for multiple cells,substrate roughnessridge width,micropillar height,nanoparticle diameter and aspect ratio of *** results from different studies were quantitativcly analyzed using comparable or unified parameters and definitions under the specific experimental conditions such as cell source,culture time,induction medium,matrix material and differentiation *** interesting phenomena and properties were discovered by this integrated and systematic analysis,which might give insights into the regulatory mechanism of surface morphology or topography on MSCs differentiation.

关键词： Mesenchymal stem cell adhesion morphology Surface topography Differentiation biomaterial

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Enhanced Compliant Adhesive Design and Fabrication with Dual-Level Hierarchical Structure

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Journal of bionic Engineering 2010年第3期7卷 228-234页

作者： Dan Sameoto Carlo Menon Department of Mechanical Engineering University of Alberta MENRVA lab School of Engineering ScienceSimon Fraser University

Synthetic dry adhesives inspired by the nano-and micro-scale hairs found on the feet of geckos and some spiders have beendeveloped for almost a decade. Elastomeric single level micro-scale mushroom shaped fibres are currently able to function evenbetter than natural dry adhesives on smooth surfaces under normal loading. However, the adhesion of these single level syntheticdry adhesives on rough surfaces is still not optimal because of the reduced contact surface area. In nature, contact area ismaximized by hierarchically structuring different scales of fibres capable of conforming surface roughness. In this paper, weadapt the nature’s solution arid propose a novel dual-level hierarchical adhesive design using Polydimethylsiloxane (PDMS),which is tested under peel loading at different orientations. A negative macro-scale mold is manufactured by using a laser cutterto define holes in a Poly(methyl methacrylate) (PMMA) plate. After casting PDMS macro-scale fibres by using the obtainedPMMA mold, a previously prepared micro-fibre adhesive is bonded to the macro-scale fibre substrate. Once the bondingpolymer is cured, the micro-fibre adhesive is cut to form macro scale mushroom caps. Each macro-fibre of the resulting hierarchicaladhesive is able to conform to loads applied in different directions. The dual-level structure enhances the peel strengthon smooth surfaces compared to a single-level dry adhesive, but also weakens the shear strength of the adhesive for a given areain contact. The adhesive appears to be very performance sensitive to the specific size of the fibre tips, and experiments indicatethat designing hierarchical structures is not as simple as placing multiple scales of fibres on top of one another, but can requiresignificant design optimization to enhance the contact mechanics and adhesion strength.

关键词： biomimetics dry adhesive hierarchical dual-level adhesive silicone polymer

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Arg-Gly-Asp(RGD)Modified biomimetic Polymeric Materials

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Journal of Materials Science & Technology 2005年第4期21卷 571-576页

作者： Xufeng NIU, Yuanliang WANG Yanfeng LUO Juan XIN Yonggang LI Key lab.of biomechanics & Tissue Engineering Ministry of Education Bioengineering College Chongqing University Chongqing400044 China

The new generation of biomaterials focuses on the design of biomimetic polymeric materials that are capable of eliciting specific cellular responses and directing new tissue formation. Since Arg-Gly-Asp （RGD） sequences have been found to promote cell adhesion in 1984, numerous polymers have been functionalized with RGD peptides for tissue engineering applications. This review gave the advance in RGD modified biomimetic polymeric materials,focusing on the mechanism of RGD, the surface and bulk modification of polymer with RGD peptides and the evaluation in vitro and in vivo of the modified biomimetic materials.

关键词： Arg-Gly-Asp (RGD) biomimetic materials Polymer

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