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Microstructure Features and the Macroscopic Acoustic Behavior of Gassy Silt in the Yellow River Delta

Journal of Ocean University of China 2024年第2期23卷 371-382页

作者： LIU Tao GUO Zhenqi ZHANG Yan WU Chen LIU Lele DENG Shenggui laboratory for Marine Geology Pilot National Laboratory for Marine Science and TechnologyQingdao 266061China Shandong Provincial key laboratory of Marine Environment and Geological Engineering Ocean University of ChinaQingdao 266100China College of Civil Engineering Anhui Jianzhu UniversityHefei 230601China The key laboratory of Gas Hydrate Ministry of Natural ResourcesQingdao Institute of Marine GeologyQingdao 266071China College of Marine Geosciences Key Laboratory of Submarine Geosciences and ProspectingOcean University of ChinaQingdao 266100China

The morphological changes in isolated bubbles in gassy silt play a critical role in the microscopic structures between soil particles and bubbles and macroscopic physical *** on X-ray CT scanning experiments under various vertical loads(four levels),self-designed acoustic macro experiments,and a series of formula revisions to the macro-air-bearing silt sound-velocity prediction model,this paper discusses the macro-and micro-scale features of gassy silts from the Yellow River *** samples consisted of different proportions of silt from the Yellow River Delta and porous media,and they were used to form two types of aerosol silts with initial gas contents of 4.23%and 7.67%.The results show that the air bubble content and external load considerably affect the microstructural parameters and acoustic behavior of gassy silt in the Yellow River *** macroscopic sound velocity showed a linear positive correlation with vertical load and relation to microstructural parameters in varying manners and *** on the traditional Biot-Stoll acoustic model,the gas-phase medium coefficient was introduced for the proper calculation and prediction of the sound velocity of air-bearing *** errors of the overall prediction varied between 5.6%and 9.6%.

关键词： gassy silt vertical load microstructure parameters bubble vibration Biot-Stoll acoustic model

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Clay mineral transformation in medium–high maturity shale oil reservoir: a case study of the Qingshankou Formation， Songliao Basin， Northeast China

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Journal of Earth Science 2024年

作者： Xinping Liang Xueyu Yao Rukai Zhu Xiaojun Wang Zhijun Jin Changrong Li Institute of Energy， Peking University State key laboratory of Shale Oil and Gas Enrichment Mechanisms and Effective Development College of Geosciences/National key laboratory of petroleum resources and Engineering， China University of petroleum (Beijing) Research Institute of petroleum exploration & Development PetroChina petroleum Exploration and Production Research Institute SINOPEC

Currently， significant hurdles lie ahead in China’s lacustrine shale oil exploration and exploitation， particularly due to the high clay mineral content， which severely impacts pore development in organic-rich shales. In this study， we take the medium- to high-maturity shale of the Qingshankou Formation (K2qn) in the Gulong Sag， Songliao Basin， China， as an example and analyze the dynamic evolution of the clay minerals and their effects on pore development by core observations， scanning electron microscopy， X-ray diffraction， physical property and nitrogen adsorptions to provide a valuable reference for the effective evaluation of lacustrine clay-rich shale oil reservoirs. Our findings reveal that the dynamic transformation of clay minerals in the Qingshankou Formation is classified into three stages based on diagenesis， thermal maturity， and mineral characteristics: the initial stage (vitrinite reflectivity (Ro) 1.3%). Clay minerals play crucial roles in controlling shale reservoirs during the rapid transformation process， which is evidenced by the formation of shrinkage fractures， enhanced pore connectivity， increased porosity， and expanded space for shale oil adsorption and storage. In addition， authigenic quartz can form during the transformation of clay minerals， contributing to increased reservoir brittleness and improving the potential for reservoir fracturing.

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Dynamic Location Method for Shallow Ocean Bottom Nodes Using the Levenberg-Marquart Algorithm

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Journal of Ocean University of China 2024年第4期23卷 953-960页

作者： TONG Siyou LI Junjie XU Xiugang FANG Yunfen WANG Zhongcheng key laboratory of Submarine Geosciences and prospecting Techniques MOEOcean University of ChinaQingdao 266100China laboratory for Marine Mineral resources Qingdao Marine Science and Technology CenterQingdao 266237China R&D Center of BGP CNPCZhuozhou 072751China Insitute of Shengli Oilfield SINOPECDongying 257022China

Ocean bottom node(OBN)data acquisition is the main development direction of marine seismic exploration;it is widely promoted,especially in shallow sea ***,the OBN receivers may move several times because they are easily affected by tides,currents,and other factors in the shallow sea environment during long-term *** uncorrected,then the imaging quality of subsequent processing will be *** conventional secondary positioning does not consider the case of multiple movements of the receivers,and the accuracy of secondary positioning is *** first arrival wave of OBN seismic data in shallow ocean mainly comprises refracted *** this study,a nonlinear model is established in accordance with the propagation mechanism of a refracted wave and its relationship with the time interval curve to realize the accurate location of multiple receiver *** addition,the Levenberg-Marquart algorithm is used to reduce the influence of the first arrival pickup error and to automatically detect the receiver movements,identifying the accurate dynamic relocation of the *** simulation and field data show that the proposed method can realize the dynamic location of multiple receiver movements,thereby improving the accuracy of seismic imaging and achieving high practical value.

关键词： OBN dynamic location method Levenberg-Marquart algorithm seismic exploration of shallow sea

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Evolution and Application of Sealing Ability of Gypsum Caprocks under Temperature-Pressure Coupling:An Example of the ZS5 Well in the Tazhong Area of the Tarim Basin

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Acta Geologica Sinica(English Edition) 2024年第1期98卷 168-184页

作者： LIU Hua ZHAO Shan YANG Xianzhang ZHU Yongfeng WANG Shen ZHANG Ke National key laboratory of Deep Oil and Gas China University of Petroleum(East China)QingdaoShandong 266580China School of Geosciences China University of Petroleum(East China)QingdaoShandong 266580China laboratory for Marine Mineral resources National Laboratory for Marine Science and TechnologyQingdaoShandong 266071China PetroChina Tarim Oil Field Company KorlaXinjiang 841001China

Gypsum caprocks'sealing ability is affected by temperature-pressure *** to the limitations of experimental conditions,there is still a lack of triaxial stress-strain experiments that simultaneously consider changes in temperature and pressure conditions,which limits the accuracy of the comprehensive evaluation of the brittle plastic evolution and sealing ability of gypsum rocks using temperature pressure *** stress-strain tests were utilized to investigate the differences in the evolution of the confinement capacity of gypsum rocks under coupled temperaturepressure action and isothermal-variable pressure action on the basis of sample feasibility *** to research,the gypsum rock's peak and residual strengths decrease under simultaneous increases in temperature and pressure over isothermal pressurization experimental conditions,and it becomes more *** reduces the amount of time it takes for the rock to transition from brittle to *** temperature is taken into account,both the brittle–plastic transformation's depth limit and the lithological transformation of gypsum rocks become shallower,and the evolution of gypsum rocks under variable temperature and pressure conditions is more complicated than that under isothermal *** sealing ability under the temperature-pressure coupling is more in line with the actual geological context when the application results of the Well#ZS5 are *** provides a theoretical basis for precisely determining the process of hydrocarbon accumulation and explains why the early hydrocarbon were not well preserved.

关键词： temperature-pressure coupling gypsum caprocks brittle-plastic evolution sealing capacity Tarim Basin

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Micromechanism and mathematical model of stress sensitivity in tight reservoirs of binary granular medium

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petroleum Science 2024年第3期21卷 1780-1795页

作者： Jian-Bang Wu Sheng-Lai Yang Qiang Li Kun Yang Can Huang Dao-Ping Lv Wei Zhou State key laboratory of petroleum resources and Engineering China University of Petroleum(Beijing)Beijing2249China Laboratoire de G eologie Ecole Normale Sup erieure/CNRS UMR8538PSL Research UniversityParis75005France Research Institute of Exploration and Development Xinjiang Oilfield CompanyKaramay834000XinjiangChina

Research on reservoir rock stress sensitivity has traditionally focused on unary granular structures,neglecting the binary nature of real reservoirs,especially tight *** the stresssensitive behavior and mathematical characterization of binary granular media remains a challenging *** this study,we conducted online-NMR experiments to investigate the permeability and porosity evolution as well as stress-sensitive control mechanisms in tight sandy conglomerate *** results revealed stress sensitivity coefficients between 0.042 and 0.098 and permeability damage rates ranging from 65.6%to 90.9%,with an average pore compression coefficient of 0.0168—0.0208 MPa ***-scale compression occurred in three stages:filling,compression,and compaction,with matrix pores playing a dominant role in pore *** stress sensitivity of binary granular media was found to be influenced by the support structure and particle *** stress sensitivity was associated with small fine particle size,high fines content,high uniformity coefficient of particle size,high plastic deformation,and low Young's ***-supported samples exhibited a high irreversible permeability damage rate(average=74.2%)and stress sensitivity coefficients(average=0.089),with pore spaces more *** contrast,grain-supported samples showed low stress sensitivity coefficients(average=0.021)at high stress *** on the experiments,we developed a mathematical model for stress sensitivity in binary granular media,considering binary granular properties and nested interactions using Hertz contact deformation and Poiseuille *** describing the change in activity content of fines under stress,we characterized the non-stationary state of compressive deformation in the binary granular structure and classified the reservoir into three *** model was applied for production prediction using actual data from the Mahu reservoir in China,showing that the e

关键词： Stress sensitivity Binary granular medium Tight reservoir Online-NMR Reservoir energy retention rate

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Thermal and exhumation history of the Songnan Low Uplift,Qiongdongnan Basin:constraints from the apatite fission-track and zircon(U-Th)/He thermochronology

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Acta Oceanologica Sinica 2024年第4期43卷 40-49页

作者： Xiaoyin Tang Kaixun Zhang Shuchun Yang Shuai Guo Xinyan Zhao Zhizhao Bai Institute of Geomechanics Chinese Academy of Geological SciencesBeijing 100081China key laboratory of Paleomagnetism and Tectonic Reconstruction Ministry of Natural ResourcesBeijing 100081China key laboratory of petroleum Geomechanics China Geological SurveyBeijing 100081China China National Offshore Oil Corporation(CNOOC)Research Center Beijing 100028China

Significant advancements have been made in the study of Mesozoic granite buried hills in the Songnan Low Uplift(SNLU)of the Qiongdongnan *** findings indicate that the bedrock buried hills in this basin hold great potential for *** samples taken from the granite buried hills in the SNLU were analyzed using apatite fission track(AFT)and zircon(U-Th)/He data to unravel the thermal history of the basement *** information is crucial for understanding the processes of exhumation and alteration that occurred after its *** modeling of a sample from the western bulge of the SNLU revealed a prolonged cooling event from the late Mesozoic to the Oligocene period(~80-23.8 Ma),followed by a heating stage from the Miocene epoch until the present(~23.8 Ma to present).In contrast,the sample from the eastern bulge experienced a more complex thermal *** underwent two cooling stages during the late Mesozoic to late Eocene period(~80-36.4 Ma)and the late Oligocene period(~30-23.8 Ma),interspersed with two heating phases during the late Eocene to early Oligocene period(~36.4-30 Ma)and the Miocene epoch to recent times(~23.8-0 Ma),*** differences in exhumation histories between the western and eastern bulges during the late Eocene to Oligocene period in the SNLU can likely be attributed to differences in fault *** typical passive continental margin basins,the SNLU has experienced accelerated subsidence after the rifting phase,which began around 5.2 Ma *** possible mechanism for this abnormal post-rifting subsidence may be the decay or movement of the deep thermal source and the rapid cooling of the ***-term and multi-episodic cooling and exhumation processes play a key role in the alteration of bedrock and contribute to the formation of *** the other hand,rapid post-rifting subsidence(sedimentation)promotes the formation of cap rocks.

关键词： granite buried hills (U-Th)/He dating fission-track dating exhumation Songnan Low Uplift

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New potential barite reference materials for LA-MC-ICP-MS sulfur isotope analysis with application to hydrothermal barite in the Huayangchuan deposit， western China

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Journal of Earth Science 2024年

作者： Jiali Fu Xinqian He Zhaochu Hu Shuo Yin Jian Ma Kaiyun Chen Wen Zhang National key laboratory of prospecting， Mining and Remote Sense Detecting on Uranium resources， East China University of Technology State key laboratory of Nuclear resources and Environment， East China University of Technology School of Earth Sciences， East China University of Technology State key laboratory of Geological Processes and Mineral resources， China University of Geosciences Wuhan State key laboratory of Continental Dynamics， Department of Geo logy， Northwest University

Sulfur isotopes of S-bearing materials are powerful tools to trace various geological processes and sulfur sources in earth sciences， especially in ore deposits where sulfide-sulfate pair coprecipitates widely. However， in-situ S isotope determination of barite is challenging without natural matrix-matched reference material. In this study， we present two natural barite reference materials （1-YS and 294-YS） for in-situ sulfur isotopic analysis. Independent LA-MC-ICP-MS laboratories were utilized to test the δ34S micron-scale homogeneity of 1-YS and 294-YS barites that have 2s repeatabilities of better than ±0.45 ‰ and ±0.41 ‰， respectively. Meanwhile， the in-situ analysis results are consistent with the results of the bulk analysis by GS-IRMS within uncertainty. The grand mean δ34S values of 1-YS （13.37‰ ± 0.42 ‰， 2s） and 294-YS （14.38‰ ± 0.44 ‰， 2s） are the final recommended values obtained from four independent laboratories. All the results confirm the suitability of 1-YS and 294-YS barite used as calibration materials with respect to in-situ S isotopic analysis. Moreover， the new developed barite reference materials were used as matrix-matched standard to calibrate the barite samples from the Huayangchuan carbonatite-hosted U-polymetallic deposit （Qinling orogenic belt， western China） to obtain δ34S values. Utilizing the temperature-dependent δ34S fractionation of barite-pyrite pair， we calculate the formation temperature of barite （i.e.， 506 to 537 ℃） and the δ34S value of mineralizing fluid （i.e.， -7.11‰ to -7.59 ‰） in the Huayangchuan deposit. The results indicate an involvement of sedimentary sulfur， presumably acting as a potential uranium source （e.g.， upper crustal materials） for the giant Huayangchuan deposit.

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Impact of volcanism on the formation and hydrocarbon generation of organic-rich shale in the Jiyang Depression, Bohai Bay Basin, China

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petroleum Science 2024年第3期21卷 1539-1551页

作者： Jia-Hong Gao Xin-Ping Liang Zhi-Jun Jin Quan-You Liu Chang-Rong Li Xiao-Wei Huang Ju-Ye Shi Peng Li State key laboratory of Shale Oil and Gas Enrichment Mechanisms and Efficient Development Institute of EnergyPeking University petroleum Exploration and Production Research Institute SINOPECBeijing100871 China School of Energy resources China University of Geosciences Beijing100083 China

Globally,most organic-rich shales are deposited with volcanic ash *** ash,a source for many sedimentary basins,can affect the sedimentary water environment,alter the primary productivity,and preserve the organic matter(OM)through physical,chemical,and biological *** an increasing number of breakthroughs in shale oil exploration in the Bohai Bay Basin in recent years,less attention has been paid to the crucial role of volcanic impact especially its influence on the OM enrichment and hydrocarbon ***,we studied the petrology,mineralogy,and geochemical characteristics of the organic-rich shale in the upper submember of the fourth member(Es_(4)^(1))and the lower submember of the third member(Es_(3)^(3))of the Shahejie Formation,aiming to better understand the volcanic impact on organic-rich shale *** results show that total organic carbon is higher in the upper shale intervals rich in volcanic ash with enriched light rare earth elements and moderate Eu *** indicates that volcanism promoted OM formation before or after the *** positive correlation between Eu/Eu*and Post-Archean Australian Shale indicates hydrothermal activity before the volcanic *** plane graph of the hydrocarbon-generating intensity(S1+S2)suggests that the heat released by volcanism promoted hydrocarbon ***,the nutrients carried by volcanic ash promoted biological blooms during Es_(4)^(1 )and Es_(3)^(3) deposition,yielding a high primary *** blooms consume large amounts of oxygen and form anoxic environments conducive to the burial and preservation of ***,this study helps to further understand the organic-inorganic interactions caused by typical geological events and provides a guide for the next step of shale oil exploration and development in other lacustrine basins in China.

关键词： Volcanic ash Hydrocarbon generation Organic-rich shale Shahejie Formation Jiyang Depression

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Geochemical Characteristics and Hydrocarbon Generation Modeling of the Paleocene Source Rocks in the Jiaojiang Sag,East China Sea Basin

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Journal of Earth Science 2024年第2期35卷 642-654页

作者： Chuang Lei Shiyan Yin Jiaren Ye Jingfu Wu Zhaosheng Wang Bin Gao Collaborative Innovation Center of Green Development and Ecological Restoration of Mineral resources North China University of Science and TechnologyTangshan063210China key laboratory of Tectonics and petroleum resources China University of GeosciencesMinistry of EducationWuhan430074China CNOOC Research Institute Ltd Beijing100028China

Jiaojiang sag in the East China Sea Basin is at the earlier exploration stage,where characterizing hydrocarbon generation of source rocks is important to understand oil-gas exploration *** geochemical and basin modeling analysis,hydrocarbon generation capacity and process of the Paleocene E_(1)y,E_(1)l and E_(1)m formations were *** show that E_(1)y and E_(1)l mudstones are high-quality source rocks with Type Ⅱ kerogen,which is dominated by both aquatic organisms and terrestrial higher plants deposited in sub-reduced environment.E_(1)m mudstone interbedded with thin carbonaceous mudstone and coal is poor-quality source rock with Type Ⅲ kerogen,whose organic matter was originated from terrestrial higher plants under oxidized *** by burial and maturity histories,E_(1)y and E_(1)l source rocks experienced two hydrocarbon generation stages,which took place in the Late Paleocene and in the Middle to Late Eocene,respectively,and had high hydrocarbon generation capacity with cumulative hydrocarbon volume of 363 and 328 mg/g,respectively.E_(1)m source rock only had one hydrocarbon generation process in the Late Eocene,which had low hydrocarbon generation capacity with cumulative hydrocarbon volume of only 24 mg/*** future oil-gas exploration in the Jiaojiang sag should focus on hydrocarbon generation center and select targets in the central uplift formed before the Miocene with high-quality traps.

关键词： East China Sea Basin Jiaojiang sag source rock geochemical characteristics hydrocarbon generation basin modeling petroleum geology

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The mechanisms of thermal solidification agent promoting steam diversion in heavy oil reservoirs

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petroleum Science 2024年第3期21卷 1902-1914页

作者： Zhan-Xi Pang Qian-Hui Wang Qiang Meng Bo Wang Dong Liu State key laboratory of petroleum resources and Engineering China University of Petroleum(Beijing)Beijing102249China Liaohe Oilfield Institute CNPC ChinaPanjin124000LiaoningChina Henan Oilfield Institute Sinopec ChinaNanyang473400HenanChina Tianjin Branch of China National Offshore Oil Company(CNOOC)Ltd. Tianjin300452China

At high cycles of steam huff&puff,oil distribution in reservoirs becomes stronger heterogeneity due to steam *** solidification agent can be used to solve this *** solution is a lowviscosity liquid at normal temperature,but it can be solidified above 80℃.The plugging degree is up to 99%at 250℃.The sweep efficiency reaches 59.2%,which is 7.3%higher than pure steam *** addition,simultaneous injection of viscosity reducer and/or nitrogen foams can further enhance oil *** mechanism of this technology depends on its strong plugging ability,which changes the flowing pattern of steam to effectively mobilize remaining *** reducer and nitrogen foams further expand the sweep range and extends the effective ***,thermal solidification agent can plug steam channeling paths and adjust steam flowing direction to significantly enhance oil recovery at high cycles of steam huff&puff.

关键词： Heavy oil reservoir Steam huff&puff Steam channeling Steam diversion Plugging performance Mechanism analysis

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