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Hybrid model for BOF oxygen blowing time prediction based on oxygen balance mechanism and deep neural network

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International Journal of Minerals,Metallurgy and Materials 2024年第1期31卷 106-117页

作者： Xin Shao Qing Liu Zicheng Xin Jiangshan Zhang Tao Zhou Shaoshuai Li State key laboratory of advanced Metallurgy University of Science and Technology BeijingBeijing 100083China Engineering Research Center of MES Technology for iron&steel Production Ministry of EducationBeijing 100083China Laiwu iron and steel Group Yinshan Section steel Co. Ltd.Jinan 271104China

The amount of oxygen blown into the converter is one of the key parameters for the control of the converter blowing process,which directly affects the tap-to-tap time of converter. In this study, a hybrid model based on oxygen balance mechanism (OBM) and deep neural network (DNN) was established for predicting oxygen blowing time in converter. A three-step method was utilized in the hybrid model. First, the oxygen consumption volume was predicted by the OBM model and DNN model, respectively. Second, a more accurate oxygen consumption volume was obtained by integrating the OBM model and DNN model. Finally, the converter oxygen blowing time was calculated according to the oxygen consumption volume and the oxygen supply intensity of each heat. The proposed hybrid model was verified using the actual data collected from an integrated steel plant in China, and compared with multiple linear regression model, OBM model, and neural network model including extreme learning machine, back propagation neural network, and DNN. The test results indicate that the hybrid model with a network structure of 3 hidden layer layers, 32-16-8 neurons per hidden layer, and 0.1 learning rate has the best prediction accuracy and stronger generalization ability compared with other models. The predicted hit ratio of oxygen consumption volume within the error±300 m^(3)is 96.67%;determination coefficient (R^(2)) and root mean square error (RMSE) are0.6984 and 150.03 m^(3), respectively. The oxygen blow time prediction hit ratio within the error±0.6 min is 89.50%;R2and RMSE are0.9486 and 0.3592 min, respectively. As a result, the proposed model can effectively predict the oxygen consumption volume and oxygen blowing time in the converter.

关键词： basic oxygen furnace oxygen consumption oxygen blowing time oxygen balance mechanism deep neural network hybrid model

Modeling of LF refining process:a review

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Journal of iron and steel Research International 2024年第2期31卷 289-317页

作者： Zi-cheng Xin Jiang-shan Zhang Kai-xiang Peng Jun-guo Zhang Chun-hui Zhang Qing Liu State key laboratory of advanced Metallurgy University of Science and Technology BeijingBeijing100083China School of Automation and Electrical Engineering University of Science and Technology BeijingBeijing100083China Tangshan Branch Hebei Iron and Steel Co.Ltd.Tangshan063000HebeiChina Xinjiang Bayi iron and steel Co. Ltd.Baosteel GroupWulumuqi830022XinjiangChina

With the increasing demand for energy conservation and emission reduction,more attentions have been paid to the intelligentization,greenization and low carbonization during the transformation and upgrading of steelmaking *** furnace(LF)refining is one of the key procedures in steelmaking process and has been widely used in steelmaking plants for its high equipment matching degree,low equipment investment and outstanding refining *** to the main tasks of LF refining process,the modeling methods of temperature prediction model,slag-making model,alloying model,argon blowing model and model of inclusions behavior were systematically reviewed,and the advantages and disadvantages of each modeling method were *** addition,the technical framework for the future has also been proposed based on existing works,including classification of raw materials,graphic representation of knowledge,introduction,upgradation and management of device/equipment,customization of steelmaking,modeling of refining process,synergy of models,intelligentization of decision-making,automation of control,and digitization of processes and operations,aiming to provide a reference for the modeling and intelligent development of LF refining process.

关键词： LF refining Temperature prediction Slag-making Alloying Argon blowing Inclusion behavior Modeling method

Particle size dependence of the microsegregation and microstructure in the atomized Ni-based superalloy powders:Theoretical and experimental study

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Journal of Materials Science & Technology 2024年第4期171卷 54-65页

作者： Jikang Li Mingsheng Yang Yunfei Cai Yuanyuan Zhang Qingshuai Feng Jiantao Liu Tong Liu key laboratory of Aerospace Materials and Performance(Ministry of Education)School of Materials Science and Engineering Beihang UniversityBeijing 100191China Central iron and steel Research Institute Beijing 100081China

The microstructure and microsegregation of atomized powder,which depend on their sizes,are of great importance to the mechanical properties of the consolidated bulk ***,it is necessary to reveal the relationship between particle size and powder *** effects of particle size on the so-lidification characterization of the atomized Ni-based superalloy powders were studied via finite element *** on the simulations,a model was developed to predict the microsegregation and mi-crostructure of atomized powders with different sizes and study the influence of thermal history on the powder attributes during the atomization *** radiation heat transfer and temperature gradi-ent within the rapid solidification alloy powders were taken into account in this *** validating the accuracy of the model,the predictions of the present model were compared with the microsegregation and microstructure of the specific size powder close to the screen mesh *** results showed that mi-crostructure depended primarily on the temperature gradient within the powder,while the solidification rate had a more significant effect on the *** model predicted microstructure features in agreement with the experiment,and for microsegregation,the deviations of prediction for most ele-ments were less than 10%.This work provides a new model to precisely predict the microsegregation and microstructure of the atomized alloy powders and sets a foundation to control the powder features for various engineering applications.

关键词： Particle size Solidification microstructure Microsegregation Numerical simulation

Boron promoted Fe^(3+)/peracetic acid process for sulfamethazine degradation:Efficiency,role of boron,and identification of the reactive species

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Journal of Environmental Sciences 2024年第1期135卷 72-85页

作者： Yanhong Zhang Guangbing Liu Yuzhu Xue Lichun Fu Yawei Qian Minhui Hou Xiang Li Chen Ling Ying Zhang Yuwei Pan Jiangsu Provincial key laboratory of Environmental Engineering Jiangsu Provincial Academy of Environmental ScienceNanjing 210036China College of Biology and the Environment Nanjing Forestry UniversityNanjing 210037China School of iron and steel Soochow UniversitySuzhou 215000China School of the Environment Nanjing UniversityNanjing 210023China SUMEC Complete Equipment&Engineering Co. LTD.Nanjing 211500China key laboratory of Pollution process and Environmental Criteria Ministry of EducationCollege of Environmental Science and EngineeringNankai UniversityTianjin 300350China School of Environment Key Laboratory for Yellow River and Huai River Water Environmental and Pollution ControlMinistry of EducationHenan Key Laboratory for Environmental Pollution ControlHenan Normal UniversityXinxiang 453007China

In this work,boron(B)was used to promote Fe^(3+)/peracetic acid(Fe^(3+)/PAA)for the degradation of sulfamethazine(SMT).An SMT degradation efficiency of 9.1%was observed in the Fe^(3+)/PAA system over 60 min,which was significantly increased to 99.3%in the B/Fe^(3+)/PAA system over 10 *** B/Fe^(3+)/PAA process also exhibited superior resistance to natural substances,excellent adaptability to different harmful substances,and good removal of antibiotics in natural fresh water *** mechanism of action of boron for Fe^(3+)reduction was determined using scanning electron microscopy(SEM),X-ray photoelectron spectroscopy(XPS),Fourier transform infrared(FT-IR)spectroscopy,density functional theory(DFT)calculations,and electrochemical *** dominant role of^(·)OH was confirmed using quenching experiments,electron spin resonance(EPR)spectroscopy,and quantitative *** radicals(R-O^(·))and Fe(IV)also significantly contribute to the removal of *** calculations on the reaction between Fe^(2+)and the PAA were conducted to further determine the contribution from ^(·)OH,R-O^(·),and Fe(IV)from the perspective of thermodynamics and the reaction *** boron dosages,Fe^(3+)dosages,and initial pH values were also investigated in the B/Fe^(3+)/PAA system to study their effect of SMT removal and the production of the reactive ***(IV)production determined the k_(R-O·+Fe(IV))value suggesting that Fe(IV)may play a more important role than R-O^(·).A comparison of the results with other processes has also proved that the procedure described in this study(B/Fe^(3+)/PAA)is an effective method for the degradation of antibiotics.

关键词： Boron Peracetic acid Sulfamethazine DFT Reactive species

Coke behavior with H_(2)O in a hydrogen-enriched blast furnace:A review

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International Journal of Minerals,Metallurgy and Materials 2024年第5期31卷 959-976页

作者： Feng Zhou Daosheng Peng Kejiang Li Alberto N.Conejo Haotian Liao Zixin Xiong Dongtao Li Jianliang Zhang School of Metallurgical and Ecological Engineering University of Science and Technology BeijingBeijing 100083China School of Chemical Engineering The University of QueenslandSt LuciaQLD 4072Australia Baosteel Central Research Institute(R&D Center of Wuhan iron&steel Co. Ltd.)Wuhan 430080China Shougang Research Institute of Technology Shougang Group Corporation Ltd.Beijing 100043China Beijing key laboratory of Green Recyclable process for iron and steel Production Technology Beijing 100043China

Hydrogen-enriched blast furnace ironmaking has become an essential route to reduce CO_(2)emissions in the ironmaking ***,hydrogen-enriched reduction produces large amounts of H_(2)O,which places new demands on coke quality in a blast *** a hydrogen-rich blast furnace,the presence of H_(2)O promotes the solution loss *** result improves the reactivity of coke,which is 20%-30%higher in a pure H_(2)O atmosphere than in a pure CO_(2)*** activation energy range is 110-300 kJ/mol between coke and CO_(2)and 80-170 kJ/mol between coke and H_(2)***_(2)and H_(2)O are shown to have different effects on coke degradation *** review provides a comprehensive overview of the effect of H_(2)O on the structure and properties of *** exploring the interactions between H_(2)O and coke,several unresolved issues in the field requiring further research were *** review aims to provide valuable insights into coke behavior in hydrogen-rich environments and promote the further development of hydrogen-rich blast furnace ironmaking processes.

关键词： hydrogen ironmaking coke behavior blast furnace gasification microstructure kinetics

Uncovering Microstructure-Property Relationship in Ni-Alloyed Fe-Mn-Al-C Low-Density steel Treated by Hot-Rolling and Air-Cooling process

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Acta Metallurgica Sinica(English Letters) 2024年第4期37卷 713-725页

作者： Xiaoliang Jia Guhui Gao Xiaolu Gui Chun Feng R.D.K.Misra Bingzhe Bai School of Mechanical Electronicand Control EngineeringBeijing Jiaotong UniversityBeijing100044China CNPC Tubular Goods Research Institute Xi’an710077China laboratory for Excellence in advanced steel Research University of Texas at El PasoEl PasoTX79968-0521USA School of Material Science and Engineering Key Laboratory of Advanced Materials of Ministry of EducationTsinghua UniversityBeijing100084China

This paper focuses on the relationship between the microstructure and tensile properties of Fe-Mn-Al-C low-density high-strength steel processes by hot-rolling and air-cooling process. The microstructure analysis reveals that the combination of hot-rolling and air-cooling results in the formation of heterogeneous structures comprising different-sized γ and B_(2) phases in the low-density steel with the addition of nickel (Ni). The addition of Ni promotes the formation of the B_(2) phase and induces the pinning of B_(2) phase particles at the γ grain boundaries. This pinning effect effectively hinders the growth of the γ grains, leading to grain refinement. The tensile test results demonstrate that LDS-5Ni (low-density steel, LDS) exhibits excellent high strength and ductility combination, e.g., a tensile strength of 1535 MPa, yield strength of 1482 MPa, and elongation of 23.3%. These remarkable mechanical properties are primarily attributed to the combined strengthening contributions of grain refinement and duplex nano-sized second-phase precipitation hardening.

关键词： Low-density steel Microstructure B_(2)phase κ-Carbide Tensile properties

Ti_(3)C_(2)T_(x) MXene/carbon composites for advanced supercapacitors:Synthesis,progress,and perspectives

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Carbon Energy 2024年第2期6卷 113-142页

作者： Yanqing Cai Xinggang Chen Ying Xu Yalin Zhang Huijun Liu Hongjuan Zhang Jing Tang College of Materials Science and Engineering North China University of Science and TechnologyTangshanChina Hebei iron and steel laboratory North China University of Science and TechnologyTangshanChina Songshan Lake Materials laboratory DongguanChina Shanghai key laboratory of Green Chemistry and Chemical processes School of Chemistry and Molecular EngineeringEast China Normal UniversityShanghaiChina State key laboratory of Petroleum Molecular and process Engineering(SKLPMPE) Sinopec Research Institute of Petroleum Processing Co.Ltd.BeijingChina Institute of Eco-Chongming ShanghaiChina

MXenes are a family of two-dimensional(2D)layered transition metal carbides/nitrides that show promising potential for energy storage applications due to their high-specific surface areas,excellent electron conductivity,good hydrophilicity,and tunable *** various types of MXenes,Ti_(3)C_(2)T_(x) is the most widely studied for use in capacitive energy storage applications,especially in supercapacitors(SCs).However,the stacking and oxidation of MXene sheets inevitably lead to a significant loss of electrochemically active *** overcome such challenges,carbon materials are frequently incorporated into MXenes to enhance their electrochemical *** review introduces the common strategies used for synthesizing Ti_(3)C_(2)T_(x),followed by a comprehensive overview of recent developments in Ti_(3)C_(2)T_(x)/carbon composites as electrode materials for ***_(3)C_(2)T_(x)/carbon composites are categorized based on the dimensions of carbons,including 0D carbon dots,1D carbon nanotubes and fibers,2D graphene,and 3D carbon materials(activated carbon,polymer-derived carbon,etc.).Finally,this review also provides a perspective on developing novel MXenes/carbon composites as electrodes for application in SCs.

关键词： electrochemical performance MXene/carbon composites supercapacitors

Experimental and simulation research on hollow AZ31 magnesium alloy three-channel joint by hot extrusion forming with sand mandrel

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Journal of Magnesium and Alloys 2024年第1期12卷 98-109页

作者： Shi Shengnan Wang Hongyu Teng Fei Jiang Lei Sun Juncai Sun Jie Zhang Shunhu Transportation Engineering College Dalian Maritime UniversityDalianLiaoning 106026China State key laboratory of Rolling and Automation Northeastern UniversityShenyangLiaoning 110819China Shagang School of iron and steel Soochow UniversitySuzhouJiangsu 215021China

Magnesium alloy is one of the lightest metal structural *** weight is further reduced through the hollow ***,the hollow structure is easily damaged during *** order to maintain the hollow structure and to transfer the stresses during the high temperature deformation,the sand mandrel is *** this paper,the hollow AZ31 magnesium alloy three-channel joint is studied by hot extrusion *** as one of solid granule medium is used to fill the hollow magnesium *** extrusion temperatures are 230℃ and 300℃,*** process parameters(die angle,temperature,bottom thickness,sidewall thickness,edge-to-middle ratio in bottom,bottom shape)of the hollow magnesium alloy are analyzed based on the results of experiments and the finite element *** results are shown that the formability of the hollow magnesium alloy will be much better when the ratio of sidewall thickness to the bottom thickness is 1:*** when edge-to-middle ratio in bottom is about 1:1.5,a better forming product can be *** best bottom shape in these experiments will be convex based on the forming *** grain will be refined obviously after the *** the microstructures will be shown as *** these lines will be well agreement with the mold in the corner.

关键词： AZ31 magnesium alloy Three-channel joint Sand Experiments and the finite element Die angle

Development and prospects of molten steel deoxidation in steelmaking process

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International Journal of Minerals,Metallurgy and Materials 2024年第1期31卷 18-32页

作者： Zhongliang Wang Yanping Bao State key laboratory of advanced Metallurgy University of Science and Technology BeijingBeijing 100083China

In the long traditional process of steelmaking,excess oxygen is blown into the converter,and alloying elements are used for *** inevitably results in excessive deoxidation of products remaining within the steel liquid,affecting the cleanliness of the *** the increasing requirements for steel performance,reducing the oxygen content in the steel liquid and ensuring its high cleanliness is *** more than a hundred years of development,the total oxygen content in steel has been reduced from approximately 100×10^(-6)to approximately 10×10^(-6),and it can be controlled below 5×10^(-6)in some steel grades.A relatively stable and mature deoxidation technology has been formed,but further reducing the oxygen content in steel is no longer significant for improving steel *** research team developed a deoxidation technology for bearing steel by optimizing the entire conventional *** technology combines silicon–manganese predeoxidation,ladle furnace diffusion deoxidation,and vacuum final *** successfully conducted industrial experiments and produced interstitial-free steel with natural decarbonization ***-aluminum deoxidation was found to control the oxygen content in bearing steel to between 4×10^(-6) and 8×10^(-6),altering the type of inclusions,eliminating large particle Ds-type inclusions,improving the flowability of the steel liquid,and deriving a higher fatigue *** natural decarbonization predeoxidation of interstitial-free steel reduced aluminum consumption and production costs and significantly improved the quality of cast billets.

关键词： steel deoxidation deoxidizer metallurgical equipment bearing steel IF steel