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Non-invasive Healthcare Analytical Platform Based on Organic Electrochemical Transistors

CHEMICAL rESEArCH IN CHINESE UNIVErSITIES 2024年第5期40卷 824-841页

作者： Hu, Xingyu Mao, Ning Yan, Xinwen Huang, Ling Liu, Xu Yang, Huige Sun, Qingqing Liu, Xuying Jia, Hanyu Zhengzhou Univ Sch Mat & Engn Zhengzhou 450001 Peoples R China Longmen lab Sci & Technol Innovat Ctr Adv Mat Intelligent Equi Luoyang 471000 Peoples R China South Cent Univ Nationalities Hubei R&D Ctr Hyperbranched Polymers Synth & Appli Key Lab Catalysis & Energy Mat Chem Minist Educ Wuhan 430074 Peoples R China South Cent Univ Nationalities Hubei R&D Ctr Hyperbranched Polymers Synth & Appli Hubei Key Lab Catalysis & Mat Sci Wuhan 430074 Peoples R China

Non-invasive bioelectronics, especially organic electrochemical transistors (OECTs), have drawn extensive attentions of academical and medical communities by virtue of their efficient bio-electronic interfacing, water-involved ionic transport, excellent ionic-electronic coupling, ultralow power consumption, wide detectable range, and outstanding detection sensitivity. designable structure diversity, low-temperature solution processability, facile bio/chemical functionalization, and excellent biocompatibility of organic mixed ionic-electronic conductors (OMIECs) render OECTs particularly suitable for non-invasive or minimally invasive healthcare analytical platform. Here, we comprehensively review recent advances of the non-invasive analytical healthcare applications based on OECTs, especially on the detection of biomarkers or metabolites in the excretory biofluids, as well as the recording of electrophysiological signals. A brief introduction of OECT and its comparison with other organic thin-film transistors upon device configuration and working mechanism are firstly discussed. State-of-the-art non-invasive OECT-based biosensors are summarized on their detection of ionic and molecular biomarkers, following with circuit design strategies of OECTs for real-time and in-situ electrophysiological recording from skin surface. In conclusion, remaining barriers and future challenges of non-invasive OECT-based bioelectronics towards lower detection limit, more accurate quantitative relationship between analyte concentrations and measured parameters, more intimate device-tissue interface, and long-term operation stability are deeply analyzed with a critical outlook.

关键词： Organic electrochemical transistor Non-invasive Bioelectronics Ion-selective Electrophysiological monitoring SENSITIVITY ION dETECTION

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Field stabilization of pulse duration in a hundredfemtosecond level

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CHINESE OPTICS LETTErS 2024年第8期22卷 081406-081406页

作者： Liu, runmin Wu, Yong Pu, Guoqing Cheng, Jiayang Mu, Huan Liu, Bowen Yi, Lilin Hu, Minglie Tianjin Univ Sch Precis Instruments & Optoelect Engn Key Lab Optoelect Informat Sci & Technol Minist EducUltrafast Laser Lab Tianjin 300072 Peoples R China Shanghai Jiao Tong Univ Sch Elect Informat & Elect Engn State Key Lab Adv Commun Syst & Networks Shanghai 200240 Peoples R China AIOPTICS Co Ltd R&D Ctr Shanghai 200240 Peoples R China

Pulse duration is considered as one of the most important characteristics of high-power femtosecond lasers. However, pulses output from the laser system are susceptible to ambient changes and manifest the instability of pulse durations in an open environment. In this paper, incorporating the algorithmic framework of the improved stochastic hill-climbing search and incremental proportional-integral controller, temperature-induced fluctuations of pulse duration can be effectively compensated by an automatic feedback control in an all-fiber chirped-pulse amplification system. In the experiment, sub-hundred femtosecond fluctuation of pulse duration is introduced to verify the performance robustness of the proposed pulse-duration feedback control (PdFC). The stability of pulse duration is obviously higher than the case without the feedback control, and the peak-to-peak fluctuation of pulse duration is reduced to 6.5%. Furthermore, the robust switching between different pulse durations proves the versatility of the PdFC. We expect that the proposed feedback control method could provide a novel insight into high-power femtosecond lasers widely applied in fundamental researches and industrial fields.

关键词： fiber amplifier femtosecond laser pulse-duration feedback control LASEr AMPLIFICATION

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Modified electronic structure and enhanced hydroxyl adsorption make quaternary Pt-based nanosheets efficient anode electrocatalysts for formic acid-/alcohol-air fuel cells

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Journal of Energy Chemistry 2024年第5期92卷 142-150页

作者： Fengling Zhao Qiang Yuan Siyang Nie Liang Wu Xun Wang State-Local joint laboratory for Comprehensive Utilization of Biomass Center for R&D of Fine ChemicalsCollege of Chemistry and Chemical EngineeringGuizhou UniversityGuiyang 550025GuizhouChina Key lab of Organic Optoelectronics&Molecular Engineering Tsinghua UniversityBeijing 100084China School of Chemistry and Chemical Engineering Shanghai Jiao Tong UniversityShanghai 200240China

Surface/interface engineering of a multimetallic nanostructure with diverse electrocatalytic properties for direct liquid fuel cells is desirable yet ***,using visible light,a class of quaternary Pt_(1)Ag_(0.1)Bi_(0.16)Te_(0.29)ultrathin nanosheets is fabricated and used as high-performance anode electrocatalysts for formic acid-/alcohol-air fuel *** modified electronic structure of Pt,enhanced hydroxyl adsorption,and abundant exterior defects afford Pt_(1)Ag_(0.1)Bi_(0.16)Te_(0.29)/C high intrinsic anodic electrocatalytic activity to boost the power densities of direct formic acid-/methanol-/ethanol-/ethylene glycol-/glycerol-air fuel cells,and the corresponding peak power density of Pt_(1)Ag_(0.1)Bi_(0.16)Te_(0.29)/C is respectively 129.7,142.3,105.4,124.3,and 128.0 mW cm^(-2),considerably outperforming Pt/*** in situ Fourier transform infrared reflection spectroscopy reveals that formic acid oxidation on Pt_(1)Ag_(0.1)Bi_(0.16)Te_(0.29)/C occurs via a CO_(2)-free direct *** functional theory calculations show that the presence of Ag,Bi,and Te in Pt_(1)Ag_(0.1)Bi_(0.16)Te_(0.29)suppresses CO^(*)formation while optimizing dehydrogenation steps and synergistic effect and modified Pt effectively enhance H_(2)O dissociation to improve electrocatalytic *** synthesis strategy can be extended to 43 other types of ultrathin multimetallic nanosheets(from ternary to octonary nanosheets),and efficiently capture precious metals(i.e.,Pd,Pt,rh,ru,Au,and Ag)from different water sources.

关键词： Pt-based nanosheets Modifiedelectronic structure Enhanced hydroxyl adsorption Formicacidand alcohol oxidation direct liquid fuel cells

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New structure transistors for advanced technology node CMOS ICs

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National Science review 2024年第3期11卷 24-41页

作者： Qingzhu Zhang Yongkui Zhang Yanna Luo Huaxiang Yin Integrated Circuit Advanced Process r&d Center Institute of Microelectronics of Chinese Academy of Sciences(IMECAS) State key lab of Fabrication Technologies for Integrated Circuits Institute of Microelectronics of Chinese Academy of Sciences School of Integrated Circuits University of Chinese Academy of Sciences

Over recent decades, advancements in complementary metal-oxide-semiconductor integrated circuits(ICs)have mainly relied on structural innovations in transistors. From planar transistors to the fin field-effect transistor(FinFET) and gate-all-around FET(GAAFET), more gate electrodes have been added to three-dimensional(3d) channels with enhanced control and carrier conductance to provide higher electrostatic integrity and higher operating currents within the same device footprint. Beyond the 1-nm node, Moore's law scaling is no longer expected to be applicable to geometrical shrinkage. Vertical transistor stacking, e.g. in complementary FETs(CFET), 3d stack(3dS) FETs and vertical-channel transistors(VFET), for enhanced density and variable circuit or system design represents a revolutionary scaling approach for sustained IC development. Herein, innovative works on specific structures, key process breakthroughs, shrinking cell sizes and design methodologies for transistor structure research and development are reviewed. Perspectives on future innovations in advanced transistors with new channel materials and operating theories are also discussed.

关键词： transistor CMOS GAAFET CFET 3dS FET

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Effects of the VGS sweep range on the short channel effect in negative capacitance FinFETs

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Science China(Information Sciences) 2024年第06期67卷 463-464页

作者： Fan ZHANG Zhaohao ZHANG Jiaxin YAO Qingzhu ZHANG Gaobo XU Zhenhua WU Huan LIU Genquan HAN Yan LIU Huaxiang YIN Integrated Circuit Advanced Process r&d Center State Key Lab of Fabrication Technologies for Integrated CircuitsInstitute of Microelectronics of Chinese Academy of Sciences School of Microelectronics Xidian University School of Integrated Circuits University of Chinese Academy of Sciences

As the CMOS technology scaling is reaching fundamental limits,there is a substantial demand for energy-efficient devices with lower operating *** capacitance field-effect transistors （NCFETs） exhibit the capability to amplify the gate voltage and become promising candidates for future advanced process *** （FE） HfO2-based materials,

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Microstructure and Shear Properties Evolution of Minor Fe-doped SAC/Cu Substrate Solder joint under Isothermal Aging

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Acta Metallurgica Sinica(English Letters) 2024年第7期37卷 1279-1290页

作者： Quanzhen Li Chengming Li Xiaojing Wang Shanshan Cai Jubo Peng Shujin Chen Jiajun Wang Xiaohong Yuan Jiangsu University of Science and Technology Zhenjiang212003China r&d Center Yunnan Tin Group(Holding)Co.LtdKunming650000China The 58 Research Institute of China Electronics Technology Group CorporationWuxi214100China Yunnan Precious Metals lab Sino-Platinum Metals Co.LtdKunming650156China

different amounts of Fe(0.005,0.01,0.03,0.05,and 0.07 wt%)were added to SAC305 to study the shear behavior damage of Fe-doped SAC solder joints under thermal loading(170℃,holding time of 0,250,500,and 750 h).The results show that during isothermal aging at 170℃,the average shear force of all solder joints decreases with increasing aging time,while the average fracture energy first increases and then decreases,reaching a maximum at 500 *** Fe doping could both increase shear forces and related fracture energy,with the optimum Fe doping amount being 0.03 wt%within the entire aging *** is because the doping Fe reduces the undercooling of the SAC305 alloy,resulting in the microstructure refining of solder *** in turn causes the microstructure changing from network structure(SAC305 joint:eutectic network+β-Sn)to a single matrix structure(0.03Fe-doped SAC305 joint:β-Sn matrix+small compound particles).Specifically,Fe atoms can replace some Cu in Cu_(6)Sn_(5)(both inside the solder joint and at the interface),and then form(Cu,Fe)_(6)Sn_(5) compounds,resulting in an increase in the elastic modulus and nanohardness of the ***,the growth of Cu_(6)Sn_(5) and Cu_(3)Sn intermetallic compounds(IMC)layer are inhibited by Fe doping even after the aging time prolonging,and Fe aggregates near the interface compound to form FeSn_(2).This study is of great significance for controlling the growth of interfacial compounds,stabilizing the microstructures,and providing strengthening strategy for solder joint alloy design.

关键词： SAC305 solder Fe doping Shear mechanical behavior Isothermal aging Interfacial intermetallic compounds(IMC)

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Layerwise third-order shear deformation theory with transverse shear stress continuity for piezolaminated plates

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CHINESE JOUrNAL OF AErONAUTICS 2024年第9期37卷 490-505页

作者： Gao, Yingshan Zhang, Shunqi Hu, Wei Ma, Songyun Markert, Bernd Shanghai Univ Sch Mech Engn & Automat Shanghai 200444 Peoples R China Shanghai Univ Key Lab Silicate Cultural Rel Conservat Minist Educ Shanghai 200444 Peoples R China rhein Westfal TH Aachen Inst Gen Mech D-52062 Aachen Germany

regarding laminated structures, an electromechanically coupled Finite Element (FE) model based on Layerwise Third-Order Shear deformation (LW-TOSd) theory is proposed for static and dynamic analysis. LW-TOSd ensures the continuity of in-plane displacements and transverse shear stresses. The current LW-TOSd can be applied to arbitrary multi-layer laminated structures with only seven degrees of Freedom (dOFs) for each element node and eliminates the use of the shear correction factors. Moreover, a shear penalty stiffness matrix is constructed to satisfy artificial constraints to optimize the structural shear strain. A dynamic finite element model is obtained based on LW-TOSd using the Hamilton's principle. First, the accuracy of the current model is validated by comparing with literature and ABAQUS results. Then, this study carries out numerical investigations of piezolaminated structures for different width-to-thickness ratios, length-to-width ratios, penalty stiffness matrix, boundary conditions, electric fields and dynamics. (c) 2024 Production and hosting by Elsevier Ltd. on behalf of Chinese Society of Aeronautics and Astronautics.

关键词： Laminated structures Piezolaminated structures Third-order shear deforma- tion theory Shear stress continuity Electromechanically coupled LAMINATEd COMPOSITE FrEE-VIBrATION SANdWICH PLATES

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The transition to turbulent fluidization in a gas-solid fluidized bed operating from ambient temperature to 1600 °C

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PArTICUOLOGY 2024年第10期93卷 111-124页

作者： Zhang, Qingjin Fu, Liangliang Xu, Guangwen Bai, dingrong Shenyang Univ Chem Technol Key Lab Resources Chem & Mat Minist Educ Shenyang 110142 Peoples R China Shenyang Univ Technol Sch Mat Sci & Engn Shenyang 110142 Peoples R China Ordos lab Ordos 017010 Peoples R China

Turbulent fluidized bed proves effective in industrial processes due to superior heat and mass transfer and chemical reaction performance. However, understanding the transition to turbulent fluidization remains limited, especially at temperatures exceeding 1000 degrees C, making it challenging to develop hightemperature fluidized bed applications. This paper presents an experimental investigation on the turbulent fluidization onset velocity (Uc), measured in a 30 mm diameter bed using corundum particles with average diameters from 0.68 mm to 1.58 mm in temperatures from ambient to 1600 degrees C. Experimental results reveal that Uc increases with temperature up to 600 degrees C, stabilizes within the 600-1200 degrees C range, and then decreases above 1200 degrees C, demonstrating the varying relative significance of hydrodynamic and interparticle forces at different temperatures. To help design and operate high-temperature applications of turbulent fluidization, we developed Uc correlations based on experimental data from both literature sources and this study, covering temperatures of up to 1600 degrees C and particles of Groups A to d.

关键词： High-temperature fluidized beds Turbulent fluidization Transition velocity Pressure fluctuations Hydrodynamic forces Interparticle forces rEGIME TrANSITION HYdrOdYNAMICS PrESSUrE VELOCITIES SIZE

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Crack propagation and damage evolution of metallic cylindrical shells under internal explosive loading

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dEFENCE TECHNOLOGY 2024年第9期39卷 133-146页

作者： Luo, Yusong Li, Weibing Li, Junbao Li, Wenbin Wang, Xiaoming Nanjing Univ Sci & Technol ZNDY Ministerial Key Lab Nanjing 210094 Peoples R China

This paper investigates the three-dimensional crack propagation and damage evolution process of metallic column shells under internal explosive loading. The calibration of four typical failure parameters for 40CrMnSiB steel was conducted through experiments and subsequently applied to simulations. The numerical simulation results employing the four failure criteria were compared with the differences and similarities observed in freeze-recovery tests and ultra-high-speed tests. This analysis addressed the critical issue of determining failure criteria for the fracture of a metal shell under internal explosive loads. Building upon this foundation, the damage parameter dc, linked to the cumulative crack density, was defined based on the evolution characteristics of a substantial number of cracks. The relationship between the damage parameter and crack velocity over time was established, and the influence of the internal central pressure on the damage parameter and crack velocity was investigated. Variations in the fracture modes were found under different failure criteria, with the principal strain failure criterion proving to be the most effective for simulating 3d crack propagation in a pure shear fracture mode. Through statistical analysis of the shell penetration fracture radius data, it was determined that the fracture radius remained essentially constant during the crack evolution process and could be considered a constant. The propagation velocity of axial cracks ranged between 5300 m/s and 12600 m/s, surpassing the rayleigh wave velocity of the shell material and decreasing linearly with time. The increase in shell damage exhibited an initial rapid phase, followed by deceleration, demonstrating accelerated damage during the propagation stage of the blast wave and decelerated damage after the arrival of the rarefaction wave. This study provides an effective approach for investigating crack propagation and damage evolution. The derived crack propagation and damag

关键词： Internal explosive loading Failure criterion Crack propagation damage evolution Freeze-recovery test INTErMEdIATE PHASE SHEAr-BANd STEEL FrAGMENTATION dEFOrMATION MECHANISM

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mtdNA-triggered pH response signal-amplified fluorescent probe for multiple cell discrimination

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Chinese Chemical Letters 2024年第3期35卷 363-368页

作者： Tianping Xia Yanxian Hou Zhuoran Xia Gengwen Chen Peichen Tang Jiangli Fan Xiaojun Peng State Key laboratory of Fine Chemicals Frontiers Science Center for Smart Materials Oriented Chemical EngineeringDalian University of TechnologyDalian 116024China Hematology reagent r&d department Mindray Bio-medical Electronics Co.Ltd.Shenzhen 518132China research Institute of dalian University of Technology in Shenzhen Shenzhen 518057China

developing fluorescence probes with multiple responses has vital significance but remains ***,for the first time,we present a mitochondrial dNA(mtdNA)-triggered pH response signalamplified fluorescent probe(QCY-dBT)for multiple cell *** probe exhibited a large stokes shift(229 nm),excellent dNA selectivity over rNA,and ultrasensitivity of detection limit(dL;74.0 ng/mL).Thus,QCY-dBT was successfully applied to analyze multiple human peripheral blood cells and visualize mtdNA in healthy and apoptotic *** the tumor acidic environment(pH 6.0–7.0),the absorbance of QCY-dBT at 436 nm increased,and the fluorescence signal(665 nm)was amplified by mtdNA,which enabled the direct observation of tumor *** study provides help in designing smart probes with multiple responses for efficient abnormal cell detection.

关键词： Fluorescence probe Mitochondrial dNA pH response Peripheral blood cells Multiple cell detection

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