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composite structure Al_(2)O_(3)/Al_(2)O_(3)-YAG:Ce/YAG ceramics with high co.or spatial uniformity for white laser lighting

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Journal of Advanced Ceramics 2024年第2期13卷 189-197页

作者： Pengfei Sang Le Zhang Jian Kang Mingzhou Li Shiwei Chen Peng Yang Bingheng Sun Yang Li Wieslaw Strek Hao Chen jiangsu Key Laboratory of Advanced Laser materials and Devices School of Physics and Electronics EngineeringJiangsu Normal UniversityXuzhou 221116China jiangsu Xiyi Advanced materials Research Institute of Industrial Technology Xuzhou 221400China Xuzhou EAGLED Technology co. Ltd.Xuzhou 221116China Xuzhou Kangna Advanced materials Technology co. Ltd.Xuzhou 221116China Xuzhou Fuchang Electronic Technology co. Ltd.Xuzhou 221116China Shanghai Institute of Optics Fine Mechanics Chinese Academy of SciencesShanghai 201800China School of Material Science and Engineering Shanghai Institute of TechnologyShanghai 201418China State Key Laboratory of Crystal materials Shandong UniversityJinan 250100China Institute of Low Temperature and Structure Research Polish Academy of SciencesWroclaw 50-422Poland

composite ceramic phosphor(CCP)is a candidate light-co.version material to obtain the high-quality laser lighting source.Phosphors based on the transmissive co.figuration model co.ld not simultaneously meet the requirements of angular co.or uniformity and high thermal stability.In this study,a novel composite structure ceramic was designed,including Al_(2)O_(3)-YAG:Ce/YAG layered ceramic with a size of 1 mm×1 mm for lighting,and Al_(2)O_(3) ceramic(φ=16.0 mm)was used as the wrapping material due to its outstanding thermal stability.The prepared ceramics exhibited excellent thermal performance and no yellow ring phenomenon.Through this design,we achieved the match of the intensity distribution of the blue and yellow lights,resulting in a high angular co.or uniformity of 0.9 with a view angle of±80°.All ceramics showed no luminous saturation phenomenon,even the laser power density was increased up to 47.51 W/mm^(2).A high-brightness white-light source with a luminous flux of 618 lm,a luminous efficiency of 126 lm/W,a CCT of 6615 K,and a CRI of 69.9 was obtained in the transmissive co.figuration.In particular,the surface temperature of the ceramic was as low as 74.1℃ under a high laser radiation(47.51 W/mm^(2)).These results indicate that Al_(2)O_(3)/Al_(2)O_(3)-YAG:Ce/YAG composite structure ceramic is a promising luminescent material in the high-power laser lighting applications.

关键词： Al_(2)O_(3)/Al_(2)O_(3)-YAG:Ce/YAG angular co.or uniformity high thermal stability high-power laser lighting

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Critical state-induced emergence of superior magnetic performances in an iron-based amorphous soft magnetic composite

Materials Futures

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materials Futures 2024年第2期3卷 149-160页

作者： Liliang Shao Rongsheng Bai Yanxue Wu Jing Zhou Xing Tong Hailong Peng Tao Liang Zongzhen Li Qiaoshi Zeng Bo Zhang Haibo Ke Weihua Wang Songshan Lake materials Laboratory Dongguan 523808People’s Republic of China Institute of Physics Chinese Academy of SciencesBeijing 100190People’s Republic of China School of Energy Power and Mechanical EngineeringNorth China Electric Power UniversityBeijing 100096People’s Republic of China School of materials Science and Engineering Central South UniversityChangsha 410083People’s Republic of China Center for High Pressure Science and Technology Advanced Research Shanghai 201203People’s Republic of China jiangsu JITRI Advanced Energy materials Research Institute co. LtdChangzhou 213000People’s Republic of China

Soft magnetic composites(SMCs)play a pivotal role in the development of high-frequency,miniaturization and co.plex forming of modern electronics.However,they usually suffer from a trade-off between high magnetization and good magnetic softness(high permeability and low co.e loss).In this work,utilizing the order modulation strategy,a critical state in a FeSiBCCr amorphous soft magnetic composite(ASMC),co.sisting of massive crystal-like orders(CLOs,∼1 nm in size)with the feature ofα-Fe,is designed.This critical-state structure endows the amorphous powder with the enhanced ferromagnetic exchange interactions and the optimized magnetic domains with uniform orientation and fewer micro-vortex dots.Superior co.prehensive soft magnetic properties at high frequency emerge in the ASMC,such as a high saturation magnetization(Ms)of 170 emu g^(-1)and effective permeability(µ_(e))of 65 co.bined with a co.e loss(Pcv)as low as 70 mW cm^(-3)(0.01 T,1 MHz).This study provides a new strategy for the development of high-frequency ASMCs,possessing suitable co.prehensive soft magnetic performance to match the requirements of the modern magnetic devices used in the third-generation semico.ductors and new energy fields.

关键词： amorphous soft magnetic composites critical state soft magnetic property rotating magnetic field annealing magnetic domain

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Phase engineering of Ni-Mn binary layered oxide cathodes for sodiumion batteries

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Journal of Energy Chemistry 2024年第4期91卷 501-511页

作者： Feifei Hong Xin Zhou Xiaohong Liu Guilin Feng Heng Zhang Weifeng Fan Bin Zhang Meihua Zuo Wangyan Xing Ping Zhang Hua Yan Wei Xiang co.lege of materials and Chemistry&Chemical Engineering Chengdu University of TechnologyChengdu 610059SichuanChina co.lege of Chemical Engineering Sichuan UniversityChengdu 610065SichuanChina Research Institute for Electronic Science(RIES)and Division of Information Science and Technology Graduate School of Information Science and TechnologyHokkaido UniversityN20W10SapporoHokkaido 001-0020Japan School of materials Science and Engineering Suzhou University of Science and TechnologySuzhou 215009JiangsuChina Yibin Libode New materials co. Ltd.Yibin 644200SichuanChina Engineering Research Center of the Ministry of Education for Advanced Battery materials School of Metallurgy and EnvironmentCentral South UniversityChangsha 410083HunanChina

Nickel-manganese binary layered oxides with high working potential and low co.t are potential candidates for sodium-ion batteries,but their electrochemical properties are highly related to co.positional diversity.Diverse composite materials with various phase structures of P3,P2/P3,P2,P2/O3,and P2/P3/O3 were synthesized by manipulating the sodium co.tent and calcination co.ditions,leading to the co.struction of a synthetic phase diagram for Na_(x)Ni_(0.25)Mn_(0.75)O_(2)(0.45≤x≤1.1).Then,we co.pared the electrochemical characteristics and structural evolution during the desodiation/sodiation process of P2,P2/P3,P2/03,and P2/P3/O3-Na_(x)Ni_(0.25)Mn_(0.75)O_(2).Among them,P2/P3-Na0.75Ni0.25Mn0.75O2exhibits the best rate capability of 90.9 mA h g^(-1)at 5 C,with an initial discharge capacity of 142.62 mA h g^(-1)at 0.1 C and a capacity retention rate of 78.25%after 100 cycles at 1 C in the voltage range of 2-4.3 V.The observed superior sodium storage performance of P2/P3 hybrids co.pared to other composite phases can be attributed to the enhanced Na^(+)transfer dynamic,reduction of the Jahn-teller effect,and improved reaction reversibility induced by the synergistic effect of P2 and P3 phases.The systematic research and exploration of phases in Na_(x)Ni_(0.25)Mn_(0.75)O_(2)provide new sights into high-performance nickel-manganese binary layered oxide for sodium-ion batteries.

关键词： Phase engineering Ni-Mn layered oxide Cathode Sodium-ion batteries

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Layered Structural PBAT composite Foams for Efficient Electromagnetic Interference Shielding

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Nano-Micro Letters 2024年第2期16卷 273-286页

作者： Jianming Yang Hu Wang Yali Zhang Hexin Zhang Junwei Gu School of Chemistry and Chemical Engineering Anhui University of TechnologyMa’anshanAnhui 243032People’s Republic of China Shaanxi Key Laboratory of Macromolecular Science and Technology School of Chemistry and Chemical EngineeringNorthwestern Polytechnical UniversityXi’an 710072ShaanxiPeople’s Republic of China School of materials Science and Engineering Jiangsu University of Science and TechnologyZhenjiang 212003JiangsuPeople’s Republic of China

The utilization of eco.friendly,lightweight,high-efficiency and high-absorbing electromagnetic interference(EMI)shielding composites is imperative in light of the worldwide promotion of sustainable manufacturing.In this work,magnetic poly(butyleneadipate-co.erephthalate)(PBAT)microspheres were firstly synthesized via phase separation method,then PBAT composite foams with layered structure was co.structed through the supercritical carbon dioxide foaming and scraping techniques.The merits of integrating ferroferric oxideloaded multi-walled carbon nanotubes(Fe3O4@MWCNTs)nanoparticles,a microcellular framework,and a highly co.ductive silver layer have been judiciously orchestrated within this distinctive layered co.figuration.Microwaves are co.sumed throughout the process of“absorption-reflection-reabsorption”as much as possible,which greatly declines the seco.dary radiation pollution.The biodegradable PBAT composite foams achieved an EMI shielding effectiveness of up to 68 dB and an absorptivity of 77%,and authenticated favorable stabilization after the tape adhesion experiment.

关键词： Electromagnetic interference shielding Layered structure Supercritical carbon dioxide foaming Poly(butyleneadipateco.terephthalate) Microcellular

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An intermittent lithium deposition model based on CuMnbimetallic MOF derivatives for composite lithium anode with ultrahigh areal capacity and current densities

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Nano Research 2024年第4期17卷 2763-2769页

作者： Tao Wei Yanyan Zhou Cheng Sun Xingtong Guo Shoudong Xu Daifen Chen Yongfu Tang School of Energy and Power Jiangsu University of Science and TechnologyZhenjiang 212003China State Key Laboratory of Metastable materials Science and Technology(MMST) Hebei Key Laboratory of Applied ChemistryYanshan UniversityQinhuangdao 066004China co.lege of materials Science and Engineering Taiyuan University of TechnologyTaiyuan 030024China

Recently,three-dimensional(3D)co.ductive frameworks have been chosen as the host for composite lithium(Li)metal anode because of their exceptional electrical co.ductivity and remarkable thermal and electrochemical stability.However,Li tends to accumulate on the top of the 3D frameworks with homogenous lithiophilicity and Li dendrite still growth.This work firstly designed a bimetallic metal-organic framework(MOF)(CuMn-MOF)derived Cu_(2)O and Mn_(3)O_(4) nanoparticles deco.ated carbon cloth(CC)substrates(CC@Cu_(2)O/Mn_(3)O_(4))to fabricate a composite Li anode.Thanks to the synergistic effects of lithiophilic Cu_(2)O and Mn_(3)O_(4),the CC@Cu_(2)O/Mn_(3)O_(4)@Li symmetrical cell can afford a prolonged cycling lifespan(1400 h)under an ultrahigh current density and areal capacity(6 mA·cm^(-2)/6 mAh·cm^(-2)).When co.pled with the LiFePO_(4)(LFP)cathode,the LFP||CC@Cu_(2)O/Mn_(3)O_(4)@Li full cell demonstrated a superior performance of 89.7 mAh·g^(-1) even at an extremely high current density(10 C).Furthermore,it can also be matched well with LiNi_(0.5)co.(0).2Mn_(0.3)O_(2)(NCM523)cathode.Importantly,to explain the excellent performances of the CC@Cu_(2)O/Mn_(3)O_(4)@Li composite anode,an intermittent model was also proposed.This study offers a novel model that can enhance our co.prehension of the Li deposition behavior and pave the way to attain stable and safe Li metal anodes by employing bimetallic MOF-derived materials to co.struct 3D frameworks.

关键词： lithium metal anode(LMA) three-dimensional(3D)frameworks intermittent lithiophilic model high areal capacity bimetallic metal-organic frameworks(MOFs)

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Synthesis and microwave absorption performance of heat-treated RF/SiO_(2)aerogels

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Defence Technology（防务技术） 2024年第4期34卷 177-186页

作者： Xinli Ye Hao Yu Kai Zheng Shan Li Xiaomin Ma Bangxiao Mao Junxiong Zhang School of Civil Aviation Northwestern Polytechnical UniversityXi’an 710072PR China Research&Development Institute of Northwestern Polytechnical University in Shenzhen Shenzhen 518057PR China Yangtze River Delta Research Institute of Northwestern Polytechnical University Suzhou 215400PR China National Equipment New Material&Technology(jiangsu)co. LtdSuzhou 215400PR China Beijing Xinfeng Aerospace Equipment co. LtdBeijing 100854PR China School of Textile and Clothing Nantong UniversityNantong 226019PR China

The well-designed composite with satisfactory electromagnetic microwave absorption at high temperatures remains a serious challenge.Herein,we fabricated a resorcinol-formaldehyde/silica dioxide composite aerogel(RF/SiO_(2))with a three-dimensional network structure using sol-gel,atmospheric pressure drying technique as well as heat-treated processes to achieve enhanced microwave absorption capabilities in the low frequency range.The pristine RF/SiO_(2)aerogel presented a typical micropores structure with a surface area,porous volume,and density of 146.82 m^(2)/g,62.40%,and 0.28 cm^(3)/g,respectively.Remarkably,the RF/SiO_(2)aerogel showed an effective absorption bandwidth of 3.56 GHz and a minimum reflection loss value of-46.10 d B at 2.25 mm after being heat-treated at 1500°C,while the maximum effective absorption bandwidth was 3.60 GHz at 2.30 mm.The intricate three-dimensional networks possessed remarkable impedance matching,multiple attenuation mechanisms,interfacial polarization,and dielectric loss,which were attributed to the exceptional ability to absorb electromagnetic microwaves.It offered a fresh approach to creating adaptable and effective microwave absorption materials in military defense.

关键词： RF/SiO_(2) Aerogel Heat-treated Microwave absorption

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In-situ powder mixing for laser-based directed energy deposition of functionally graded materials

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Advances in Manufacturing 2024年第1期12卷 150-166页

作者： Ji-Peng Chen Shou-Chun Xie He Huang School of Mechanical and Electronic Engineering Nanjing Forestry UniversityNanjing210037People’s Republic of China Nanjing Huirui Photoelectric Technology co. LtdNanjing211121People’s Republic of China

The mixing of powders is a highly relevant field under additive manufacturing,however,it has attracted limited interest to date.The in-situ mixing of various powders remains a significant challenge.This paper proposes a new method utilizing a static mixer for the in-situ mixing of multiple powders through the laser-based directed energy deposition(DED)of functionally graded materials.Firstly,a powder-mixing experimental platform was established;WC and 316L powders were selected for the mixing experiments.Seco.dly,scanning electron microsco.y,energy dispersive spectrosco.y,and image processing were used to visually evaluate the homogeneity and proportion of the in-situ mixed powder.Furthermore,powder-mixing simulations were co.ducted to determine the powder-mixing mechanism.In the simulations,a powder carrier gas flow field and particle mixing were employed.Finally,a WC/316L metal matrix composite sample was produced using laser-based DED to verify the application potential of the static mixer.It was found that the static mixer co.ld adjust the powder ratio online,and a response time of 1–2 s should be co.sidered when adjusting the ratio of the mixed powder.A feasible approach for in-situ powder mixing for laser-based DED was demonstrated and investigated,creating the basis for functionally graded materials.

关键词： Laser Deposition Static mixer Powder mixing Functionally graded materials

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Improved photocatalytic performance of acetaldehyde degradation via crystal plane regulation on truncated octahedral CeO2

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Rare Metals 2024年第5期43卷 2026-2038页

作者： Bin Xu Lu Jia Hui Yang Yue Wang Si-Yu Fan Sai-Sai Yuan Qi-Tao Zhang Ming Zhang Teruhisa Ohno School of Chemistry and Chemical Engineering Yangzhou University co.lege of Environmental Science and Engineering Yangzhou University Department of Applied Chemistry Faculty of EngineeringKyushu Institute of Technology School of Environmental and Chemical Engineering Jiangsu University of Science and Technology National & Local Joint Engineering Research Center for Mineral Salt Deep Utilization Huaiyin Institute of Technology School of materials Science and Engineering Henan University of Science and Technology International co.laborative Laboratory of 2D materials for Optoelectronics Science and Technology of Ministry of Education Institute of Microscale Optoelectronics Shenzhen University

In this study,the truncated octahedral Ce O2（Ce O2-to） with special morphology was prepared by the solvothermal method with oleic acid （OA） and oleamine（OM） as the morphology-directing agents.High-resolution transmission electron microsco.y （HRTEM） results show that Ce O2-to exposes composite{100}and{111}facets,while Ce O2cubic （Ce O2-c） and Ce O2octahedral （Ce O2-o）only expose single crystal facets of{100}plane and{111}plane,respectively.Interestingly,this Ce O2-to photocatalyst exhibits remarkable photooxidation performance of gaseous acetaldehyde （CH3CHO） degradation,in which co.generation value reaches 1.78 and 7.97-times greater than that of Ce O2-c and Ce O2-o,respectively.In addition,the active species trapping experiment signifies that superoxide （·O2-） and holes （h+） are the main reactive substances during the CH3CHO degradation process,and the electron paramagnetic resonance （EPR） spectra indicates that the former is the major co.tributor.Notably,the electron transfer mechanism between Ce O2-to{100}and{111}facets and the surface oxygen adsorption ability are revealed via density functional theory （DFT） calculations.It is also co.firmed that{100}facets are more co.ducive to the absorption of acetaldehyde than{111}facets.Finally,a reasonable mechanism for improved photocatalytic CH3CHO degradation on Ce O2-to is proposed based on relevant experiments and DFT calculations.This study demonstrates that the systematic development of surface homojunction structured photocatalysts can efficiently increase the degradation activity for volatile organic co.pounds （VOCs）.It also offers additional direction for optimizing the photocatalytic activity of other ceriumbased photocatalysts.

关键词： Truncated octahedral CeO 2 (CeO 2 -to) composite crystal faces Surface energy level Efficient electron transfer

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Engineering and understanding SnS_(0.5)Se_(0.5)@N/S/Se triple-doped carbon nanofibers for enhanced sodium-ion batteries

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Chinese Chemical Letters 2024年第4期35卷 226-230页

作者： Fanjun Kong Yixin Ge Shi Tao Zhengqiu Yuan Chen Lu Zhida Han Lianghao Yu Bin Qian School of Electronic and Information Engineering Changshu Institute of TechnologyChangshu 215500China Key Laboratory of Spin Electron and Nanomaterials of Anhui Higher Education Institutes Suzhou UniversitySuzhou 234000China Far East Holding Group co. Ltd.Yixing 214200China

Tin-based chalco.enides have attracted tremendous attention as an anode material for sodium storage owing to their unique structure and high theoretical capacity. Unfortunately, the large volume change and poor co.ductivity lead to sluggish reaction kinetics and poor cycling performance. Herein, SnS_(0.5)Se_(0.5)nanoparticles co.pled with N/S/Se triple-doped carbon nanofibers(SnS_(0.5)Se_(0.5)@NSSe-C) are designed and synthesized through electrospinning and annealing process. Benefiting from the synergistic effects of SnS_(0.5)Se_(0.5)and NSSe-C, the SnS_(0.5)Se_(0.5)@NSSe-C nanofibers exhibit a high reversible capacity and ultralong cycle life at higher current density for sodium-ion batteries. Furthermore, the sodium storage mechanism and electrochemical reaction kinetics of the SnS_(0.5)Se_(0.5)@NSSe-C composite are characterized by the in-situ measurements. The theoretical calculations further reveal the structural advantages of SnS_(0.5)Se_(0.5)@NSSeC composite, which exhibits a high adsorption energy of Na+. This work can provide a novel idea for the synthesis of ternary tin-based chalco.enides and is beneficial for the investigation of their reaction kinetics.

关键词： SnS_(0.5)Se_(0.5) Carbon nanofibers Doping Density functional theory Sodium ion batteries

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Synergistically co.pling of graphene quantum dots with Zn-intercalated MnO2 cathode for high-performance aqueous Zn-ion batteries

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International Journal of Minerals,Metallurgy and materials 2023年第1期30卷 25-32页

作者： Minjie Shi Hangtian Zhu co.g Chen Jintian Jiang Liping Zhao Chao Yan School of materials Science and Engineering Jiangsu University of Science and TechnologyZhenjiang 212003China State Key Laboratory for Metallic Matrix composite materials School of Materials Science and EngineeringShanghai Jiao Tong UniversityShanghai 200240China Zhejiang Research Institute of Chemical Industry co. LtdHangzhou 310012China

co.t-effective,safe,and highly performing energy storage devices require rechargeable batteries,and among various options,aqueous zinc-ion batteries(ZIBs)have shown high promise in this regard.As a cathode material for the aqueous ZIBs,manganese dioxide(MnO_(2))has been found to be promising,but certain drawbacks of this cathode material are slow charge-transfer capability and poor cycling performance.Herein,a novel design of graphene quantum dots(GQDs)integrated with Zn-intercalated MnO_(2)nanosheets is put forward to co.struct a 3D nanoflower-like GQDs@ZnxMnO_(2)composite cathode for aqueous ZIBs.The synergistic co.pling of GQDs modification with Zn intercalation provides abundant active sites and co.ductive medium to facilitate the ion/electron transmission,as well as ensure the GQDs@ZnxMnO_(2)composite cathode with enhanced charge-transfer capability and high electrochemical reversibility,which are elucidated by experiment results and in-situ Raman investigation.These impressive properties endow the GQDs@ZnxMnO_(2)composite cathode with superior aqueous Zn^(2+) storage capacity(~403.6 mAh·g^(−1)),excellent electrochemical kinetics,and good structural stability.For actual applications,the fabricated aqueous ZIBs can deliver a substantial energy density(226.8 W·h·kg^(−1)),a remarkable power density(650 W·kg^(−1)),and long-term cycle performance,further stimulating their potential application as efficient electrochemical storage devices for various energy-related fields.

关键词： synergistically co.pling intercalation engineering graphene quantum dots manganese oxides aqueous batteries

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