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Chitosan Nanoparticles as Biostimulant in Lettuce (Lactuca sativa L.) Plants

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Phyton-International Journal of Experimental Botany 2024年第4期93卷 777-787页

作者： Silvia C.Ramírez-Rodríguez Pablo Preciado-Rangel Marcelino cabrera-De La Fuente Susana González-Morales Hortensia Ortega-Ortiz Tecnológico Nacional de México Instituto Tecnológico de TorreónEjido AnaTorreónCoahuila27170México Departamento de Horticultura Universidad Autónoma Agraria Antonio NarroSaltillo25315México Departamento de Materiales Avanzados Centro de Investigación en Química AplicadaSaltilloCoahuila25294México

Biodegradable nanoparticles such as chitosan nanoparticles (CSNPs) are used in sustainable agriculture since theyavoid damage to the environment;CSNPs have positive effects such as the accumulation of bioactive compoundsand increased productivity in plants. This study aimed to investigate the impact of applying CSNPs on lettuce,specifically focusing on enzymatic activity, bioactive compounds, and yield. The trial was conducted using a completelyrandomized design, incorporating CSNPs: 0, 0.05, 0.1, 0.2, 0.4, and 0.8 mg mL−1. The doses of 0.4 mg mL−1improve yields up to 24.6% increases and 0.1 mg mL−1 of CSNPs increases total phenols by 31.2% and antioxidantcapacity by 34.6%. In addition, when low concentrations of CSNPs (0.05 and 0.1 mg L−1) were applied, anincrease in catalase was determined. The CSNPs represent a good alternative to be used as a biostimulant in sustainableagriculture because they improve the yield and quality of lettuce by increasing the bioactive compounds.

关键词： Biostimulant bioactive compounds enzymatic activity

Plasmon-induced dual-wavelength operation in a Yb^(3+) laser

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Light(Science & Applications) 2019年第1期8卷 1042-1050页

作者： Laura Sanchez-Garcia Mariola O.Ramirez Rosa Maria Sole Joan J.Carvajal Francesc Diaz Luisa E.Bausa Deparment Fisica de Materiales Instituto Nicolas Cabrera and Condensed Matter Physics Center(IFIMAC)Universidad Autonoma de Madrid28049 MadridSpain Universitat Rovira i Virgili Departament Quimica Fisica i InorganicaFisica i Cristal·lografia de Materials i Nanomaterials(FiCMA-FiCNA)-EMaSE-43007 TarragonaSpain

Expanding the functionalities of plasmon-assisted lasers is essential for emergent applications in nanoscience and nanotechnology.Here,we report on a novel ability of plasmonic structures to induce dual-wavelength lasing in the near-infrared region in a Yb^(3+) solid-state laser.By means of the effects of disordered plasmonic networks deposited on the surface of a Yb^(3+)-doped nonlinear RTP crystal,room-temperature dual-wavelength lasing,with a frequency difference between the lines in the THz range,is realized.The dual-wavelength laser is produced by the simultaneous activation of two lasing channels,namely,an electronic-and a phonon-terminated laser transition.The latter is enabled by the out-of-plane field components that are generated by the plasmonic structures,which excite specific Raman modes.Additionally,multiline radiation at three different wavelengths is demonstrated in the visible spectral region via two self-frequency conversion processes,which occur in the vicinities of the plasmonic structures.The results demonstrate the potential of plasmonic nanostructures for inducing drastic modifications in the operational mode of a solid-state laser and hold promise for applications in a variety of fields,including multiplexing,precise spectroscopies,and THz radiation generation via a simple and cost-effective procedure.

关键词： laser lasing dual

ZnO/CeO_(2)/carbon xerogel composites with direct Z-scheme heterojunctions:Enhancing photocatalytic remediation of 4-chlorophenol under visible light

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Journal of Rare Earths 2024年第2期42卷 314-322,I0003页

作者： nicolas Perciani de Moraes Maite Birkett de Campos Sanmartin Robson da Silva Rocha Abner de Siervo Marcos Roberto de Vasconcelos Lanza D.Amaranatha Reddy Lianqing Yu Liana Alvares Rodrigues Escola de Engenharia de Lorena-EEL/USP Estrada Municipal do Campinho S/NCEP 12602-810LorenaSao PauloBrazil Institute of Physics"Gleb Wataghin" Applied Physics DepartmentState University of Campinas13083-859CampinasSPBrazi instituto de Quimica de Sao Carlos Universidade de Sao PauloAv.Trab.Sao Carlense400-Parque Arnold SchimidtSao CarlosSP13566-590Spain Department of Sciences Indian Institute of Information Technology Design and ManufacturingKurnoolAndhra Pradesh518007India School of Materials Science and Engineering China University of PetroleumQingdao266580China

This paper aims to create visible light driven ternary photocatalysts using zinc oxide(ZnO),cerium(IV)oxide(CeO_(2)),and carbon xerogel(CX) as constituent materials.The use of CeO_(2) is based on the creation of direct-Z-scheme heterojunctions with the ZnO and the consequent diminishing of charge recombination,whereas the carbon xerogel inclusion is predicted to minimize bandgap energy,decrease electro n-hole reco mbination,and boost specific surface area.Furthermo re,the choice of the black-wattle tannin as a carbonaceous precursor was targeted at the development of an environmentally friendly and affordable composite.The existence of the hexagonal phase of zinc oxide and cubic structure of the cerium(IV) oxide in the ternary material was confirmed by X-ray diffractometry and X-ray photoelectron spectroscopy,with the latter also suggesting chemical bonding between the ZnO and the CX due to the creation of zinc oxycarbide complexes.The inclusion of the carbon xerogel provokes a significant modification in the morphology of the ternary material,resulting in an increased surface area and smaller particle aggregates.The CX/ZnO-CeO_(2) ternary composite obtains the highest photocatalytic efficiency among all the materials studied,degrading 100% of 4-chlorophenol under simulated sunlight and 68% under visible radiation,after 5 h.The increased photocatalytic activity can be attributed to the formation of direct Z-scheme heterojunctions between the semiconductors,higher visible light response,and higher specific surface area,as evidenced by the results obtained by active radical scavenging,chronoamperometry,diffuse reflectance spectroscopy,and N_(2) adsorption-desorption isotherms.

关键词： Zinc oxide Cerium(Ⅳ)oxide Carbon xerogel Photocatalysis Direct Z-scheme heterojunction 4-Chlorophenol Rare earths

There is life after coking for Ir nanocatalyst superlattices

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Nano Research 2022年第8期15卷 6969-6976页

作者： Antonio J.Martínez-Galera Haojie Guo Mariano D.Jiménez-Sánchez Stefano Franchi Kevin C.Prince José M.Gómez-Rodríguez Departamento de Física de la Materia Condensada Universidad Autónoma de MadridMadrid E-28049Spain instituto Nicolás cabrera Universidad Autónoma de MadridMadrid E-28049Spain Elettra-Sincrotrone Trieste S.C.p.A. in Area Science ParkBasovizza(Trieste)34149Italy Condensed Matter Physics Center(IFIMAC) Universidad Autónoma de MadridMadrid E-28049Spain

Achieving superior performance of nanoparticle systems is one of the biggest challenges in catalysis.Two major phenomena,occurring during the reactions,hinder the development of the full potential of nanoparticle catalysts:sintering and contamination with carbon containing species,sometimes called coking.Here,we demonstrate that Ir nanocrystals,arranged into periodic networks on hexagonal boron nitride(h-BN)supports,can be restored without sintering after contamination by persistent carbon.This restoration yields the complete removal of carbon from the nanocrystals,which keep their crystalline structure,allowing operation without degradation.These findings,together with the possibility of fine tuning the nanocrystals size,confer this nanoparticle system a great potential as a testbed to extract key information about catalysis-mediated oxidation reactions.For the case of the CO oxidation by O2,reaction of interest in environmental science and green energy production,the existence of chemical processes not observed before in other nanoparticle systems is demonstrated.

关键词： catalysis coke nanoparticles scanning tunneling microscopy(STM) X-ray photoemission spectroscopy(XPS)

Foliar persistence and residual activity of methoxyfenozide against beet armyworm （Lepidoptera： Noctuidae）

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Insect Science 2013年第6期20卷 734-742页

作者： Omar-Ulises Aguirre Ana-Mabel Martinez Jesus Campos-Garcia Luis-Antonio Hernaindez Jose-Isaac Figueroa Philippe Lobit Elisa Vinuela Juan-Manuel Chavarrieta Guy Smagghe Samuel Pineda instituto de Investigaciones Agropecuarias y Forestales Universidad Michoacana de San Nicolas de Hidalgo Michoacan instituto de Investigaciones Quimico Biologicas Universidad Michoacana de San Nicolas de Hidalgo Edif. B-3 Ciudad Universitaria CP 58030 Morelia Michoacan Mexico Proteccion de Cultivos Escuela Tecnica Superior de Ingenieros Agronomos Madrid E-28040 Spain Department of Crop Protection Faculty of Bioscience Engineering Ghent University Ghent B-9000 Belgium

A greenhouse study was conducted to investigate the persistence of methoxyfenozide in pepper （Capsicum annuum L.） foliage. An aqueous suspension of methoxyfenozide was sprayed on pepper plants at concentrations of 72 and 144 mg of active ingredient （a.i.）/L. Foliage was collected at different intervals of time （0, 3, 5, 10, 20, 30, 40, and 50 days） after the treatment, and the methoxyfenozide residue was measured by high-performance liquid chromatography. The foliage was also used in bioas- says to determine the residual toxicity on and the consumption rate of the third-instar larvae of the beet armyworm, Spodoptera exigua （Htibner）（Lepidoptera： Noctuidae）. The methoxyfenozide concentrations observed after 50 days had decreased to 19 and 69μg/g per sample, corresponding to a loss of 61% and 28% from the application concentrations of 72 and 144 mg a.i./L, respectively. When fitting a first-order kinetics degradation model, the half-life （DT50） of this compound was 76 days. Both application concentrations of methoxyfenozide caused a high mortality rate （〉97%） when the larvae were fed the pepper foliage collected at all of the time intervals. Lastly, at all of the time points, the consumption rate by the larvae was reduced to between 57% and 92% for both concentrations that were bioassayed. Our results indicate that, under the present greenhouse conditions, the degradation of methoxyfenozide was slower than that reported by other authors and that its residues were highly toxic to S. exigua larvae. The implications of these results for the management programs of this pest are discussed.

关键词： consumption rate foliar persistence methoxyfenozide residue residualactivity Spodoptera exigua

Erratum to:Influence of metal support in-plane symmetry on the corrugation of hexagonal boron nitride and graphene monolayers

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Nano Research 2019年第5期12卷 1217-1218页

作者： Antonio J.Martinez-Galera Jose M.Gomez-Rodriguez Departamento de Fisica de la Materia Condensada Universidad Autonoma de MadridMadrid E-28049Spain Condensed Matter Physics Center(IFIMAC) Universidad Autonoma de MadridMadrid E-28049Spain instituto nicolas cabrera Universidad Autonoma de MadridMadrid E-28049Spain

The writings of the text on the last line,left column on the 4^th page and the text on lines 8^th,10^th,11^th and 16^th in the 4^th paragraph,left column and on lines from 1st to 8^th in the 1st paragraph,right column on the 5^th page,and the text on line 4^th in the 1^st paragraph,left column on the 9^th page,and Fig.3 and its caption on the 5^th page in the original version of this article were unfortunately incorrect.

关键词： corrugation hexagonal boron nitride graphene monolayers

Laser Wavelength Estimation Method Based on a High-Birefringence Fiber Loop Mirror

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Photonic Sensors 2019年第1期9卷 89-96页

作者： Ricardo I.ALVAREZ-TAMAYO Patricia PRIETO-CORTES Manuel DURAN-SANCHEZ Baldemar IBARRA-ESCAMILLA Antonio BARCELATA-PINZON Evgeny A.KUZIN Faculty of Physical-Mathematical Sciences CONACYT-Universidad Autonoma de Nuevo LeonSan Nicolas de los Garza 66451Mexico Faculty of Physical-Mathematical Sciences Universidad Autonoma de Nuevo LednSan Nicolas de los Garza 66451 Mexico Optics department CONA CYT-Instituto Nacional de AstrofisieaOptica y EleetronieaTonantzintla 72480Mexico Optics department Instituto Nacional de AstrofisicaOptica y ElectronicaTonantzintla 72480Mexico Mechatronics division Universidad Tecnologica de PueblaPuebla 72300Mexico

A simple method for the estimation of the wavelength of a fiber laser system is proposed. The method is based on the use of a high-birefringence-fiber loop mirror(HBFLM).The HBFLM exhibits a periodic transmission/reflection spectrum whose spectral characteristics are determined by the length and temperature of the high-birefringence fiber(HBF).Then,by the previous characterization of the HBFLM spectral transmission response,the central wavelength of the generated laser line can be estimated.By using a photodetector,the wav.elength of the laser line is estimated during an HBF temperature scanning by measuring the temperature at which the maximum transmitted power of the HBFLM is reached.The proposed method is demonstrated in a linear cavity tunable Er/Yb fiber laser.This method is a reliable and low-cost alternative for laser wavelength determination in short wavelength ranges without the use of specialized and expensive equipment.

关键词： Wavelength meter fiber lasers fiber optical loop mirror high-birefringence fiber

Influence of metal support in-plane symmetry on the corrugation of hexagonal boron nitride and graphene monolayers

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Nano Research 2018年第9期11卷 4643-4653页

作者： Antonio d. Martinez-Galera Jose M. Gomez-Rodriguez Departamento de Fisica de la Matefia Condensada Universidad Autonoma de Madrid Madrid E-28049 Spain Condensed Matter Physics Center (IFIMAC) UniversidadAutdnoma de Madrid Madrid E-28049 Spain instituto Nicolds cabrera Universidad Autonoma de Madrid Madrid E-28049 Spain

Predicting the properties of two-dimensional （2D） materials as graphene and hexagonal boron nitride （h-BN） monolayers after their growth on any given substrate is a major challenge. While the influence of the electron configuration of the atoms of the underlying surface is well-understood, the effect of substrate geometry still remains unclear. The structural properties of h-BN monolayers grown on a rectangularly packed Rh（110） surface were characterized in situ by ultrahigh vacuum scanning tunneling microscopy and were compared to those that this material exhibits when grown on substrates showing different crystallographic orientations. Although the h-BN monolayer grown on Rh（110） was dominated by a unique quasiunidimensional moir6 pattern, suggesting considerable interface interaction, the moir6 corrugation was unexpectedly smaller than those reported for strongly interacting interfaces with hexagonal-terminated substrates, owing to differences in the possible binding landscapes at interfaces with differently oriented substrates. Moreover, a rule was derived for predicting how interface corrugation and the existence and extent of subregions within moir6 supercells containing favorable sites for orbital mixing between h-BN monolayers and their supports depend on substrate symmetry. These general symmetry considerations can be applied to numerous 2D materials, including graphene, thereby enabling the prediction of how substrate choice determines the properties of these materials. Furthermore, they could also provide new routes for tuning 2D material properties and for developing nanotemplates showing different geometries for Krowing adsorbate superlattices.

关键词： hexagonal boron nitride graphene two-dimensional materials scanning tunneling microscopy moire superstructures nanotemplates

正癸烷+正戊醇,+1-己醇,+庚醇二元混合物在293.15到363.15K和大气压力下的密度和粘度（英文）

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Chinese Journal of Chemical Engineering 2015年第3期23卷 559-571页

作者： Alejandro Estrada-Baltazar Micael Gerardo Bravo-Sanchez Gustavo Arturo Iglesias-Silva Juan Francisco Javier Alvarado Edgar Omar Castrejon-Gonzalez Mariana Ramos-Estrada Department of Chemical Engineering instituto Tecnologico de Celaya Faculty of Chemical Engineering Universidad Michoacana de San Nicolas de Hidalgo

Densities(ρ) and dynamic viscosities(η) for three binary mixtures of n-decane with 1-pentanol,1-hexanol and1-heptanol are presented at temperatures from 293.15 to 363.15 K and atmospheric pressure over the entire composition range.The density and viscosity are measured using a vibrating tube densimeter and a cylindrical Couette type rotating viscometer,respectively.Excess molar volumes(V^E),viscosity deviations(△η) and excess Gibbs energy of activation of viscous flow(△G^(*E)) are calculated from the experimental measurements.Intermolecular and structural interactions are indicated by the sign and magnitude of these properties.Partial molar volumes and infinity dilution molar partial volumes are also calculated for each binary system.These results are correlated using Redlich-Kister type equations.

关键词：振动管密度计二元混合物动态粘度大气压力正戊醇正癸烷温度庚醇