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Investigation of pore structure alteration and permeability enhancement of shale matrix by supercritical water treatment after hydraulic fracturing

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petroleum 2024年第2期10卷 265-274页

作者： Yili Kang Peisong Li Wangkun Cao Mingjun Chen Lijun You Jiang Liu Zhehan Lai State Key Laboratory of Oil and Gas Reservoir Geology and Exploitation Southwest Petroleum University institute of Engineering Technology PetroChina Coalbed Methane Company Limited Chemical and petroleum Engineering University of Calgary

Shale gas reservoirs are unconventional tight gas reservoirs, in which horizontal wells and hydraulic fracturing are required to achieve commercial development. The fracture networks created by hydraulic fracturing can increase the drainage area extensively to enhance shale gas recovery. However, large volumes of fracturing fluid that is difficult to flow back to the surface and remained in the shale formation, will inevitably lead to damages of the shale formations and limit the effectiveness of *** water(SCW) treatment after hydraulic fracturing is a new method to enhance shale gas recovery by using appropriate heat treatment methods to the specific formation to convert the retained fracturing fluid into a supercritical state(at temperatures in excess of 373.946°C and pressures in excess of 22.064 MPa). An experiment was conducted to simulate the reaction between shale and SCW, and the capacity of SCW treatment to enhance the permeability of the shale was evaluated by measuring the response of the shale porosity and permeability on SCW treatment. The experimental results show that the shale porosity and permeability increase by 213.43% and 2198.37%, respectively. The pore structure alteration and permeability enhancement of the shale matrix were determined by analyzing the changes in pore structure and mineral composition after SCW treatment. The mechanisms that affect pore structure and mineral composition include oxidative catalysis decomposition of organic matters and reducing minerals, acid-catalyzed decomposition of carbonate minerals and feldspar minerals, hydrothermal catalysis induced fracture extension and cementation weakening induced fracture *** treatment converts harm into a benefit by reducing the intrusion of harmful substances into the shale formation, which will broaden the scope and scale of shale formation stimulation.

关键词： Shale gas Formation damage control Formation heat treatment Supercritical water

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Effect of alumina and silica nanocomposite based on polyacrylamide on light and heavy oil recovery in presence of formation water using micromodel

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petroleum 2024年第2期10卷 338-353页

作者： Ashkan Maleki Behnam Sedaee Alireza Bahramian Sajjad Gharechelou Nahid Sarlak Arash Mehdizad Mohammad reza Rasaei Aliakbar Dehghan Science and Research Branch Islamic Azad University institute of petroleum Engineering School of Chemical Engineering University of Tehran School of Geology College of Science University of Tehran Department of chemistry Lorestan University Iranian Offshore Oil Company

Increasing world request for energy has made oil extraction from reservoirs more desirable. Many novel EOR methods have been proposed and utilized for this purpose. Using nanocomposites in chemical flooding is one of these novel methods. In this study, we investigated the impact of six injection solutions on the recovery of light and heavy oil with the presence of two different brines as formation water using a homogenous glass micromodel. All of the injection solutions were based on a 40,000 ppm Na Cl synthetic seawater(SSW), one of which was additive free and the others were prepared by dispersing nanocomposite silica-based polyacrylamide(NCSP), nanocomposite alumina-based polyacrylamide(NCAP), the combination of both nanocomposites silica and alumina based on polyacrylamide(NCSAP),surfactant(CTAB) and polyacrylamide(PAM) with a concentration of 1000 ppm as additives. The Stability of nanocomposites was tested against the salinity of the brine and temperature using salinity and DSC tests which were successful. Alongside stability tests, IFT, contact angle and oil recovery measurements were made. Visual results revealed that in addition to the effect of silica and alumina nanocomposite in reducing interfacial tension and wettability alteration, control of mobility ratio caused a major improvement in sweeping efficiency and oil recovery. According to the sweeping behavior of injected fluids, it was found that the main effect of surfactant was wettability alteration, for polyacrylamide was mobility control and for nanocomposites was the reduction of interfacial tension between oil and injected fluid, which was completely analyzed and checked out. Also, NCSAP with 95.83% and 70.33% and CTAB with 84.35% and 91% have the highest light oil recoveries at 250,000 ppm and 180,000 ppm salinity, respectively which is related to the superposition effect of interactions between nanocomposites, solution and oil. Based on our results it can be concluded that the most effective me

关键词： Enhanced oil recovery Micromodel Polyacrylamide Nanocomposite Salinity Alumina and silica nanoparticles

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Application status and prospect of ionic liquids in oilfield chemistry

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petroleum 2024年第1期10卷 11-18页

作者： Jinsheng Sun Zhuoyang Xiu Li Li Kaihe Lv Xianfa Zhang Zonglun Wang Zhiwen Dai Zhe Xu Ning Huang Jingping Liu School of petroleum Engineering China University of Petroleum (East China) CNPC Engineering Technology R&D Company Limited Oil & Gas Technology Research institute of Changqing Oilfield Company

The ionic liquid, as a new treatment agent, has been increasingly applied in oil fields due to its strong temperature resistance, good solubility and high surface activity. In this paper, we systematically discuss the action mechanism and application effect of ionic liquids in oilfield chemistry. Ionic liquids can inhibit shale hydration expansion and reduce fluid loss through adsorption and intercalation, inhibit the formation of natural gas hydrate through imidazole five-membered ring structure as a space barrier, reduce viscosity of heavy oil by breaking chemical bonds of heavy oil macromolecules and charge transfer,improve oil displacement efficiency by forming ions pairs with carboxyl groups in crude oil, demulsify by forming channels between dispersed water droplets, acidify the formation by reacting with water to produce acid, interacts with organic material through weak hydrogen bonds and extracts it from oilfield wastewater, desulphurize by inserting sulfide molecules into the “stack” structure and form liquid inclusion complex, inhibit corrosion by forming a protective film on the metal surface. Based on the above aspects, the development direction of ionic liquids is proposed. The application of ionic liquids in oilfield chemistry is still in its infancy. It is urgent to fully explore the application performance of ionic liquids in oilfield chemistry, which also provides theoretical and technical supports for efficient reservoir development.

关键词： Ionic liquids Oilfield chemistry Shale inhibitor Drilling fluid

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Ti_(3)C_(2)T_(x) MXene/carbon composites for advanced supercapacitors:Synthesis,progress,and perspectives

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Carbon Energy 2024年第2期6卷 113-142页

作者： Yanqing Cai Xinggang Chen Ying Xu Yalin Zhang Huijun Liu Hongjuan Zhang Jing Tang College of Materials Science and Engineering North China University of Science and TechnologyTangshanChina Hebei Iron and Steel Laboratory North China University of Science and TechnologyTangshanChina Songshan Lake Materials Laboratory DongguanChina Shanghai Key Laboratory of Green chemistry and Chemical Processes School of Chemistry and Molecular EngineeringEast China Normal UniversityShanghaiChina State Key Laboratory of petroleum Molecular and Process Engineering(SKLPMPE) Sinopec Research Institute of Petroleum Processing Co.Ltd.BeijingChina institute of Eco-Chongming ShanghaiChina

MXenes are a family of two-dimensional(2D)layered transition metal carbides/nitrides that show promising potential for energy storage applications due to their high-specific surface areas,excellent electron conductivity,good hydrophilicity,and tunable *** various types of MXenes,Ti_(3)C_(2)T_(x) is the most widely studied for use in capacitive energy storage applications,especially in supercapacitors(SCs).However,the stacking and oxidation of MXene sheets inevitably lead to a significant loss of electrochemically active *** overcome such challenges,carbon materials are frequently incorporated into MXenes to enhance their electrochemical *** review introduces the common strategies used for synthesizing Ti_(3)C_(2)T_(x),followed by a comprehensive overview of recent developments in Ti_(3)C_(2)T_(x)/carbon composites as electrode materials for ***_(3)C_(2)T_(x)/carbon composites are categorized based on the dimensions of carbons,including 0D carbon dots,1D carbon nanotubes and fibers,2D graphene,and 3D carbon materials(activated carbon,polymer-derived carbon,etc.).Finally,this review also provides a perspective on developing novel MXenes/carbon composites as electrodes for application in SCs.

关键词： electrochemical performance MXene/carbon composites supercapacitors

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Experimental analysis of matrix moveable oil saturation in tight sandstone reservoirs of the south Ordos Basin,China

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Energy Geoscience 2024年第1期5卷 184-195页

作者： Ting Xu Jun Pu Xuejie Qin Yi Wei Science and Technology Development Department Petroleum Exploration&Production Research InstituteSINOPECBeijing100083China Center Research Department of North China petroleum Exploration&Production Research institute SINOPECBeijing100083China Oil Field Development Department Petroleum Exploration&Production Research InstituteSINOPECBeijing100083China

Tight oil reservoirs in the south Ordos Basin are characterized by fractured,heterogeneous oil-bearing strata(an oil saturation of less than 55%on average),normal pressure(0.8±)and extra-low permeability(less than 0.3 mD).In the Chang 8 tight sandstone reservoir in Honghe oilfield,micro-and nanopores,especially those with a pore-throat radius of less than 1 mm,account for more than 90%.Fluid flow in the matrix is non-linear and crude oil flow rates are very low under normal pressure *** improved understanding of oil mobility in a tight matrix is key to further development of normalpressure tight-oil resources in the continental *** this study,constant-velocity and high-pressure mercury injection experiments were conducted using samples of typical tight sandstone cores obtained from the south of Ordos Basin.A new method for reconstructing the full-scale pore-throat distribution characteristics of tight sandstone reservoirs was established successfully,based on which multistage centrifugal tests,tests of low-pressure differential displacement of oil by water,and nuclear magnetic resonance tests were conducted in order to obtain the distribution characteristics of moveable fluid in different *** moveable oil saturation(MOS)and degree of oil recovery(*** of accumulative oil production to producing geologic reserves)of the core samples under different differential pressures for displacement were *** for the tight oil reservoirs in the south Ordos Basin,the moveable fluids are mainly stored in sub-micron(0.10-0.5 mm)*** Type I reservoirs(k>0.1 mD),the volume percentage of moveable fluid in pores with a radius larger than 0.5 mm is relatively high(greater than 40%).The degree of oil recovery of water flooding serves as the basis for forecasting recoverable reserves for tight oil *** reserves under water flooding,mainly occur in pores with a radius greater than 0.5 *** contribution of Type I reserves to oil pro

关键词： Tight reservoir Pore-throat structure Moveable fluid volume Moveable oil saturation(MOS) Waterflooding oil recovery South Ordos basin

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Chemical, carbon and sulfur isotopic compositions constrain the origin of Upper Carboniferous-Lower Triassic gases in eastern Sichuan Basin, SW China

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Science China Earth Sciences 2024年第10期67卷 3169-3185页

作者： Chunfang CAI Ilya KUTUZOV Wenhua MEI Daowei WANG Bing LUO Shipeng HUANG Bing HE Alon AMRANI China University of petroleum National Key Lab Petroleum Resource & Engineering State Key Laboratory of Lithospheric and Environmental Coevolution Institute of Geology and Geophysics Chinese Academy of Sciences College of Earth and Planetary Sciences University of Chinese Academy of Sciences institute of Earth Sciences The Hebrew University Yulin University Research institute of Exploration and Development Southwest Oil & Gas Field Company Petro China Petro China Research Institute of Petroleum Exploration and Development

Methane dominated gas is one of the cleanest energy resources; however, there is no direct method to determine its source rock. Natural gases produced from the eastern Sichuan Basin together with seismic data were studied for their sources and secondary alteration by thermochemical sulfate reduction（TSR）. Our results demonstrate that Upper Permian to Lower Triassic（P3ch-T1f） gases in the surrounding of the Kaijiang-Liangping area show volatile organic sulfur compounds（VOSCs） δ34S values close to those of the associated H2S, and may have been altered by methane-dominated TSR, resulting in positive shift in methane δ13C1values with increasing TSR extents. Other（or group 2） gases produced from the P3ch-T1f reservoirs from the southern area and the Upper Carboniferous to Middle Permian（C2h-P2q） from the eastern Sichuan Basin are not significantly changed by TSR, show similar δ34S values between the kerogens and some VOSCs, and may have been derived from the Lower Silurian and Middle Permian source rocks. This study demonstrates a case for the first time showing the δ34S values of VOSCs can be used as a tool for direct correlation between non-TSR altered gas and source rocks. Methane-dominated gas pools can be found using gas and source rock geochemistry combined with seismic data.

关键词： Sulfur isotopes Volatile organic sulfur compounds Thermochemical sulfate reduction Sichuan Basin Gas-source rock correlation

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Research on a TOPSIS energy efficiency evaluation system for crude oil gathering and transportation systems based on a GA-BP neural network

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petroleum Science 2024年第1期21卷 621-640页

作者： Xue-Qiang Zhang Qing-Lin Cheng Wei Sun Yi Zhao Zhi-Min Li Key Lab of Ministry of Education for Enhancing the Oil and Gas Recovery Ratio Northeast Petroleum UniversityDaqing163318HeilongjiangChina China petroleum Pipeline Material and Equipment Co. LtdLangfang065000HebeiChina Research institute of petroleum Engineering and Technology Sinopec Northwest Oilfield CompanyUrumqi830011XinjiangChina

As the main link of ground engineering,crude oil gathering and transportation systems require huge energy consumption and complex *** is necessary to establish an energy efficiency evaluation system for crude oil gathering and transportation systems and identify the energy efficiency *** this paper,the energy efficiency evaluation system of the crude oil gathering and transportation system in an oilfield in western China is *** with the big data analysis method,the GA-BP neural network is used to establish the energy efficiency index prediction model for crude oil gathering and transportation *** comprehensive energy consumption,gas consumption,power consumption,energy utilization rate,heat utilization rate,and power utilization rate of crude oil gathering and transportation systems are *** the efficiency and unit consumption index of the crude oil gathering and transportation system,the energy efficiency evaluation system of the crude oil gathering and transportation system is established based on a game theory combined weighting method and TOPSIS evaluation method,and the subjective weight is determined by the triangular fuzzy analytic hierarchy *** entropy weight method determines the objective weight,and the combined weight of game theory combines subjectivity with objectivity to comprehensively evaluate the comprehensive energy efficiency of crude oil gathering and transportation systems and their ***,the weak links in energy utilization are identified,and energy conservation and consumption reduction are *** above research provides technical support for the green,efficient and intelligent development of crude oil gathering and transportation systems.

关键词： Crude oil gathering and transportation system GA-BP neural network Energy efficiency evaluation TOPSIS evaluation method Energy saving and consumption reduction

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Seismic identification and characterization of complex storage space oil and gas reservoirs

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Applied Geophysics 2024年第3期21卷 606-615,620页

作者： XiaoYu-Jiang Tao Song Li Deng-Gan Xiao Yue-Zhou Jing Liang Lele-Wei Ming Zhang Xiaofeng-Dai Research institute of petroleum Exploration&Development Beijing100083China

To predict complex reservoir spaces(with developed caves,pores,and fractures),based on the results of full-azimuth depth migration processing,we adopted reverse weighted nonlinear inversion to improve the accuracy of porous reservoir *** imaging three-parameter wavelet transform technology was used to accurately predict small-scale cave *** joint inversion method of velocity and amplitude anisotropy was developed to improve the accuracy of small and medium-sized fracture *** results of multiscale fracture modeling and characterization,interwell connectivity analysis,and connection path prediction are consistent with the production ***,based on the above prediction findings,favorable reservoir development areas were *** above ideas and strategies have great application value for the efficient exploration and development of complex storage space reservoirs and the optimization of high-yield well locations.

关键词： complex storage space fracture prediction reservoir prediction cave prediction

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In situ modification of heavy oil catalyzed by nanosized metal-organic framework at mild temperature and its mechanism

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Chinese Journal of Chemical Engineering 2024年第3期67卷 166-173页

作者： Li Wang Ji-Xiang Guo Rui-Ying Xiong Chen-Hao Gao Xiao-Jun Zhang Dan Luo The Unconventional Oil and Gas institute China University of Petroleum-BeijingBeijing 102200China Beijing institute of Nanoenergy and Nanosystems Chinese Academy of SciencesBeijing 101400China

Two catalysts, nano-sized cobalt-metal-organic framework(Co-MOF) and nickel(Ni)-MOF, were successfully prepared by the modification method. Tetralin(C10H12) was used as the hydrogen donor for the catalytic cracking and hydrogenation modification study of the dehydrated crude oil from the Shengli Oilfield. The optimal reaction conditions were determined through orthogonal experiments, and the components of the crude oil and modified oil samples were analyzed. The results revealed that the nanoMOF catalysts were successfully prepared and exhibited high catalytic activity. They could catalyze the cracking of large molecules in heavy oil at mild temperatures(<300°C), leading to the decomposition of the hydrogen donor. When the mass fraction of the catalyst was 0.2%, the mass fraction of the hydrogen donor was 1%, and the reaction temperature was 280°C, the Ni-MOF showed the best catalytic viscosity reduction effect. It could reduce the viscosity of heavy oil at 50°C from 15761.9 m Pa.s to 1266.2 m Pa.s,with a viscosity reduction rate of 91.97%. The modification effect of Co-MOF was the next best, which could reduce the viscosity of heavy oil to 2500.1 m Pa.s with a viscosity reduction rate of 84.14%. Molecular dynamics simulations revealed a strong interaction force between the MOF surface and asphaltene molecules. In the process of heavy-oil catalytic hydrogenation, the nano-MOF catalyst exhibited high catalytic activity. On the one hand, the empty d orbitals outside the metal atoms in the catalyst could polarize the carbon atoms in the organic matter, accelerating the breaking of long chains. On the other hand, the metal atoms in the catalyst could bond with the carbon σ bonds, breaking the carbon-carbon bonds. This disrupted the structure of the recombined components in the crude oil, irreversibly reducing the viscosity of the heavy oil and improving its fluidity.

关键词： Nano-sized MOF petroleum Viscosity reduction Catalyst Nanomaterials

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A semi-analytical model for coupled flow in stress-sensitive multi-scale shale reservoirs with fractal characteristics

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petroleum Science 2024年第1期21卷 327-342页

作者： Qian Zhang Wen-Dong Wang Yu-Liang Su Wei Chen Zheng-Dong Lei Lei Li Yong-Mao Hao Key Laboratory of Unconventional Oil&Gas Development(China University of petroleum(East China)) Ministry of EducationQingdao266580ShandongChina School of petroleum Engineering China University of Petroleum(East China)Qingdao266580ShandongChina Shale Oil Development Branch Changqing Oilfield CompanyPetroChinaQingyang745708GansuChina PetroChina Research institute of petroleum Exploration&Development Beijing100083China

A large number of nanopores and complex fracture structures in shale reservoirs results in multi-scale flow of oil. With the development of shale oil reservoirs, the permeability of multi-scale media undergoes changes due to stress sensitivity, which plays a crucial role in controlling pressure propagation and oil flow. This paper proposes a multi-scale coupled flow mathematical model of matrix nanopores, induced fractures, and hydraulic fractures. In this model, the micro-scale effects of shale oil flow in fractal nanopores, fractal induced fracture network, and stress sensitivity of multi-scale media are considered. We solved the model iteratively using Pedrosa transform, semi-analytic Segmented Bessel function, Laplace transform. The results of this model exhibit good agreement with the numerical solution and field production data, confirming the high accuracy of the model. As well, the influence of stress sensitivity on permeability, pressure and production is analyzed. It is shown that the permeability and production decrease significantly when induced fractures are weakly supported. Closed induced fractures can inhibit interporosity flow in the stimulated reservoir volume (SRV). It has been shown in sensitivity analysis that hydraulic fractures are beneficial to early production, and induced fractures in SRV are beneficial to middle production. The model can characterize multi-scale flow characteristics of shale oil, providing theoretical guidance for rapid productivity evaluation.

关键词： Multi-scale coupled flow Stress sensitivity Shale oil Micro-scale effect Fractal theory

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