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Journal of Iron and steel Research International 2024年第8期31卷 1886-1899页

作者： Zhan-peng Tie Xue-yuan Jiang Hai-yan Tang ·Gen Li Yu-hang Wang Jia-quan Zhang School of Metallurgical and Ecological engineering University of Science and Technology BeijingBeijing 100083China Continuous Casting Business Section CISDI Engineering Co.Ltd.Chongqing 401122China Special steel institute Central Iron and Steel Research Institute Co.Ltd.Beijing 100081China

The influence of Al content(0.0053,0.0171,and 0.0578 wt.%)on the modification behavior of non-metallic inclusions in 20CrMoVTiB steel treated with rare earth elements was studied through high-temperature experiments and thermodynamic *** results showed that the modification products varied with the Al content in steel under 0.01 wt.%of Ce *** formation sequence of typical rare earth inclusions in steel with the increase in Al content was Ce_(2)O_(3)→CeAlO_(3)→CeAl_(11)O_(18),and the final stable products were highly Al content *** the Al content was 0.0053 wt.%,the stable phase in steel was Ce2O3;while the[Al]reached 0.0171 wt.%,the stable phase became CeA1O_(3).As the A1 content reached 0.0578 wt.%,CeAl_(11)O_(18) became the stable *** a result,increasing the Al content could inhibit the precipitation of Ce_(2)O_(3) inclusions in steel while promote the formation of CeAIO3 and CeAl_(11)O_(18) *** addition,both Ca treatment and Ce treatment could effectively refine the size of inclusions in steel by changing their ***,the feeding amount of Ca wire into molten steel should be appropriately reduced under the condition of adding Ce simultaneously,which is expected to be beneficial for an improved Ce treatment effect.

关键词： Rare earth Al content steel Inclusion Thermodynamics Ca treatment

Characteristics and stability of oxide+carbonitride in H13 steel at 1250℃

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Journal of Iron and steel Research International 2024年第1期31卷 134-142页

作者： Xiao-lin Sun Han-jie Guo Jing Guo Fei Wang Dong Xu Gao-yang Song Shuai Wang School of Materials Science and engineering Hebei University of EngineeringHandan056038HebeiChina School of Metallurgical and Ecological engineering University of Science and Technology BeijingBeijing100083China High Temperature Materials Research institute Central Iron and Steel Research Institute Co.Ltd.Beijing100081China Technology Innovation Center for High Quality Cold Heading steel of Hebei Province Hebei University of EngineeringHandan056038HebeiChina

The morphology,size,quantity,and composition of complex oxide+carbonitride in H13 steel held at 1250℃for 5,10,and 15 h were *** results show that the ratio and number of complex carbonitrides with cores in H13 steel are gradually increased when holding at 1250℃compared with those in the original H13 steel,and the core size *** are one or more oxide cores in(Ti_(x),V_(1-x))(Cy,N_(1-y)),including xCaO·zAl_(2)O_(3),xCaO·yMgO·zAl_(2)O_(3),and CaO after holding at 1250℃,in addition to MgO·Al_(2)O_(3)and Al_(2)O_(3)in the original *** equilibrium temperature for(Ti_(x),V_(1-x))(Cy,N_(1-y))precipitation at the solidification front and decomposition in the solid state was theoretically analyzed,which was affected by the x value and the product of Ti and N contents in H13 ***,the composition of(Ti_(x),V_(1-x))(Cy,N_(1-y))is influenced by the oxide *** is convinced that(Ti_(x),V_(1-x))(Cy,N_(1-y))with oxide cores has a higher stability,especially for oxides with a high Al_(2)O_(3)*** treatment at high temperature facilitates a more reasonable analysis of oxide+carbonitride,and the generation mechanism of oxide+carbonitride was discussed.

关键词： Complex carbonitride Decomposition Oxide core Characteristic Stability

Multi-performance evaluation of high-throughput accelerated corrosion test for high-strength low-alloy 921A steel

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Journal of Iron and steel Research International 2024年第5期31卷 1260-1278页

作者： Cong-cong Du Ming-hua Qin Zhan-fang Wu Dong-ling Li Lei Zhao Xiang-yang Li Hai-zhou Wang Beijing Advanced Innovation Center for Materials Genome engineering National Center for Materials Service SafetyUniversity of Science and Technology BeijingBeijing100083China China Iron and steel Research institute Group Co. Ltd.Beijing100081China Beijing Advanced Innovation Center for Materials Genome engineering Central Iron and Steel Research InstituteBeijing100081China

The corrosion behavior of high-strength low-alloy 921A steel in a simulated marine atmospheric environment was studied using a high-throughput experimental *** corrosion behavior,corrosion morphology,and corrosion products of 921A steels were analyzed using various techniques,including corrosion mass loss method,polarization curve,white-light interferometry,scanning electron microscopy,energy-dispersive spectrometry,microbeam X-ray fluorescence spectrometry,X-ray diffraction technique,and X-ray photoelectron *** test results indicated that 921A steel exhibits better corrosion resistance than Q450NQR1 steel in simulated harsh atmospheric environments,as evidenced by a lower corrosion mass loss rate throughout the corrosion *** corrosion products of both steels consisted ofα-FeOOH,Fe_(3)O_(4),andγ-FeOOH,withα-FeOOH being more prevalent in the rust layer of 921A steel than in Q450NQR1 *** inner rust layer of 921A steel also exhibited an appositional enrichment region of Cr,Ni,Mo,and V,leading to its superior corrosion resistance compared to that of Q450NQR1 *** efficacy of high-throughput accelerated corrosion experimental methods was highlighted for evaluating the corrosion resistance of steel materials in harsh environmental *** findings suggest that 921A steel exhibits better corrosion resistance compared to Q450NQR1 steel and has the potential to be more suitable in harsh marine atmospheric *** characterization of the rust layer structures and composition reveals the parallel enrichment of certain elements in the inner rust layer of 921A steel,which enhances its corrosion resistance.

关键词： Atmospheric corrosion High-throughput experimental method High-strength low-alloy steel Corrosion characteristics Rust layer Element enrichment

Achieving strength–ductility synergy in novel paramagnetic Fe-based medium-entropy alloys through deep cryogenic deformation

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Rare Metals 2024年第9期43卷 4493-4507页

作者： Hu-Wen Ma Yan-Chun Zhao Li Feng Tian-Zeng Liu Zhi-Qi Yu Bo Jin Wang-Chun Duan Peter K.Liaw Dong Ma State Key Laboratory of Advanced Processing and Recycling of Non-Ferrous Metals Lanzhou University of Technology Wenzhou Pump and Valve engineering Research institute Lanzhou University of Technology Iron and steel Research institute Jiuquan Iron and Steel Corporation Lanzhou Resources and Environment Voc-Tech University Department of Materials Science and engineering The University of Tennessee Neutron Science Center Songshan Lake Materials Laboratory

Cryogenic pre-deformation treatment has been widely used to effectively improve the comprehensive mechanical properties of steels and novel metals. However,the dislocation evolution and phase transformation induced by different degrees of deep cryogenic deformation are not yet fully elucidated. In this study, the effects of multiple cryogenic pre-treatments on the mechanical properties and deformation mechanisms of a paramagnetic Fe63.3Mn14-Si9.1Cr9.8C3.8medium-entropy alloy（MEA） were investigated, leading to the discovery of a pretreated MEA that exhibits exceptional mechanical properties, including a fracture strength of 3.0 GPa, plastic strain of 26.1% and work-hardening index of 0.57. In addition, X-ray diffraction（XRD） and transmission electron microscopy（TEM）analyses revealed that multiple cryogenic pre-deformation treatments significantly increased the dislocation density of the MEA(from 9 × 1015to 4 × 1016m-2after three pretreatments), along with a transition in the dislocation type from predominantly edge dislocations to mixed dislocations（including screw-and edge-type dislocations）. Notably, this pretreated MEA retained its paramagnetic properties（μr< 1.0200） even after fracture. Thermodynamic calculations showed that cryogenic pretreatment can significantly reduce the stacking fault energy of the MEA by a factor of approximately four(i.e., from 9.7 to2.6 m J·m-2), thereby activating the synergistic effects of transformation-induced plasticity, twinning-induced plasticity and dislocation strengthening mechanisms. These synergistic effects lead to simultaneous strength and ductility enhancement of the MEA.

关键词： Deep cryogenic transformation Dislocation evolution Iron-based medium-entropy alloys Phase transformation Stacking fault energy

Microstructure Modification and Ductility Improvement for TaMoNbZrTiAl Refractory High Entropy Alloys via Increasing Ti Content

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Acta Metallurgica Sinica(English Letters) 2024年第7期37卷 1186-1200页

作者： Yujing Zhou Siyi Peng Yueling Guo Xiaoxiang Wu Changmeng Liu Zhiming Li School of Mechanical engineering Beijing Institute of TechnologyBeijing100081China Shagang School of Iron and steel Soochow UniversitySuzhou215137China School of Materials Science and engineering Central South UniversityChangsha410083China

Here, the composition of TaMoNbZrTiAl refractory high entropy alloy (RHEA) is optimized by increasing Ti content to improve its mechanical property especially the ductility, through comparing two RHEAs with different Ti content. The RHEAs contain two body-centered-cubic (BCC) phases. The BCC phase in the dendritic region is rich in Ta, Mo and Nb, and the BCC phase in the interdendritic region is enriched in Zr, Ti and Al. The as-cast RHEA with a higher Ti content remains dendritic microstructures, and Ti is mainly enriched in the interdendritic region. After annealing treatment at 1300 ℃ for 48 h, the dendritic microstructures change into equiaxed-grain morphology, accompanied by needle-like micron precipitates at grain boundaries in the RHEA with higher Ti content. For the as-cast RHEAs, the fracture strain increases by ~ 6.6% and the uniform plastic strain increases by ~ 5.9% at the compression test due to the increase of Ti content. Our work offers a reference for the composition design of RHEAs and makes a preliminary exploration of the optimization of the microstructures and mechanical properties.

关键词： Refractory high entropy alloys Solidification Grain morphology Microstructure Mechanical property

Review on the plastic instability of medium -Mn steels for identifying the formation mechanisms of Lüders and Portevin -Le Chatelier bands

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International Journal of Minerals,Metallurgy and Materials 2024年第6期31卷 1285-1297页

作者： Bin Hu Han Sui Qinghua Wen Zheng Wang Alexander Gramlich Haiwen Luo School of Metallurgical and Ecological engineering University of Science and Technology BeijingBeijing 100083China steel institute RWTH Aachen UniversityIntzestraße 152072 AachenGermany

Plastic instability,including both the discontinuous yielding and stress serrations,has been frequently observed during the tensile deformation of medium-Mn steels(MMnS)and has been intensively studied in recent ***,research results are controversial,and no consensus has been achieved regarding the ***,we first summarize all the possible factors that affect the yielding and flow stress serrations in MMnS,including the morphology and stability of austenite,the feature of the phase interface,and the deformation ***,we propose a universal mechanism to explain the conflicting experimental *** conclude that the discontinuous yielding can be attributed to the lack of mobile dislocation before deformation and the rapid dislocation multiplication at the beginning of plastic ***,the results show that the stress serrations are formed due to the pinning and depinning between dislocations and interstitial atoms in ***-induced martensitic transformation,influenced by the mechanical stability of austenite grain and deformation parameters,should not be the intrinsic cause of plastic ***,it can intensify or weaken the discontinuous yielding and the stress serrations by affecting the mobility and density of dislocations,as well as the interaction between the interstitial atoms and dislocations in austenite grains.

关键词： medium manganese steel discontinuous yielding stress serrations retained austenite dislocations

Particle size dependence of the microsegregation and microstructure in the atomized Ni-based superalloy powders:Theoretical and experimental study

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Journal of Materials Science & Technology 2024年第4期171卷 54-65页

作者： Jikang Li Mingsheng Yang Yunfei Cai Yuanyuan Zhang Qingshuai Feng Jiantao Liu Tong Liu Key Laboratory of Aerospace Materials and Performance(Ministry of Education)School of Materials Science and engineering Beihang UniversityBeijing 100191China Central Iron and steel Research institute Beijing 100081China

The microstructure and microsegregation of atomized powder,which depend on their sizes,are of great importance to the mechanical properties of the consolidated bulk ***,it is necessary to reveal the relationship between particle size and powder *** effects of particle size on the so-lidification characterization of the atomized Ni-based superalloy powders were studied via finite element *** on the simulations,a model was developed to predict the microsegregation and mi-crostructure of atomized powders with different sizes and study the influence of thermal history on the powder attributes during the atomization *** radiation heat transfer and temperature gradi-ent within the rapid solidification alloy powders were taken into account in this *** validating the accuracy of the model,the predictions of the present model were compared with the microsegregation and microstructure of the specific size powder close to the screen mesh *** results showed that mi-crostructure depended primarily on the temperature gradient within the powder,while the solidification rate had a more significant effect on the *** model predicted microstructure features in agreement with the experiment,and for microsegregation,the deviations of prediction for most ele-ments were less than 10%.This work provides a new model to precisely predict the microsegregation and microstructure of the atomized alloy powders and sets a foundation to control the powder features for various engineering applications.

关键词： Particle size Solidification microstructure Microsegregation Numerical simulation

Effect of heat treatment on microstructure and mechanical properties of selective laser-melted PH13-8Mo stainless steel

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Journal of Iron and steel Research International 2024年第4期31卷 945-955页

作者： Yuan Zhang Xiang Liu Chang-jun Wang Chang Liu School of Material Science and engineering Kunming University of Science and TechnologyKunming 650093YunnanChina Central Iron&steel Research institute Co. Ltd.Beijing 100081China

PH13-8Mo stainless steel powder with high sphericity and well fluidity was prepared by the plasma rotating electrode *** formed parts with ultra-high purity were manufactured by selective laser *** tensile and impact mechanical properties of the printed parts under three heat treatment regimes were compared to those without heat *** microstructure,grain orientation and phase composition were characterized by electron-backscatter diffraction,X-ray diffraction and transmission electron *** characterization results reveal that the addition of heat treatment makes the grains enlarge,and after different heat treatments,the average grain size from 1.51μm in the printed state increases to 2.78,3.09 and 2.06μm,*** formed parts are mainly composed of martensite and retained ***,the NiAl and M23C precipitates form,which are the major strengthening phases of PH13-8Mo stainless *** optimal heat treatment process is 925℃×1 h water cooling(WC)+0℃×2 h air cooling(AC)+540℃×4 h *** this heat treatment process,PH13-8Mo formed parts have the optimal comprehensive mechanical properties:the tensile strength,yield strength and impact energy KU2 are 1492 MPa,1432 MPa and 63 J,*** strengthening and toughening via heat treatment are mainly attributed to dislocation strengthening,the formation of NiAl and M23Co precipitates and the change of volume fraction of the retained austenite.

关键词： High-strength stainless steel-Selective laser melting-Heat treatment Microstructure Mechanical property

Unveiling the cellular microstructure-property relations in martensitic stainless steel via laser powder bed fusion

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International Journal of Minerals,Metallurgy and Materials 2024年第11期31卷 2476-2487页

作者： Lingzhi Wu Cong Zhang Dil Faraz Khan Ruijie Zhang Yongwei Wang Xue Jiang Haiqing Yin Xuanhui Qu Geng Liu Jie Su Collaborative Innovation Center of steel Technology University of Science and Technology BeijingBeijing 100083China Department of Physics University of Science and Technology BannuBannu 28100Pakistan Beijing Advanced Innovation Center for Materials Genome engineering University of Science and Technology BeijingBeijing 100083China Beijing Key Laboratory of Materials Genome engineering University of Science and Technology BeijingBeijing 100083China institute for Advanced Materials and Technology University of Science and Technology BeijingBeijing 100083China institute for Special steel Research Central Iron and Steel Research InstituteBeijing 100081China

Laser powder bed fusion(LPBF)is a widely recognized additive manufacturing technology that can fabricate complex components rapidly through layer-by-layer ***,there is a paucity of research on the effect of laser scanning speed on the cellular microstructure and mechanical properties of martensitic stainless *** study systematically investigated the influence of laser scanning speed on the cellular microstructure and mechanical properties of a developed Fe11Cr8Ni5Co3Mo martensitic stainless steel produced by *** results show that increasing the laser scanning speed from 400 to 1000 mm/s does not lead to a noticeable change in the phase fraction,but it reduces the average size of the cellular microstructure from 0.60 to 0.35μ*** scanning speeds of 400 and 1000 mm/s both had adverse effects on performances of sample,resulting in inadequate fusion and keyhole defects *** optimal scanning speed for fabricating samples was determined to be 800 mm/s,which obtained the highest room temperature tensile strength and elongation,with the ultimate tensile strength measured at(1088.3±2.0)MPa and the elongation of(16.76±0.10)%.Furthermore,the mechanism of the evolution of surface morphology,defects,and energy input were clarified,and the relationship between cellular microstructure size and mechanical properties was also established.

关键词： laser powder bed fusion martensitic stainless steel cellular microstructure mechanical properties strengthening mechanism

Effect of La on the Corrosion Behavior and Mechanism of 3Ni Weathering steel in a Simulated Marine Atmospheric Environment

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Acta Metallurgica Sinica(English Letters) 2024年第2期37卷 308-324页

作者： Gang Niu Rui Yuan R.D.K.Misra Na Gong Zhi-Hui Zhang Hao-Xiu Chen Hui-Bin Wu Cheng-Jia Shang Xin-Ping Mao Collaborative Innovation Center of steel Technology University of Science and Technology BeijingBeijing100083China Laboratory for Excellence in Advanced steel Research Department of MetallurgicalMaterials and Biomedical EngineeringUniversity of Texas at El PasoEl PasoTX79968USA institute of Materials Research and engineering Agency for ScienceTechnologyand ResearchSingapore138634Singapore Department of Materials Science and engineering University of TorontoTorontoONM5S 3E4Canada

The corrosion behavior and mechanism of 3Ni weathering steel in a simulated oceanic atmospheric environment are investigated in order to comprehend the impacts of La,as determined through electrochemical analysis and rust layer *** results of this study demonstrate that the addition of La enhances the corrosion resistance of 3Ni weathering steel in the marine atmospheric environment,thereby reducing the corrosion rate and improving the protection of the rust *** influence of La on corrosion resistance can be attributed to two primary ***,La functions as a grain refiner,minimizing the potential difference of the micro-regions on the substrate surface,thereby significantly reducing the corrosion of bare steel in the marine ***,La inhibits the process of Fe_(3)O_(4) oxidation back toγ-FeOOH during corrosion at the local site,thus decreasing the formation ofγ-FeOOH and enhancing the charge transfer *** research work may serve as a reference for expanding the application of rare earth elements in the field of weathering steel.

关键词： Weathering steel Rare earth Rust layer Corrosion behavior Corrosion resistance