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Application of in-situ characterization techniques in modern aqueous batteries

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Rare Metals 2024年第8期43卷 3553-3575页

作者： Jia-Hao Wu Hong-Wei Cai Zhao-Hui deng Jean-Jacques Gaumet Yu Bao Wen Luo department of Physics State Key Laboratory of Advanced Technology for Materials Synthesis and ProcessingSchool of Materials Science and EngineeringWuhan University of TechnologyWuhan430070China Laboratoire de Chimie Et physique:Approche Multi-Echelles Des Milieux Complexes(LCP-A2MC)Institut Jean BarriolUniversitéde Lorraine57070MetzFrance department of Medicinal Chemistry Hubei College of Chinese MedicineJingzhou 434020China

The development of high-performance aqueous batteries calls for an in-depth knowledge of their chargedischarge redox and failure mechanism,as well as a systematic understanding of the dynamic evolution of microstructure,phase composition,chemical composition,and local chemical environment of the materials for ***-situ characterization technology is expected to understand and reveal the problems faced by aqueous rechargeable batteries,such as the dissolution of electrode materials,the growth of metal negative electrode dendrites,passivation,corrosion,side reactions and a series of *** on this,typical in-situ characterization techniques and their basic mechanisms are summarized,including in-situ optical visualization,in-situ microscopy techniques(in-situ scanning electron microscopy(SEM),in-situ transmission electron microscopy(TEM)),in-situ X-ray techniques(in-situ X-ray diffraction(XRD),in-situ X-ray photoelectron spectroscopy(XPS),in-situ near-edge structural X-ray absorption spectroscopy(XANES)),and in-situ spectroscopy techniques(in-situ Raman spectroscopy,in-situ Fourier transform infrared(FTIR)).Moreover,some emerging techniques concerning aqueous battery research,especially gas evolution and materials dissolution issues,such as in-situ electrochemical quartz crystal microbalance(EQCM).in-situ fiber-optic sensing,in-situ gas chromatography(GC) are *** last,the applications of advanced in-situ characterizations in future research of aqueous batteries are emphasized and discussed,along with some of the remaining challenges and possible solutions.

关键词： Aqueous battery In-situ characterization Phase transformation Solid electrolyte interphase Zinc dendrite growth

New Approach to Rock Classification Based on Sparse Representations

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Open Journal of Applied Sciences 2024年第1期14卷 145-158页

作者： Wognin Joseph Vangah Bi G. Théodore Toa Alico Nango Jerôme Ouattara Sie Alain Clément Unité de Recherche et d’expertise Numérique (UREN) Université Virtuelle de C&#244te d’Ivoire (UVCI) Abidjan C&#244te d’Ivoire UFR Sciences et technologique Département de Physique Université polytechnique de Man (UPM) Man C&#244te d’Ivoire Classe Préparatoire des Grandes Ecoles (CPGE) Université de San Pédro (USP) San Pédro C&#244te d’Ivoire institut National Polytechnique Houphou&#235 t (INPHB) Yamoussoukro C&#244te d’Ivoire Laboratoire Angevin de Recherche en Ingénierie des Systèmes (LARIS) Institut Universitaire de Technologie (IUT) Université d’Angers Angers France

In geology, classification and lithological recognition of rocks plays an important role in the area of oil and gas exploration, mineral exploration and geological analysis. In other fields of activity such as construction and decoration, this classification makes sense and fully plays its role. However, this classification is slow, approximate and subjective. Automatic classification curbs this subjectivity and fills this gap by offering methods that reflect human perception. We propose a new approach to rock classification based on direct-view images of rocks. The aim is to take advantage of feature extraction methods to estimate a rock dictionary. In this work, we have developed a classification method obtained by concatenating four (4) K-SVD variants into a single signature. This method is based on the K-SVD algorithm combined with four (4) feature extraction techniques: DCT, Gabor filters, D-ALBPCSF and G-ALBPCSF, resulting in the four (4) variants named K-Gabor, K-DCT, KD-ALBPCSF and KD-ALBPCSF respectively. In this work, we developed a classification method obtained by concatenating four (4) variants of K-SVD. The performance of our method was evaluated on the basis of performance indicators such as accuracy with other 96% success rate.

关键词： Rock Recognition Dictionary Signature Color Texture K-SVD Variants KD-ALBPCSF Et KG-ALBPCSF

Ion emission from warm dense matter produced by irradiation with a soft x-ray free-electron laser

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Matter and Radiation at Extremes 2024年第1期9卷 71-84页

作者： Josef Krása Tomás Burian Vera Hájková Jaromír Chalupský Šimon Jelínek Katerina Frantálová Michal Krupka Zuzana Kuglerová Sushil Kumar Singh Vojtech Vozda Ludek Vysín MichalŠmíd Pablo Perez-Martin Marion Kühlman Juan Pintor Jakub Cikhardt Matthias Dreimann dennis Eckermann Felix Rosenthal Sam M.Vinko Alessandro Forte Thomas Gawne Thomas Campbell Shenyuan Ren YuanFeng Shi Trevor Hutchinson Oliver Humphries Thomas Preston Mikako Makita Motoaki Nakatsutsumi Xiayun Pan Alexander Köhler Marion Harmand Sven Toleikis Katerina Falk Libor Juha department of Radiation and Chemical Physics Institute of PhysicsCzech Academy of SciencesNa Slovance 218221 Prague 8Czech Republic Laser Plasma department Institute of Plasma PhysicsCzech Academy of SciencesZa Slovankou 318200 Prague 8Czech Republic department of Surface and Plasma Science Faculty of Mathematics and PhysicsCharles University in PragueV Holesovi ckách 218000 Prague 8Czech Republic department of Physical Electronics Faculty of Nuclear Science and Engineering PhysicsCzech Technical University in PragueV Holesovi ckách 218000 Prague 8Czech Republic Helmholtz-Zentrum Dresden-Rossendorf Bautzner Landstraße 40001328 DresdenGermany desY Photon Science Notkestraße 85D-22607 HamburgGermany institut de Minéralogie de Physique des Matériaux et de CosmochimieUMR 7590–UPMC/CNRS/IRD/MNHNSorbonne Université4 place Jussieu75005 ParisFrance department of Physics Faculty of Electrical EngineeringCzech Technical University in PragueTechnická216627 Prague 6Czech Republic Center for Soft Nanoscience University of MünsterBusso-Peus-Straße 10D-48149 MünsterGermany department of Physics Clarendon LaboratoryUniversity of OxfordParks RoadOxford OX13PUUnited Kingdom Central Laser Facility STFC Rutherford Appleton LaboratoryDidcot OX110QXUnited Kingdom Lawrence Livermore National Laboratory 7000 East AvenueLivermoreCalifornia 94550USA European XFEL GmbH Holzkoppel 4D-22869 SchenefeldGermany Technische Universität Dresden 01062 DresdenGermany

We report on an experiment performed at the FLASH2 free-electron laser(FEL)aimed at producing warm dense matter via soft x-ray isochoric *** the experiment,we focus on study of the ions emitted during the soft x-ray ablation process using time-of-flight electron multipliers and a shifted Maxwell–Boltzmann velocity distribution *** find that most emitted ions are thermal,but that some impurities chemisorbed on the target surface,such as protons,are accelerated by the electrostatic field created in the plasma by escaped *** morphology of the complex crater structure indicates the presence of several ion groups with varying *** find that the ion sound velocity is controlled by the ion temperature and show how the ion yield depends on the FEL radiation attenuation length in different materials.

关键词： electrostatic emitted chemi

Phytochemical Analysis and Antimicrobial Activity of Lawsonia inermis Leaf Extracts from Burkina Faso

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American Journal of Plant Sciences 2024年第7期15卷 552-576页

作者： Ollo Youl Soumaïla Konaté Ernest N. Sombié Rainatou Boly Boukaré Kaboré Moumouni Koala Arouna Zoungrana Saybou Savadogo Christian Marc Tahita Innocent Valea Halidou Tinto Adama Hilou Maminata Traoré-Coulibaly Laboratoire de Biochimie et de Chimie Applique (LABIOCA) Universit de Ouagadougou Ouagadougou Burkina Faso Agence Nationale Pour la Scurit Sanitaire de lEnvironnement de lAlimentation du Travail et des Produits de Sant (ANSSEAT) Ouagadougou Burkina Faso Laboratoire de Recherche-Dveloppement de Phytomdicaments et Mdicaments (L-RD/PM) Institut de Recherche en Sciences de la Sant (IRSS-CNRST) Ouagadougou Burkina Faso Laboratoire de Chimie Organique et de physique Applique (LCOPA) cole Doctorale Sciences et Technologie Universit Joseph KI-ZERBO Ouagadougou Burkina Faso Laboratoire Sciences de la Vie et de la Terre (LASVT) cole Doctorale Sciences et Technologie Universit Norbert ZONGO Koudougou Burkina Faso Unit de Recherche Clinique de Nanoro Institut de Recherche en Sciences de la Sant (IRSS-CNRST) Nanoro Burkina Faso

Lawsonia inermis is a hairless plant growing in various regions of North Africa, the Indian subcontinent, and the Middle East. It possesses many medicinal attributes, including curative properties against infectious dermatoses. This study was carried out to evaluate the phytochemical profile of the crude ethanolic extract of the plant leaves and its fractions as well as their antimicrobial activities. The phytochemical profile was performed using high-performance thin-layer chromatography (HPTLC), gas chromatography-mass spectrometry (GC-MS), and high-performance liquid chromatography (HPLC). Additionally, the phenolic and flavonoid contents were determined using the Folin-Ciocalteu spectrophotometric and the aluminum trichloride methods. Antimicrobial activity was tested using disc diffusion and microdilution methods. The presence of flavonoids, tannins, sterols, and triterpenes was revealed. GC-MS detected twelve compounds main compounds consisting of saturated and unsaturated fatty acids and phenolic and terpenoid compounds among twenty-seven components. HPLC also detected high contents of phenolic acids and flavonoids. The most abundant triterpene and sterols were ursolic acid (around 43.14 g/100g DW, 13.9 g/100g dry weight (DW), and 0.68 g/100g DW) in the crude ethanolic extract of leaves (FeLi), hexane fraction (FHLi) and dichloromethane fraction (FDLi), respectively and, β-sitosterol in FeLi (56.7 mg/100g DW), FHLi (10.55 g/100g DW), FDLi (106.1 mg/100g DW) and butanol fraction (FBLi) (357.4 mg/100g DW). Among the flavonoids, rutin = 3.24 g/100g and quercetin = 0.63 g/100g in the ethanolic extract, rutin = 15.73 g/100g in the dichloromethane fraction, and rutin = 0.23 g/100g) in the aqueous fraction;and among phenolic compounds, caffeic acid (37.65 g/100g DW) and vanillic acid (22.70 g/100g DW) were the most important in the ethyl acetate fraction (FAeLi). All organic fractions exhibited interesting antibacterial and antifungal activities against the tested s

关键词： Lawsonia inermis Phytochemical Profile HPLC GC-MS Analysis Antimicrobial Activity

Search for a lighter neutral custodial fiveplet scalar in the Georgi-Machacek model

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Chinese Physics C 2022年第8期46卷 114-121页

作者：王储陶军全 M.Aamir Shahzad 陈国明 S.Gascon-Shotkin institute of High Energy Physics Chinese Academy of SciencesBeijing 100049China University of Chinese Academy of Sciences Beijing 100049China institut de physique des 2 infinis de Lyon Universitéde LyonUniversitéClaude Bernard Lyon 1CNRS-IN2P3Villeurbanne 69622France

Many researches from both theoretical and experimental perspectives have been performed to search for a new Higgs Boson that is lighter than the 125 GeV Higgs boson,which was discovered at the LHC in *** this study,we explore the possibility of constraining a lighter neutral custodial fiveplet scalar H_(5)^(0) in the GeorgiMachacek(GM) model using the latest results of the search for a lighter Higgs boson decaying into two photons from LHC *** custodial-singlet mass eigenstate h or H is considered to be the LHC observed 125 GeV Higgs boson.A new set of constrained parameters that is favoured by low-mass H_(5)^(0) is proposed to generate events *** production of H_(5)^(0) from a scan based on the constrained parameters is compared to the latest results of the search for a lighter Higgs boson decaying into two photons by the CMS Collaboration after applying theoretical constraints from the GM model and constraints from all existing relevant experimental measurements,including the recent results of the Higgs boson searches by the *** analyses of the surviving GM parameter space are *** tendencies and correlations of the GM input parameters from phenomenological studies are *** addition,the discovery potential of the other interesting decay channels of this low-mass neutral custodial fiveplet scalar are discussed.

关键词： Georgi-Machacek model lighter neutral custodial fiveplet scalar phenomenological studies

Performance Evaluation of Solar Chimney Draft: Application to Ventilation

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Smart Grid and Renewable Energy 2024年第4期15卷 107-122页

作者： Boukaré Ouedraogo Adama Ouedraogo Arouna Kabore Kalifa Palm Dieudonné Joseph Bahiebo Laboratoire denergies Thermiques Renouvelables (LETRE) Universit Joseph KI-ZERBO: UFR/SEA Ouagadougou Burkina Faso Laboratoire de Chimie Analytique Physique Spatiale et Energtique (LACAPSE) Universit Norbert ZONGO Koudougou Burkina Faso Centre Universitaire Polytechnique de Kaya (CUP-Kaya) Universit Joseph KI-ZERBO Ouagadougou Burkina Faso Laboratoire des Systmes denergie Renouvelable et Environnement Institut de Recherche en Sciences Appliques et Technologies (IRSAT) Centre National de la Recherche Scientifique et Technologique (CNRST) Ouagadougou Burkina Faso

Ventilation is one of the factors contributing to energy consumption in buildings and food preservation. The solar chimney proves to be an alternative for reducing conventional energy consumption. Thus, in this study, the performance of a solar chimney with two active faces for thermally drawing air from a chamber for preserving agri-food products was evaluated. These performances were experimentally assessed through data measurements: temperatures and velocities within the chimney, and their analysis using Excel and MATLAB. The obtained results were compared with those from literature to verify their validity. From this study, it is found that the maximum temperature at the chimney outlet reaches 49.4˚C with an average value of 43.7˚C. Additionally, the heating evolution of the chimney air presents four (04) identical phases in pairs, reflecting the chimney’s operation throughout day. The temperature difference between the outlet and inlet of the chimney reaches a maximum of 17˚C with an average of 12.6˚C. Regarding airflow, the maximum air velocity at the chimney outlet is 0.8 m/s, and the average velocities have consistently been greater than or equal to 0.46 m/s. Thus, it can be concluded that the solar chimney is capable of providing ventilation for the preservation chamber through thermal draft.

关键词： Solar Chimney Natural Ventilation Thermal Draft Airflow Chimney Effect

Using Optical Tweezers to Study the Friction of the Red Blood Cells

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Advances in Bioscience and Biotechnology 2024年第2期15卷 100-111页

作者： Edoukoua Jean Michel Konin Pavel Yale Abadê Ange-Boris N’guessan Kouassi Benoit Kouakou Abaka Michel Kouacou Eugene Megnassan Département des Sciences et Techniques Université Alassane Ouattara Bouaké C&#244te d’Ivoire Laboratoire d’Instrumentation Image et Spectroscopie (L2IS) Institut National Polytechnique Félix Houphou&#235t-Boigny (INPHB) Yamoussoukro C&#244te d’Ivoire Classes préparatoires aux grandes Ecoles Université de San Pedro San Pedro C&#244te d’Ivoire Laboratoire de physique Fondamentale et Appliquée Université Nangui Abrogoua (UNA) Abidjan C&#244te d’Ivoire

In the last two decades the study of red blood cell elasticity using optical tweezers has known a rise appearing in the scientific research with regard to the various works carried out. despite the various work done, no study has been done so far to study the influence of friction on the red blood cell indentation response using optical tweezers. In this study, we have developed a new approach to determine the coefficient of friction as well as the frictional forces of the red blood cell. This approach therefore allowed us to simultaneously carry out the indentation and traction test, which allowed us to extract the interfacial properties of the microbead red blood cell couple, among other things, the friction coefficient. This property would be extremely important to investigate the survival and mechanical features of cells, which will be of great physiological and pathological significance. But taking into account the hypothesis of friction as defined by the isotropic Coulomb law. The experiment performed for this purpose is the Brinell Hardness Test (DB).

关键词： Friction Indentation Optical Tweezers Tribology Red Blood Cells

Thermal Performance Analysis of Plaster Reinforced with Raffia Vinifera Particles for Use as Insulating Materials in Building

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Journal of Minerals and Materials Characterization and Engineering 2024年第2期12卷 112-138页

作者： Etienne Malbila Danielle Manuella Djouego Tagne Bouto Kossi Imbga Lareba Adelaide Ouedraogo Sié Kam David Yemboini Kader Toguyeni Ecole Sup&#233 rieure d&#8217Ing&#233nierie (ESI) Universit&#233 de Fada N&#8217Gourma Fada N&#8217Gourma Burkina Faso Laboratoire d217 Energies Thermiques Renouvelables (LETRE) Universit&#233 Joseph KI-ZERBO Ouagadougou Burkina Faso institut Sup&#233 rieur des Techniques Industrielles et Commerciales (ISTIC) Bangangt&#233 Cameroun Unité de Formation et de Recherche en Sciences et Technologies (UFR/ST) Université Norbert ZONGO Koudougou Burkina Faso Laboratoire de physique et Chimie de l217 Environnemen (LPCE) Universit&#233 Joseph KI-ZERBO Ouagadougou Burkina Faso Ecole Polytechnique de Ouagadougou (EPO) Ouagadougou Burkina Faso

The present study focuses on the formulation of new composite consisting of plaster and raffia vinifera particle (RVP) with the purpose to reducing energy consumption. The aim of this study is to test this new compound as an insulating eco-material in building in a tropical climate. The composites samples were developed by mixing plaster with raffia vinifera particles (RVP) using three different sizes (1.6 mm, 2.5 mm and 4 mm). The effects of four different RVP incorporations rates (i.e., 0wt%, 5wt%;10wt%;15wt%) on physical, thermal, mechanicals properties of the composites were investigated. In addition, the use of the raffia vinifera particles and plaster based composite material as building envelopes thermal insulation material is studied by the habitable cell thermal behavior instrumentation. The results indicate that the incorporation of raffia vinifera particle leads to improve the new composite physical, mechanical and thermal properties. And the parametric analysis reveals that the sampling rate and the size of raffia vinifera particles are the most decisive factor to impact these properties, and to decreases in the thermal conductivity which leads to an improvement to the thermal resistance and energy savings. The best improvement of plaster composite was obtained at the raffia vinifera particles size between 2.5 and 4.0 mm loading of 5wt% (C95P5R) with a good ratio of thermo-physical-mechanical properties. Additionally, the habitable cell experimental thermal behavior, with the new raffia vinifera particles and plaster-based composite as thermal insulating material for building walls, gives an average damping of 4°C and 5.8°C in the insulated house interior environment respectively for cold and hot cases compared to the outside environment and the uninsulated house interior environment. The current study highlights that this mixture gives the new composite thermal insulation properties applicable in the eco-construction of habitats in tropical environments

关键词： Fibres Plaster Thermal Test Mechanical Test Insulating Material Indoor Comfort

Stability of Three-Dimensional Interfacial Waves Under Subharmonic Disturbances

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中国海洋工程:英文版 2023年第4期37卷 558-567页

作者： Nabil ALLALOU Mohammed deBIANE Christian KHARIF Facultéde physique Universitédes Sciences et de la Technologie Houari Boumediene(USTHB)Algiers 16123Algeria Technopole de Chateau-Gombert Institut de Recherche sur les Phénomènes Hors Equilibre(IRPHE)Marseille 13384France

This study examines the stability regimes of three-dimensional interfacial gravity *** numerical results of the linear stability analysis extend the three-dimensional surface waves results of Ioualalen and Kharif(1994)to three-dimensional interfacial *** approach of the collocation type has been developed for this *** equations of motion are reduced to an eigenvalue problem where the perturbations are spectrally decomposed into normal *** results obtained showed that the density ratio plays a stabilizing *** addition,the dominant instability is of three-dimensional structure,and it belongs to class I for all values of density ratio.

关键词： short-crested interfacial waves linear stability collocation method Padéapproximant