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Realizing efficient emission and triple-mode photoluminescence switching in air-stable tin(IV)-based metal halides via antimony doping and rational structural modulation

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Aggregate 2024年第1期5卷 257-269页

作者： Xuefei He Hui Peng Qilin Wei Zhijie Zhou Guolun Zhang Zhentao Du Jialong Zhao Bingsuo Zou Department of materials Physics and Chemistry State Key Laboratory of Featured Metal Materials and Life-cycle Safety for Composite StructuresMOE Key Laboratory of New Processing Technology for Nonferrous Metals and Materialsand School of ResourcesEnvironment and MaterialsGuangxi UniversityNanningChina

Recently,many lead-free metal halides with diverse structures and highly efficient emission have been ***,their poor stability and single-mode emission color severely limit their ***,three homologous Sb^(3+)-doped zero-dimensional(0D)air-stable Sn(IV)-based metal halides with different crystal structures were developed by inserting a single organic ligand into SnCl_(4)lattice,which brings different optical *** photoexcitation,(C_(25)H_(22)P)SnC_(l5)@Sb⋅CH_(4O)(Sb^(3+)−1)does not emit light,(C_(25)H_(22)P)_(2)SnC_(l6)@Sb-α(Sb^(3+)−2α)shines bright yellow emission with a photoluminescence quantum yield(PLQY)of 92%,and(C_(25)H_(22)P)_(2)SnC_(l6)@Sb-β(Sb^(3+)−2β)exhibits intense red emission with a PLQY of 78%.The above three compounds show quite different optical properties should be due to their different crystal structures and the lattice ***,Sb^(3+)−1 can be successfully converted into Sb^(3+)−2αunder the treatment of C_(25)H_(22)PCl solution,accompanied by a transition from nonemission to efficient yellow emission,serving as a“turn-on”photoluminescence(PL)***,a reversible structure conversion between Sb^(3+)−2αand Sb^(3+)−2βwas witnessed after dichloromethane or volatilization treatment,accompanied by yellow and red emission ***,a triple-mode tunable PL switching of off-onI-onII can be constructed in Sb^(3+)-doped Sn(IV)-based ***,we demonstrated the as-synthesized compounds in fluorescent anticounterfeiting,information encryption,and optical logic gates.

关键词： information encryption Sb^(3+)-doping Sn(IV)-based metal halides structural modulation triple-mode

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Coupling Co-Ni phosphides for energy-saving alkaline seawater splitting

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Nano Research 2024年第6期17卷 4797-4806页

作者： Weijia Liu Wenxian Liu Tong Hou Junyang Ding Zhigui Wang Ruilian Yin Xingyuan San Ligang Feng Jun Luo Xijun Liu State key laboratory of featured Metal materials and Life-cycle Safety for Composite Structures Guangxi Key Laboratory of Processing for Nonferrous Metals and Featured MaterialsMOE Key Laboratory of New Processing Technology for Nonferrous Metals and MaterialsSchool of ResourcesEnvironment and MaterialsGuangxi UniversityNanning 530004China College of materials Science and Engineering Zhejiang University of TechnologyHangzhou 310014China Hebei key laboratory of Optic-electronic Information and materials the College of Physics Science and TechnologyHebei UniversityBaoding 071002China School of Chemistry and Chemical Engineering Yangzhou UniversityYangzhou 225002China ShenSi lab Shenzhen Institute for Advanced StudyUniversity of Electronic Science and Technology of ChinaShenzhen 518110China

The coupling of energy-saving small molecule conversion reactions and hydrogen evolution reaction(HER)in seawater electrolytes can reduce the energy consumption of seawater electrolysis and mitigate chlorine corrosion ***,the fabrication of efficient multifunctional catalysts for this promising technology is of great ***,a heterostructured catalyst comprising CoP and Ni_(2)P on nickel foam(CoP/Ni_(2)P@NF)is reported for hydrazine oxidation(HzOR)-assisted alkaline seawater *** coupling of CoP and Ni_(2)P optimizes the electronic structure of the active sites and endows excellent electrocatalytic performance for HzOR and ***,the two-electrode HzOR-assisted alkaline seawater splitting(OHzS)cell based on the CoP/Ni_(2)P@NF required only 0.108 V to deliver 100 mA·cm^(−2),much lower than 1.695 V for alkaline seawater electrolysis ***,the OHzS cell exhibits satisfactory stability over 48 h at a high current density of 500 mA·cm^(−2).Furthermore,the CoP/Ni_(2)P@NF heterostructured catalyst also efficiently catalyzed glucose oxidation,methanol oxidation,and urea oxidation in alkaline seawater *** work paves a path for high-performance heterostructured catalyst preparation for energy-saving seawater electrolysis for H_(2) production.

关键词： seawater splitting heterostructure electrocatalysis hydrazine oxidation reaction hydrogen evolution reaction

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Interface optimization and defects suppression via Na F introduction enable efficient flexible Sb_(2)Se_(3) thin-film solar cells

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Journal of Energy Chemistry 2024年第3期90卷 165-175,I0006页

作者： Mingdong Chen Muhammad Ishaq Donglou Ren Hongli Ma Zhenghua Su Ping Fan David Le Coq Xianghua Zhang guangxing Liang Shuo Chen Shenzhen key laboratory of Advanced Thin Films and Applications Key Laboratory of Optoelectronic Devices and Systems of Ministry of Education and Guangdong ProvinceCollege of Physics and Optoelectronic EngineeringShenzhen UniversityShenzhen 518060GuangdongChina State key laboratory of featured Metal materials and Life-cycle Safety for Composite Structures MOE Key Laboratory of New Processing Technology for Nonferrous Metals and MaterialsSchool of ResourcesEnvironment and MaterialsGuangxi UniversityNanning 530004GuangxiChina CNRS ISCR(Institut des Sciences Chimiques de Rennes)UMR 6226Universitéde RennesRennes F-35000France

Sb_(2)Se_(3) with unique one-dimensional(1D) crystal structure exhibits exceptional deformation tolerance,demonstrating great application potential in flexible ***,the power conversion efficiency(PCE) of flexible Sb_(2)Se_(3) photovoltaic devices is temporarily limited by the complicated intrinsic defects and the undesirable contact ***,a high-quality Sb_(2)Se_(3) absorber layer with large crystal grains and benign [hkl] growth orientation can be first prepared on a Mo foil *** NaF intermediate layer is introduced between Mo and Sb_(2)Se_(3),which can further optimize the growth of Sb_(2)Se_(3)thin ***,positive Na ion diffusion enables it to dramatically lower barrier height at the back contact interface and passivate harmful defects at both bulk and *** a result,the champion substrate structured Mo-foil/Mo/NaF/Sb_(2)Se_(3)/CdS/ITO/Ag flexible thin-film solar cell delivers an obviously higher efficiency of 8.03% and a record open-circuit voltage(V_(OC)) of 0.492 *** flexible Sb_(2)Se_(3) device also exhibits excellent stability and flexibility to stand large bending radius and multiple bending times,as well as superior weak light photo-response with derived efficiency of 12.60%.This work presents an effective strategy to enhance the flexible Sb_(2)Se_(3) device performance and expand its potential photovoltaic applications.

关键词： Sb_(2)Se_(3) Flexible solar cells NaF intermediate layer Interface optimization Defects suppression

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Nanostructured Pt@RuO_(x) catalyst for boosting overall acidic seawater splitting

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Chinese Journal of Structural Chemistry 2024年第1期43卷 6-15页

作者： Zimo Peng Quan Zhang Gaocan Qi Hao Zhang Qian Liu Guangzhi Hu Jun Luo Xijun Liu Institute for new Energy materials&Low-Carbon Technologies School of Materials Science and EngineeringTianjin University of TechnologyTianjin300384China School of materials Science and Engineering Tianjin University of TechnologyTianjin 300384China Institute for Advanced Study Chengdu UniversityChengdu610106China Institute for Ecological Research and Pollution Control of Plateau Lakes School of Ecology and Environmental ScienceYunnan UniversityKunming650091China ShenSi lab Shenzhen Institute for Advanced StudyUniversity of Electronic Science and Technology of ChinaLonghua DistrictShenzhen518110China State key laboratory of featured Metal materials and Life-cycle Safety for Composite Structures Guangxi Key Laboratory of Processing for Non-ferrous Metals and Featured MaterialsMOE Key Laboratory of New Processing Technology for Nonferrous Metals and MaterialsSchool of ResourcesEnvironment and MaterialsGuangxi UniversityNanning530004China

In the domain of acidic water splitting,designing bifunctional catalysts that marry high activity with enduring stability is a formidable ***,we have constructed platinum-containing ruthenium oxide nanoparticles(Pt@RuO_(x)NPs)to achieve excellent overall water splitting performance in acidic ***@RuO_(x)NPs demonstrate exceptional catalytic activity for both the hydrogen evolution reaction(HER)and oxygen evolution reaction(OER)in acidic seawater,requiring overpotentials of only 20 and 157 mV,respectively to achieve a current density of 10 mA cm^(-2).Furthermore,in 0.5 M H_(2)SO_(4),this catalyst exhibits high HER(19 mV)and OER(236 mV)catalytic *** two-electrode water splitting system composed of bifunctional Pt@RuO_(x)NPs requires cell voltages of only 1.442 and 1.465 V to deliver a current density of 10 mA cm^(-2)in acidic seawater and 0.5 M H_(2)SO_(4).Remarkably,this catalyst displays remarkable stability in the water splitting *** is shown that the introduction of Pt could augment oxygen vacancies and enhance catalytic activity *** synergy between Pt and Ru further contributes to the improved ***,we have observed that acidic seawater holds distinct advantages for acidic water splitting,along with a thorough exploration of the relationship between Cl^(-)concentration and catalytic *** study not only provides a strategy to improve the catalytic activity and stability of ruthenium-based catalysts for water splitting in acidic environments,but also unveils the promoting effect of Cl^(-)on the catalytic activity in acidic water splitting.

关键词： Acidic water splitting Bifunctional catalysts Pt@RuOx nanoparticles Synergistic effect

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Steering surface reconstruction of hybrid metal oxides for efficient oxygen evolution reaction in water splitting and zinc-air batteries

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Journal of Energy Chemistry 2024年第5期92卷 383-393页

作者： Jie Zhu Junxue Chen Xida Li Kun Luo Zewei Xiong Zhiyu Zhou Wenyun Zhu Zhihong Luo Jingbin Huang Yibing Li key lab of new processing technology for nonferrous metals and materials Ministry of EducationSchool of Materials Science and EngineeringGuilin University of TechnologyGuilin 541000GuangxiChina The key laboratory of Rare Earth Functional materials and Applications Zhoukou Normal UniversityZhoukou 466001HenanChina School of Chemistry and Chemical Engineering Beijing Institute of TechnologyBeijing 100081China School of materials Science and Engineering Changzhou UniversityChangzhou 213164JiangsuChina Wuhan Sunmoon Battery Co. LtdWuhan 430090HubeiChina

Surface reconstruction yields real active species in electrochemical oxygen evolution reaction(OER)conditions;however,rationally regulating reconstruction in a targeted manner for constructing highly active OER electrocatalysts remains a formidable ***,an electrochemical activation strategy with selective etching was utilized to guide the reconstruction process of a hybrid cobalt-molybdenum oxide(CoMoO_(4)/Co_(3)O_(4)@CC)in a favorable direction to improve the OER *** in-situ Raman and multiple ex-situ characterization tools demonstrate that controlled surface reconstruction can be easily achieved through Mo etching,with the formation of a dynamically stable amorphous-crystalline *** calculations together with experimental results reveal that the synergistic effects between amorphous CoOOH and crystalline Co_(3)O_(4) are crucial in enhancing the catalytic ***,the reconstructed CoMoO_(4)/Co_(3)O_(4)@CC exhibits a low overpotential of 250 mV to achieve a current density of 10 mA cm^(-2) in 1 M KOH,and more importantly it can be practiced in electrolytic water splitting and rechargeable zinc-air batteries devices,achieving ultra-long stability for over 500 and 1200 h,*** work provides a promising route for the construction of high-performance electrocatalysts.

关键词： Electrocatalyst Oxygen evolution reaction Surface reconstruction Selective etching Amorphous-crystalline heterostructures

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Ternary layered boride MoAlB:A novel thermo-regulation microwave absorbing ceramic material

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Journal of Advanced Ceramics 2024年第5期13卷 699-710页

作者： Zhangjue Wang Fan Zhang Nannan Wang Wei Li Yongqiang Chen Hailong Wang Rui Zhang Yanqiu Zhu Bingbing Fan School of Material Science and Engineering Zhengzhou UniversityZhengzhou 450001China Henan Academy of Sciences Zhengzhou 450046China State key laboratory of featured Metal materials and Life Cycle Safety for Composite Structures MOE Key Laboratory of New Processing Technology for Nonferrous Metals MaterialsSchool of ResourcesEnvironment and MaterialsGuangxi UniversityNanning 530004China Department of materials and Earth Sciences Technical University of DarmstadtDarmstadt 64287Germany School of Material Science and Engineering Luoyang Institute of Science and TechnologyLuoyang 471023China Department of Engineering Faculty of EnvironmentScience and EconomyUniversity of ExeterExeter EX44QFUK

In the context of the fifth-generation(5G)smart era,the demand for electromagnetic wave(EMW)-absorbing materials has become increasingly prominent,so it is necessary to explore promising candidate *** work focuses on the exploration of the material absorbing properties of a MoAlB MAB(MAB represents a promising group of alternatives,where M stands for a transition metal,A typically denotes Al,and B is boron)phase ***,the first-principles calculations were performed to reveal the unique crystal and layered structure of the MoAlB ceramics and to predict their potential for use as an EMW absorption ***,a series of MoAlB ceramics were synthesized at temperatures ranging from 800 to 1300℃,and the influence of temperature on the phase compositions and microstructures of the obtained MoAlB ceramics was characterized and ***,the practical EMW absorption performance of the prepared MoAlB ceramics was evaluated via a combination of experiments and radar cross-sectional *** MoAlB sample synthesized at 900℃ exhibits superior EMW absorption performance,achieving an impressive minimum reflection loss(RL)of−50.33 *** unique layered structure and good electrical conductivity of the MoAlB samples are the main reasons for their enhanced wave absorption performance,which provides interfacial polarization and multiple dielectric loss ***,this study not only contributes to the understanding of the preparation of MoAlB materials but also provides potential guidance for their utilization in the realm of electromagnetic wave absorption.

关键词： MoAlB electronic band structure electromagnetic wave(EMW)absorption layered ternary boride density of states

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Au nanoclusters anchored on TiO_(2) nanosheets for high-efficiency electroreduction of nitrate to ammonia

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Nano Research 2024年第3期17卷 1209-1216页

作者： Miaosen Yang Tianran Wei Jia He Qian Liu Ligang Feng Hongyi Li Jun Luo Xijun Liu School of Chemical Engineering Northeast Electric Power UniversityJilin 132012China Nanchang Institute of technology Nanchang 330044China State key laboratory of Chemistry and Utilization of Carbon Based Energy Resources College of ChemistryXinjiang UniversityUrumqi 830017China State key laboratory of featured Metal materials and Life-cycle Safety for Composite Structures Guangxi Key Laboratory of Processing for Non-Ferrous Metals and Featured MaterialsSchool of ResourcesEnvironment and MaterialsGuangxi UniversityNanning 530004China Institute for new Energy materials and Low-Carbon Technologies School of Materials Science and EngineeringTianjin University of TechnologyTianjin 300384China Institute for Advanced Study Chengdu UniversityChengdu 610106China School of Chemistry and Chemical Engineering Yangzhou UniversityYangzhou 225002China Guangzhou Panyu Polytechnic Guangzhou 511483China ShenSi lab Shenzhen Institute for Advanced StudyUniversity of Electronic Science and Technology of ChinaLonghua DistrictShenzhen 518110China

Electrocatalytic nitrate reduction reaction(NO_(3)RR)offers a unique rationale for green NH_(3) synthesis,yet the lack of high-efficiency NO_(3)RR catalysts remains a great *** this work,we show that Au nanoclusters anchored on TiO_(2) nanosheets can efficiently catalyze the conversion of NO_(3)RR-to-NH_(3) under ambient conditions,achieving a maximal Faradic efficiency of 91%,a peak yield rate of 1923μg·h^(-1)·mgcat.-1,and high durability over 10 consecutive cycles,all of which are comparable to the recently reported metrics(including transition metal and noble metal-based catalysts)and exceed those of pristine TiO_(2).Moreover,a galvanic Zn-nitrate battery using the catalyst as the cathode was proposed,which shows a power density of 3.62 mW·cm^(-2) and a yield rate of 452μg·h^(-1)·mgcat.-*** simulations further indicate that the atomically dispersed Au clusters can promote the adsorption and activation of NO_(3)-species,and reduce the NO_(3)RR-to-NH_(3) barrier,thus leading to an accelerated cathodic *** work highlights the importance of metal clusters for the NH_(3) electrosynthesis and nitrate removal.

关键词： NH3 electrosynthesis Zn-nitrate battery Au nanoclusters nitrate reduction reaction(NRR) TiO_(2)nanosheets

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Solar-powered miniature robot for on-site oil spill treatment under magnetic steering

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Science China(Technological Sciences) 2024年第7期67卷 2164-2175页

作者： WANG Ben CHEN YunRui WANG Yun JI FengTong LI HongYuan NIU ShiChao HAN ZhiWu ZHANG YaBin GUO ZhiGuang College of Chemistry and Environmental Engineering Shenzhen UniversityShenzhen 518060China State key laboratory of featured Metal materials and Life-cycle Safety for Composite Structures Ministry of Education Key Laboratory of New Processing Technology for Nonferrous Metals and Materialsand School of ResourcesEnvironment and MaterialsGuangxi UniversityNanning 530004China key laboratory for Bionic Engineering Ministry of Education Jilin UniversityChangchun 130022China Hubei Collaborative Innovation Centre for Advanced Organic Chemical materials Ministry of Education Key Laboratory for the Green Preparation and Application of Functional MaterialsHubei UniversityWuhan 430062China Wellcome Trust/Cancer Research UK Gurdon Institute University of CambridgeCambridge CB21QNUK Department of Physiology Development and NeuroscienceUniversity of CambridgeCambridge CB21QNUK State key laboratory for Turbulence and Complex Systems Department of Mechanics and Engineering ScienceBeijing Innovation Center for Engineering Science and Advanced TechnologyCollege of EngineeringPeking UniversityBeijing 100871China

Walking on the water surface is an effective method for miniature robots to transport payloads with dramatically decreased interfacial drag. Current aquatic robots reported are generally actuated by a beam of focused light that can trigger asymmetrical deformation, enabling the directional movement through horizontal momentum transfer of photoinduced actuation force to the water. However, the operations are heavily dependent on manual manipulation of the focused light, making the long-term actuation and application of the aquatic robots in vast scenarios challenging. Herein, we developed a kind of water striderinspired robot that can autonomously manage the motion on the water surface under solar irradiation, with their direction steerable by a magnetic field. The motion of this bioinspired robot on the water surface was achieved by the use of a solar cell panel as a driving module to enable propulsive motion based on the conversion of light-electric-mechanical energies. The superhydrophobic design of its leg surfaces enables the aquatic robots with weight-bearing and drag-reducing abilities. With the assistance of magnetic navigation, the bioinspired robot can continuously and controllably locomote to the oily spill floating on the water body and collect them with high efficiency. For further demonstration, the treatment of oil spills in a campus pool with high efficiency has also been achieved. This on-site oil-spill treating strategy, taking advantage of a home-made bioinspired robot actuated by natural sunlight under magnetic steering, shows great potential applications in water-body remediation.

关键词： miniature robot superhydrophobic water strider interfacial friction magnetic actuation

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A Two-in-One Annealing Enables Dopant Free Block Copolymer Based Organic Solar Cells with over 16% Efficiency

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Chinese Journal of Chemistry 2023年第7期41卷 672-678页

作者： Shangfei Yao Linji Yang Shasha Shi Yang Zhou Min Long Wenhao Zhang Songlin Cai Ciyuan Huang Tao Liu Bingsuo Zou guangxi key lab of processing for nonferrous metals and featured materials and key lab of new processing technology for nonferrous metals and materials Ministry of EducationSchool of Physical Science and Technology and School of ResourcesEnvironments and MaterialsGuangxiUniversityNanningGuangxi 530004China

The organic solar cells(OSCs)based on block copolymer systems bear the hope of achieving the optimal balance of power conversion efficiency(PCE)and stability,but the key index,PCE of this type devices is still *** improve the efficiency,regulating the thin-film morphology is always the core engineering,which is usually achieved via two aspects:precursor optimization and post treatments.

关键词： Block copolymer system Morphology Post treatment Organic solar cells Efficiency

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Multi-functional layered double hydroxides supported by nanoporous gold toward overall hydrazine splitting

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Frontiers of Chemical Science and Engineering 2024年第1期18卷 61-69页

作者： Yongji Qin Huijie Cao Qian Liu Shaoqing Yang Xincai Feng Hao Wang Meiling Lian Dongxing Zhang Hua Wang Jun Luo Xijun Liu ShenSi lab Shenzhen Institute for Advanced StudyUniversity of Electronic Science and Technology of ChinaShenzhen 518110China Institute for new Energy materials and Low-Carbon Technologies School of Materials Science and EngineeringTianjin University of TechnologyTianjin 300384China State key laboratory of featured Metal materials and Life-cycle Safety for Composite Structures Guangxi Key Laboratory of Processing for Non-ferrous Metals and Featured MaterialsSchool of ResourcesEnvironment and MaterialsGuangxi UniversityNanning 530004China Institute for Advanced Study Chengdu UniversityChengdu 610106China China National Coal Group Corporation Beijing 100120China Tianjin Engineering Research Center of Civil Aviation Energy Environment and Green Development School of Transportation Science and EngineeringCivil Aviation University of ChinaTianjin 300300China

Layered double hydroxides have demonstrated great potential for the oxygen evolution reaction,which is a crucial half-reaction of overall water ***,it remains challenging to apply layered double hydroxides in other electrochemical reactions with high efficiency and ***,we report two-dimensional multifunctional layered double hydroxides derived from metalorganic framework sheet precursors supported by nanoporous gold with high porosity,which exhibit appealing performances toward oxygen/hydrogen evolution reactions,hydrazine oxidation reaction,and overall hydrazine *** as-prepared catalyst only requires an overpotential of 233 mV to reach 10 mA·cm^(-2) toward oxygen evolution *** overall hydrazine splitting cell only needs a cell voltage of 0.984 V to deliver 10 mA·cm^(-2),which is far more superior than that of the overall water splitting system(1.849 V).The appealing performances of the catalyst can be contributed to the synergistic effect between the metal components of the layered double hydroxides and the supporting effect of the nanoporous gold substrate,which could endow the sample with high surface area and excellent conductivity,resulting in superior activity and stability.

关键词： layered double hydroxide oxygen evolution reaction hydrazine oxidation reaction overall hydrazine splitting hydrogen production

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