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STUDIES ON PRIMARY CRYSTALLIZATION OF RAPIDLY QUENCHED Al-Ni-Cu-Nd METALLIC GLASS BY USING HIGH RESOLUTION TRASMISSION ELECTRON MICROSCOPY

引用

Acta Metallurgica Sinica(English Letters) 2003年第5期16卷 407-415页

作者： M.T.Clavaguera-Mora J.Rodriguez-Viejo Y.D.Xiao W.X.Li D.Jacovkis N.Clavaguera grupdefisicadematerialsi DepartamentdeFisicaUniversitat-AutonomadeBarcelona08193BellaterraSlaain CollegeofMaterialsScienceandEngineering Central-SouthUniversityChangsha410083China Fisicadel‘EstatSolid FacultatdeFisicaUniversitatdeBarcelonaDiagonal64708028BarcelonaSpain

Rapidly solidified Al87Ni7Cu3Nd3 metallic glasses, prepared by using melt spinning, were treated under both isothermal and non-isothermal regime. The amorphous ribbon and the annealed samples were closely examined by means of differential scanning calorimetric, conventional X-ray diffraction and high resolution transmission electron microscopy with selected-area electron diffraction, with special interest in primary crystallization into α-Al nanocrystalline particles, in order to understand structural characteristics of Al-based amorphous/nanocrystalline alloys, and nucleation and grain growth mechanism on the nanometer scale during primary crystallization. The results show that, the as-prepared ribbons are fully amorphous and homogeneous in the micron scale, but contain high density of quenched-in clusters or crystallite embryos. Primary crystallization mainly leads to formation of two-phase mixture of a-Al crystal and residual amorphous phase. The annealed ribbons exposed isother-mally at HOP C for 5, 130 minutes and heated continuously up to less than 310℃ at 40℃ C/min consist of large amount of α-Al fcc crystal nanoparticles dispersed uniformly in an amorphous matrix. However, a very little amount of finer orthorhombic Al3Ni intermetalics particles exist in the annealed ribbons heated up to 310℃. During primary crystallization, the leading kinetic mechanics to impede growth of the α-Al crystal is soft impingement, instead of geometric impingement.

关键词： rapid solidification Al-rich amorphous alloy crystallization nu- cleation and growth mechanism

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