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Effect of different metal element substitution on microstructural and comprehensive hydrogen storage performance of Ti0.9Zr0.1Mn0.95Cr0.7V0.2M0.15（M=Fe,Co,Ni,Cu,Mo） alloy

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Progress in Natural science:Materials International 2024年第2期34卷 304-313页

作者： Baojia Ni Jianhui Zhu Guo Yang Linhua Xu Haiyan Leng Wei Liu Taijun Pan Xingbo Han Lijun Lv school of Materials science and engineering Changzhou University Shanghai Institute of Applied Physics Chinese Academy of Sciences school of Materials science and engineering Shanghai University

Hydrogen is now being used as a renewable clean energy carrier.One of the main issues with the application of hydrogen energy is a shortage of security and efficient hydrogen storage technology.TiMn-based alloys are considered promising hydrogen storage materials,but their comprehensive hydrogen storage properties and cyclic stable performance limit their further practical application.The hydrogen storage properties of alloys can be enhanced by substituting transition metal elements.Therefore,the comprehensive hydrogen storage performance of the Ti0.9Zr0.1Mn0.95Cr0.7V0.2M0.15（M=Fe,Co,Ni,Cu,Mo） alloys was systematically investigated according to the Mn element on the B side is partially replaced by variety of transition metal elements.The M=Ni alloy,which showed the highest hydrogen storage capacity among the group of alloys,was used to explore cycle stability.The plateau pressures of the series alloys decreased in order,Fe>Co>Ni>Cu>Mo.Aspects of hydrogen absorption kinetics,all of the alloys can reach full hydrogen absorption saturation within 400 s at 303 K.The Ti0.9Zr0.1Mn0.95Cr0.7V0.2Mo0.15alloy possessed the fastest hydrogen absorption kinetic rate(t0.9=65 s) and the smallest hysteresis factor.This suggests that the substitution of Mo elements is effective in improving the hysteresis of the Laves phase alloys.Among the series of alloys,the M=Ni alloy exhibited the best overall hydrogen storage performance,which hydrogen storage capacity can reach 1.81 wt% and 97% of its capacity is kept after 100 cycles.

关键词： Cyclic stable performance Element substitution Hydrogen storage properties Laves phase TiMn-Based hydrogen storage alloy

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An extended numerical model of the first exothermic peak for three dimensional printed cement-based materials

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Frontiers of Structural and Civil engineering 2024年第1期18卷 80-88页

作者： Wei JIANG Wenqian LI Xi CHEN school of Materials science and engineering Tongji UniversityShanghai 200092China school of Civil engineering Tongji UniversityShanghai 200092China

The first exothermic peak of cement-based material occurs a few minutes after mixing,and the properties of three dimensional(3D)printed concrete,such as setting time,are very sensitive to this.Against this background,based on the classical Park cement exothermic model of hydration,we propose and construct a numerical model of the first exothermic peak,taking into account the proportions of C_(3)S,C_(3)A and quicklime in particular.The calculated parameters are calibrated by means of relevant published exothermic test data.It is found that this developed model offers a good simulation of the first exothermic peak of hydration for C_(3)S and C_(3)A proportions from 0 to 100% of cement clinker and reflects the effect of quicklime content at 8%-10%.The unique value of this research is provision of an important computational tool for applications that are sensitive to the first exothermic peak of hydration,such as 3D printing.

关键词： 3D printed cement-based materials cement hydration the first exothermic peak liquid quick-setting agent numerical model

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Hierarchical V3S4/C nanofibers with fast kinetics for superior alkali metal batteries

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Rare Metals 2024年第4期43卷 1836-1844页

作者： Li Chen Zhi-Xin Rao Zhi Chen Zhao-Hui Wu Shuai Yang Zhi-Jun Feng Hui-Yong Yang Fan-Yan Zeng Xi-Bao Li Jin-Yang Hu Jun-Tong Huang school of Materials science and engineering Nanchang Hangkong University school of Aeronautical Manufacturing engineering Nanchang Hangkong University

Owing to the numerous benefits,including low cost and great theoretical capacity,V3S4 has been a research hotspot for Li+/Na+/K+storage.Nonetheless,the V3S4electrode with long cycling stability and high specific capacities continues to pose significant challenges.In this work,vacuum vulcanization is combined with electrospinning to synthesize V3S4/C composite nanofibers （V3S4@CNF）.

关键词： Sulfur compounds

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Multi-physics multi-scale simulation of unique equiaxed-to-columnar-to-equiaxed transition during the whole solidification process of Al-Li alloy laser welding

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Journal of Materials science & Technology 2024年第4期171卷 235-251页

作者： Chu Han Ping Jiang Shaoning Geng Liangyuan Ren school of Mechanical science and engineering Huazhong University of Science&Technology(HUST)Wuhan430074China

In this study,a novel multi-physics multi-scale model with the dilute multicomponent phase-field method in three-dimensional(3D)space was developed to investigate the complex microstructure evolu-tion in the molten pool during laser welding of Al-Li alloy.To accurately compute mass data within both two and three-dimensional computational domains,three efficient computing methods,including central processing unit parallel computing,adaptive mesh refinement,and moving-frame algorithm,were uti-lized.Emphasis was placed on the distinctive equiaxed-to-columnar-to-equiaxed transition phenomenon that occurs during the entire solidification process of Al-Li alloy laser welding.Simulation results indi-cated that the growth distance of columnar grains that epitaxially grew from the base metal(BM)de-creased as the nucleation rate increased.As the nucleation rate increased,the morphology of the newly formed grains near the fusion boundary(FB)changed from columnar to equiaxed,and newly formed equiaxed grains changed from having high-order dendrites to no obvious dendrite structure.When the nucleation rate was sufficiently high,non-dendritic equiaxed grains could directly form near the FB,and there was nearly no epitaxial growth from the BM.Additionally,simulation results illustrated the com-petition among multiple grains with varying orientations that grow in 3D space near the FB.Finally,how equiaxed grain bands develop was elucidated.The equiaxed band not only hindered the growth of early columnar grains but also some of its grains could grow epitaxially to form new columnar grains.These predicted results were in good agreement with experimental measurements and observations.

关键词： Laser welding Al-Li alloy Equiaxed-to-columnar-to-equiaxed transition Multi-physics multi-scale model Multicomponent alloys 3D phase-field model

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Dynamical switchable quantum nonreciprocity induced by off-resonant chiral two-photon driving

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science China(Physics,Mechanics & Astronomy) 2024年第6期67卷 31-37页

作者： Da-Wei Liu Zi-Hao Li Shi-Lei Chao Ying Wu Liu-Gang Si school of Physics and Institute for Quantum science and engineering Huazhong University of Science and TechnologyWuhan 430074China

Optical nonreciprocity,which refers to the direction-dependent emission,scattering and absorption of photons,plays a very important role in quantum engineering and quantum information processing.Here,we propose an all-optical approach to achieve the optical dynamical switchable quantum nonreciprocity by an off-resonant chiral two-photon driving in a single microring cavity,which differs from the conventional nonreciprocal schemes.It is shown that the optical field with time-dependent statistical properties can be generated and the nonreciprocity flips periodically,with switchable photon blockade and photon-induced tunneling effects.We find that the dynamical system is robust and immune to the parameter variations,which loosens the parameter range of system.Meanwhile,the time window for one-way quantum information is sufficiently wide and tunable.Our work opens a new idea for the current quantum nonreciprocal research,which can facilitate a memory functionality and be used for future inmemory superconducting quantum compute.The other nonreciprocal quantum devices,i.e.,dynamical switchable nonreciprocal squeezing and entanglement,may be inspired by our method,which is expected to have important applications in future quantum technology.

关键词： dynamical switchable nonreciprocity single-photon source chiral two-photon driving

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Re-delocalization of localized d-electrons in VO2（R）-VS4 hetero-structure enables high performance of rechargeable Mg-ion batteries

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Journal of Magnesium and Alloys 2024年第5期12卷 1830-1840页

作者： Lijiao Zhou Chao Shen Xueyang Hou Zhao Fang Ting Jin Keyu Xie school of Materials science and engineering Northwestern Polytechnical University school of Metallurgical engineering Xi'an University of Architecture and Technology

Rechargeable Mg-ion batteries（MIBs） have attracted much more attentions by virtue of the high capacity from the two electrons chemistry.However, the reversible Mg2+diffusion in cathode materials is restricted by the strong interactions between the high-polarized bivalent Mg2+ions and anionic lattice. Herein, we design and propose a hetero-structural VO2（R）-VS4cathode, in which the re-delocalized d-electrons can effectively shield the polarity of Mg2+ions. Theoretically, the electrons should spontaneously transfer from VS4to VO2（R） through the interfaces of hetero-structure due to the lower work function value of VS4. Furthermore, the internal electrons transfer lead to the electronic injection into VO2（R） from VS4and the partially broken V-V dimers, indicating the presence of lone pair electrons and charge re-delocalization. Benefiting from the shield effect of re-delocalized electrons, and the weakened attraction between cations and O/S anions enables more S2--S22-redox groups to participate the electrochemical reactions and compensate the double charge of Mg2+ions. Accordingly,VO2（R）-VS4hetero-structure exhibits a high specific capacity of 554 mA h g-1at 50 mA g-1. It is believed that the charge re-delocalization of cathode extremely boost the Mg2+ions migration for the high-capacity of MIBs.

关键词： Mg-ion batteries Cathode Charge delocalization Electronic structure Heterostructure

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A frequency servo SoC with output power stabilization loop technology for miniaturized atomic clocks

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Journal of Semiconductors 2024年第6期45卷 13-22页

作者： Hongyang Zhang Xinlin Geng Zonglin Ye Kailei Wang Qian Xie Zheng Wang school of Integrated Circuit science and engineering University of Electronic Science and Technology of ChinaChengdu 611731China

A frequency servo system-on-chip(FS-SoC)featuring output power stabilization technology is introduced in this study for high-precision and miniaturized cesium(Cs)atomic clocks.The proposed power stabilization loop(PSL)technique,incorporating an off-chip power detector(PD),ensures that the output power of the FS-SoC remains stable,mitigating the impact of power fluctuations on the atomic clock's stability.Additionally,a one-pulse-per-second(1PPS)is employed to syn-chronize the clock with GPS.Fabricated using 65 nm CMOS technology,the measured phase noise of the FS-SoC stands at-69.5 dBc/Hz@100 Hz offset and-83.9 dBc/Hz@1 kHz offset,accompanied by a power dissipation of 19.7 mW.The Cs atomic clock employing the proposed FS-SoC and PSL obtains an Allan deviation of 1.7×10^(-11) with 1-s averaging time.

关键词： CMOS technology atomic clock phase-locked loop output power stabilization 1PPS

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Hydrogels for active photonics

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Microsystems & Nanoengineering 2024年第1期10卷 1-16页

作者： Byoungsu Ko Nara Jeon Jaekyung Kim Hyunjung Kang Junhwa Seong Suhyeon Yun Trevon Badloe Junsuk Rho Department of Mechanical engineering Pohang University of Science and Technology(POSTECH)Pohang 37673Republic of Korea Department of Chemical engineering Pohang University of Science and Technology(POSTECH)Pohang 37673Republic of Korea graduate school of Artificial Intelligence Pohang University of Science and Technology(POSTECH)Pohang 37673Republic of Korea POSCO-POSTECH-RIST Convergence Research Center for Flat Optics and Metaphotonics Pohang 37673Republic of Korea

Conventional photonic devices exhibit static optical properties that are design-dependent,including the material’s refractive index and geometrical parameters.However,they still possess attractive optical responses for applications and are already exploited in devices across various fields.Hydrogel photonics has emerged as a promising solution in the field of active photonics by providing primarily deformable geometric parameters in response to external stimuli.Over the past few years,various studies have been undertaken to attain stimuli-responsive photonic devices with tunable optical properties.Herein,we focus on the recent advancements in hydrogel-based photonics and micro/nanofabrication techniques for hydrogels.In particular,fabrication techniques for hydrogel photonic devices are categorized into film growth,photolithography(PL),electron-beam lithography(EBL),and nanoimprint lithography(NIL).Furthermore,we provide insights into future directions and prospects for deformable hydrogel photonics,along with their potential practical applications.

关键词： lithography photonics attractive

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Effect of titanium on the wettability between Fe-P-Ti alloy and Al2O3 substrate

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Progress in Natural science:Materials International 2024年第3期34卷 555-561页

作者： Rui Wang Shengjie Bai Xu Chen Likui Xie Zhiqiang Yu Yang Kang Yihong Li Yong Hu Zhiyue Shi Zhijie Yan school of Materials science and engineering North University of China Shanxi Key Laboratory of Advanced Metal Materials for Special Environments North University of China CISDI engineering CO. LTD. school of Materials science and engineering Taiyuan University of Science and Technology

It is of significance that the wettability between the molten alloy and the Al2O3affects the inclusion removal,nozzle clogging and refractory erosion. In the present work, the wettability between the Al2O3substrate and Fe–P–Ti alloys with different Ti content was investigated by using the sessile droplets method. The interfacial characteristics were investigated by scanning electron microscope（SEM）. The contact angles between the sintered Al2O3substrate and Fe–P–Ti alloys with 0, 0.05, 0.10 and 0.15 wt% Ti are 100.1°, 97.3°, 94.5°and 90.5°,respectively. The oxidation of [Al] and [Ti] in the molten alloys leads to the formation of the oxides on the droplets. With the increase of Ti content in the Fe–P–Ti alloys, the formed oxides change from Al2O3to Ticontaining oxides. The reaction between [Ti] and Al2O3substrate in the interface results in the formation of Ti-containing oxides. The quantity of the interfacial oxides increases with the increase of Ti content in the alloys.As a result, the synergetic effect of the formation of the interfacial products and the oxides on the surface of droplets leads to the decrease of the contact angles between the Al2O3substrate and Fe–P–Ti alloys due to the increase of Ti content.

关键词： Al2O3 substrate Contact angle Fe–P–Ti alloys Interfacial reaction Wettability

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Color Image Compression and Encryption Algorithm Based on 2D Compressed Sensing and Hyperchaotic System

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Computers, Materials & Continua 2024年第2期78卷 1977-1993页

作者： Zhiqing Dong Zhao Zhang Hongyan Zhou Xuebo Chen school of Computer science and Software engineering University of Science and Technology LiaoningAnshan114051China school of Electronic and Information engineering University of Science and Technology LiaoningAnshan114051China

With the advent of the information security era,it is necessary to guarantee the privacy,accuracy,and dependable transfer of pictures.This study presents a new approach to the encryption and compression of color images.It is predicated on 2D compressed sensing(CS)and the hyperchaotic system.First,an optimized Arnold scrambling algorithm is applied to the initial color images to ensure strong security.Then,the processed images are con-currently encrypted and compressed using 2D CS.Among them,chaotic sequences replace traditional random measurement matrices to increase the system’s security.Third,the processed images are re-encrypted using a combination of permutation and diffusion algorithms.In addition,the 2D projected gradient with an embedding decryption(2DPG-ED)algorithm is used to reconstruct images.Compared with the traditional reconstruction algorithm,the 2DPG-ED algorithm can improve security and reduce computational complexity.Furthermore,it has better robustness.The experimental outcome and the performance analysis indicate that this algorithm can withstand malicious attacks and prove the method is effective.

关键词： Image encryption image compression hyperchaotic system compressed sensing

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