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Surface engineering of ZnO electrocatalyst by N doping towards electrochemical CO_(2) reduction

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Journal of Energy Chemistry 2024年第1期88卷 71-81,I0002页

作者： Rohini Subhash Kanase Getasew Mulualem Zewdie Maheswari Arunachalam Jyoti Badiger Suzan Abdelfattah Sayed Kwang-Soon Ahn Jun-Seok Ha Uk Sim Hyeyoung Shin Soon Hyung Kang Department of Interdisciplinary program for Photonic engineering Chonnam National UniversityGwangju 61186Republic of Korea graduate School of Energy Science and Technology(GEST) Chungnam National University99 Daehak-roYuseong-guDaejeon 34134Republic of Korea Department of Chemistry Education and Optoelectronic convergence Research Center Chonnam National UniversityGwangju 61186Republic of Korea Department of Advanced Chemicals and engineering Chonnam National UniversityGwangju 61186Republic of Korea School of Chemical engineering Yeungnam UniversityGyeongsan 38541Republic of Korea Department of Energy engineering Korea Institute of Energy Technology(KENTECH)Naju 58217Republic of Korea

The discovery of efficient,selective,and stable electrocatalysts can be a key point to produce the largescale chemical fuels via electrochemical CO_(2) reduction(ECR).In this study,an earth-abundant and nontoxic ZnO-based electrocatalyst was developed for use in gas-diffusion electrodes(GDE),and the effect of nitrogen(N)doping on the ECR activity of ZnO electrocatalysts was ***,a ZnO nanosheet was prepared via the hydrothermal method,and nitridation was performed at different times to control the N-doping *** an increase in the N-doping content,the morphological properties of the nanosheet changed significantly,namely,the 2D nanosheets transformed into irregularly shaped ***,the ECR performance of Zn O electrocatalysts with different N-doping content was assessed in 1.0 M KHCO_(3) electrolyte using a gas-diffusion electrode-based ECR *** the ECR activity increased after a small amount of N doping,it decreased for higher N doping *** them,the N:ZnO-1 h electrocatalysts showed the best CO selectivity,with a faradaic efficiency(FE_(CO))of 92.7%at-0.73 V *** hydrogen electrode(RHE),which was greater than that of an undoped Zn O electrocatalyst(FE_(CO)of 63.4%at-0.78 V_(RHE)).Also,the N:ZnO-1 h electrocatalyst exhibited outstanding durability for 16 h,with a partial current density of-92.1 mA cm^(-2).This improvement of N:ZnO-1 h electrocatalyst can be explained by density functional theory calculations,demonstrating that this improvement of N:ZnO-1 h electrocatalyst comes from(ⅰ)the optimized active sites lowering the free energy barrier for the rate-determining step(RDS),and(ⅱ)the modification of electronic structure enhancing the electron transfer rate by N doping.

关键词： ZnO N-doped ZnO Gas-diffusion electrode CO Selectivity Electrochemical CO_(2)reduction

Hydrogels for active photonics

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Microsystems & Nanoengineering 2024年第1期10卷 1-16页

作者： Byoungsu Ko Nara Jeon Jaekyung Kim Hyunjung Kang Junhwa Seong Suhyeon Yun Trevon Badloe Junsuk Rho Department of Mechanical engineering Pohang University of Science and Technology(POSTECH)Pohang 37673Republic of Korea Department of Chemical engineering Pohang University of Science and Technology(POSTECH)Pohang 37673Republic of Korea graduate School of Artificial Intelligence Pohang University of Science and Technology(POSTECH)Pohang 37673Republic of Korea POSCO-POSTECH-RIST convergence Research Center for Flat Optics and Metaphotonics Pohang 37673Republic of Korea

Conventional photonic devices exhibit static optical properties that are design-dependent,including the material’s refractive index and geometrical ***,they still possess attractive optical responses for applications and are already exploited in devices across various *** photonics has emerged as a promising solution in the field of active photonics by providing primarily deformable geometric parameters in response to external *** the past few years,various studies have been undertaken to attain stimuli-responsive photonic devices with tunable optical ***,we focus on the recent advancements in hydrogel-based photonics and micro/nanofabrication techniques for *** particular,fabrication techniques for hydrogel photonic devices are categorized into film growth,photolithography(PL),electron-beam lithography(EBL),and nanoimprint lithography(NIL).Furthermore,we provide insights into future directions and prospects for deformable hydrogel photonics,along with their potential practical applications.

关键词： lithography photonics attractive

Assessing mixing uniformity in microreactors via in-line spectroscopy

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Chinese Journal of Chemical engineering 2024年第2期66卷 119-124页

作者： Shusaku Asano Shinji Kudo Taisuke Maki Yosuke Muranaka Kazuhiro Mae Jun-ichiro Hayashi Institute for Materials Chemistry and engineering Kyushu UniversityKasuga 816-8580Japan Department of Chemical engineering Graduate School of EngineeringKyoto UniversityJapan

Mixing behavior is critical for enhancing the selectivity of fast chemical reactions in microreactors.A high Reynolds number(Re)improves the mixing rate and selectivity of the reactions,but some exceptions of increasing side product yield with the higher Re have been *** study investigated the mixing uniformity in microreactors with in-line UV-vis spectroscopy to clarify the relationship between reaction selectivity and chaotic mixing with the higher Re.A colorization experiment of thymolphthalein in an acidic solution was conducted with an excess acid amount to the base to indicate a non-uniformly mixed ***-uniformity significantly increased with *** the same time,the degree of mixing,which was measured by a usual decolorization experiment,showed that the mixing rate increased with *** in-line analysis of the Villermaux-Dushman reaction during the mixing clarified that side product yield significantly increased with Re at around 300 and then decreased at around *** results suggest the compensation effect between the mixing uniformity and mixing rate on the selectivity of the mixing-sensitive *** mixing,characterized by a larger Re,can disturb mixing uniformity and,in some cases,decrease reaction selectivity.

关键词： Microreactor Villermaux-Dushman reaction In-line analysis Mixing Mass transfer Uniformity

Tailoring high-refractive-index nanocomposites for manufacturing of ultraviolet metasurfaces

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Microsystems & Nanoengineering 2024年第2期10卷 303-310页

作者： Hyunjung Kang Dongkyo Oh Nara Jeon Joohoon Kim Hongyoon Kim Trevon Badloe Junsuk Rho Department of Mechanical engineering Pohang University of Science and Technology(POSTECH)PohangRepublic of Korea graduate School of Artificial Intelligence Pohang University of Science and Technology(POSTECH)PohangRepublic of Korea Department of Chemical engineering Pohang University of Science and Technology(POSTECH)PohangRepublic of Korea Department of Electrical engineering Pohang University of Science and Technology(POSTECH)PohangRepublic of Korea POSCO-POSTECH-RIST convergence Research Center for Flat Optics and Metaphotonics PohangRepublic of Korea National Institute of Nanomaterials Technology(NINT) PohangRepublic of Korea

Nanoimprint lithography(NIL)has been utilized to address the manufacturing challenges of high cost and low throughput for optical *** overcome the limitations inherent in conventional imprint resins characterized by a low refractive index(n),high-n nanocomposites have been introduced to directly serve as ***,comprehensive research on these nanocomposites is notably *** this study,we focus on the composition of high-n zirconium dioxide(ZrO_(2))nanoparticle(NP)concentration and solvents used to produce ultraviolet(UV)metaholograms and quantify the transfer fidelity by the measured conversion *** utilization of 80 wt%ZrO_(2)NPs in MIBK,MEK,and acetone results in conversion efficiencies of 62.3%,51.4%,and 61.5%,respectively,at a wavelength of 325 *** analysis of the solvent composition and NP concentration can further enhance the manufacturing capabilities of high-n nanocomposites in NIL,enabling potential practical use of optical metasurfaces.

关键词： ultraviolet refractive nanocomposites

Evolutionary Variational YOLOv8 Network for Fault Detection in Wind Turbines

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Computers, Materials & Continua 2024年第7期80卷 625-642页

作者： Hongjiang Wang Qingze Shen Qin Dai Yingcai Gao Jing Gao Tian Zhang College of Information Shenyang Institute of EngineeringShenyang110136China graduate School Shenyang Institute of EngineeringShenyang110136China College of Software Northeastern UniversityShenyang110169China

Deep learning has emerged in many practical applications,such as image classification,fault diagnosis,and object *** recently,convolutional neural networks(CNNs),representative models of deep learning,have been used to solve fault ***,the current design of CNNs for fault detection of wind turbine blades is highly dependent on domain knowledge and requires a large amount of trial and *** this reason,an evolutionary YOLOv8 network has been developed to automatically find the network architecture for wind turbine blade-based fault ***8 is a CNN-backed object detection ***,to reduce the parameter count,we first design an improved FasterNet module based on the Partial Convolution(PConv)***,to enhance convergence performance,we improve the loss function based on the efficient complete intersection over the *** on this,a flexible variable-length encoding is proposed,and the corresponding reproduction operators are *** experimental results confirmthat the proposed approach can achieve better fault detection results and improve by 2.6%in mean precision at 50(mAP50)compared to the existing ***,compared to training with the YOLOv8n model,the YOLOBFE model reduces the training parameters by 933,937 and decreases the GFLOPS(Giga Floating Point Operations Per Second)by 1.1.

关键词： Neural architecture search YOLOv8 evolutionary computation fault detection

Functionally graded structure of a nitride-strengthened Mg_(2)Si-based hybrid composite

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Journal of Magnesium and Alloys 2024年第3期12卷 1239-1256页

作者： Jeongho Yang Woongbeom Heogh Hogi Ju Sukhyun Kang Tae-Sik Jang Hyun-Do Jung Mohammad Jahazi Seung Chul Han Seong Je Park Hyoung Seop Kim Susmita Bose Amit Bandyopadhyay Martin Byung-Guk Jun Young Won Kim Dae-kyeom Kim Rigoberto CAdvincula Clodualdo Aranas Jr Sang Hoon Kim School of Mechanical engineering Pusan National UniversityBusan 46241Republic of Korea Department of Mechanical Design engineering Hanyang UniversitySeoul 04763Republic of Korea Process Research 3 Team LG Display Co.Ltd.PajuGyeonggi-do 10845Republic of Korea Department of Materials Science and engineering Chosun UniversityGwangju 61452Republic of Korea Institute of Well-Aging Medicare&Chosun University LAMP Center Chosun UniversityGwangju 61452Republic of Korea Division of Materials Science and engineering Hanyang UniversitySeoul 04763Republic of Korea Department of Mechanical engineering École de Technologie SupérieureMontrealQuebec H3C 1K3Canada Material&Component convergence R&D Center Korea Construction Equipment Technology InstituteGunsanJeollabuk-do 54002Republic of Korea School of Mechanical and Aerospace engineering Nanyang Technological UniversitySingapore 639798Singapore graduate Institute of Ferrous&Eco Materials Technology Pohang University of Science and TechnologyPohangGyeongsangbuk-do 37673Republic of Korea Advanced Institute for Materials Research Tohoku UniversitySendai 980-8577Japan Institute for convergence Research and Education in Advanced Technology Yonsei UniversitySeoul 03722Republic of Korea School of Mechanical and Materials engineering Washington State UniversityPullmanWashington 99164USA School of Mechanical engineering Purdue UniversityWest LafayetteIndiana 47907USA Research Institute of Advanced Manufacturing Technology Korea Institute of Industrial TechnologyIncheon 21999Republic of Korea Department of Macromolecular Science and engineering Case Western Reserve UniversityClevelandOhio 44106USA Department of Chemical and Biomolecular engineering and Joint Institute for Advanced Materials University of TennesseeKnoxvilleTennessee 37996USA Center for Nanophase Materials and Sciences Oak Ridge National LaboratoryOak RidgeTennessee 37830USA Department of Mechanical engineering University of New BrunswickFrederictonNew Brunswick E3B 5A3Cana

The ex-situ incorporation of the secondary SiC reinforcement,along with the in-situ incorporation of the tertiary and quaternary Mg_(3)N_(2) and Si_(3)N_(4) phases,in the primary matrix of Mg_(2)Si is employed in order to provide ultimate wear resistance based on the laser-irradiation-induced inclusion of N_(2) gas during laser powder bed *** is substantialized based on both the thermal diffusion-and chemical reactionbased metallurgy of the Mg_(2)Si–SiC/nitride hybrid *** study also proposes a functional platform for systematically modulating a functionally graded structure and modeling build-direction-dependent architectonics during additive *** strategy enables the development of a compositional gradient from the center to the edge of each melt pool of the Mg_(2)Si–SiC/nitride hybrid ***,the coefficient of friction of the hybrid composite exhibits a 309.3%decrease to–1.67 compared to–0.54 for the conventional nonreinforced Mg_(2)Si structure,while the tensile strength exhibits a 171.3%increase to 831.5 MPa compared to 485.3 MPa for the conventional *** outstanding mechanical behavior is due to the(1)the complementary and synergistic reinforcement effects of the SiC and nitride compounds,each of which possesses an intrinsically high hardness,and(2)the strong adhesion of these compounds to the Mg_(2)Si matrix despite their small sizes and low concentrations.

关键词： Laser powder bed fusion Mg_(2)Si-SiC/nitride hybrid composite Both the thermal diffusion-and chemical reaction-based metallurgy Functionally graded structure Compositional gradient Wear resistance.

SUV39H1-driven NFATc1 methylation is essential for the c-Cbl-mediated degradation of NFATc1 in an osteoclast lineage

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Genes & Diseases 2024年第4期11卷 86-89页

作者： Do-Won Jeong Hye-Jin Kim Jong-Wan Park Seulbee Lee Hyeryeon Jung Eugene C.Yi Nacksung Kime Yang-Sook Chun Department of Biomedical Sciences Seoul National University College of MedicineSeoul 03080Republic of Korea Department of Physiology Seoul National University College of MedicineSeoul 03080Republic of Korea Ischemic/Hypoxic Disease Institute Seoul National University College of MedicineSeoul 03080Republic of Korea Department of Molecular Medicine and Biopharmaceutical Sciences Graduate School of Convergence Science and Technology and College of Medicine Or College of PharmacySeoul National UniversitySeoul 03080Republic of Korea Department of Pharmacology Chonnam National University Medical SchoolGwangju 61469Republic of Korea

Bone undergoes continuous remodeling by tightly-coordinated actions of bone-resorbing osteoclasts and boneforming osteoblasts.1 Recent studies document that the dysregulation of histone methylation profiles is associated with the progression of ***,the specific epigenetic modifiers are incompletely *** this study,we demonstrate an inhibitory role of a variegation 3-9 homolog 1(SUV39H1)in osteoclast formation.

关键词： osteoclast remodeling incomplete

Evaluation of Psychological Changes on Women Following Coordination Exercises: Immediate Effects of Life Kinetik® Implementation

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Open Journal of Therapy and Rehabilitation 2024年第3期12卷 256-262页

作者： Yutaro Hyodo Takumi Jiroumaru Hikaru Kitagawa Yasumasa Oka Junko Ochi Nobuko Shichiri Takamitsu Fujikawa Department of Physical Therapy Bukkyo University Kyoto City Japan Kanazawa Orthopaedic and sports Medicine Clinic Ritto Japan Department of Applied Biology Graduate School of Science and Technology Kyoto Institute of Technology Kyoto City Japan

Objective: This study aimed to evaluate the immediate psychological effects of coordination exercises on women in Japan. Methods: The subjects were 17 adult women (height, 160.1 ± 5.1 cm;weight, 54.3 ± 10.5 kg;age, 57.8 ± 8.3 years) living in the community and attending a fitness club. The subjects performed a coordination exercise called Life Kinetik®. The subjects responded to the Two-Dimensional Mood Scale–Short Term before and after performing 30 minutes of Life Kinetik®. The results were tabulated and four psychological states were calculated (i.e., vitality, stability, pleasure, and arousal). The pre- and post-implementation results were statistically analyzed using a corresponding t-test. Results: Significant differences were found in activation and arousal levels, but not in stability and comfort levels. Conclusion: The coordination exercise, Life Kinetik®, was found to be an exercise program with potential psychological benefits, as it could change women’s psychological condition to active and excited states.

关键词： Psychological State Life Kinetik® Mood Scale

Copper nanowire/multi-walled carbon nanotube com- posites as all-nanowire flexible electrode for fast-charging/ discharging lithium-ion battery

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Nano Research 2018年第2期11卷 769-779页

作者： Zhenxing Yin Sanghun Cho Duck-Jae You Yong-keon Ahn Jeeyoung Yoo Youn Sang Kim program in Nano Science and Technology Graduate School of Convergence Science and Technology Seoul National University Seoul Republic of Korea Advanced Institutes of convergence Technology Gyeonggi-do Republic of Korea

A novel lightweight three-dimensional （3D） composite anode for a fast-charging] discharging Li-ion battery （LIB） was fabricated entirely using one-dimensional （1D） nanomaterials, i.e., Cu nanowires （CuNWs） and multi-walled C nanotubes （MWCNTs）. Because of the excellent electrical conductivity, high-aspect ratio structures, and large surface areas of these nanomaterials, the CuNW-MWCNT composite （CNMC） with 3D structure provides significant advantages regarding the transport pathways for both electrons and ions. As an advanced binder-free anode, a CuNW-MWCNT composite film with a controllable thickness （~ 600 prn） exhibited a considerably low sheet resistance, and internal cell resistance. Furthermore, the random CuNW network with 3D structure acting as a rigid framework not only prevented MWCNT shrinkage and expansion due to aggregation and swelling but also minimized the effect of the volume change during the charge/discharge process. Both a half cell and a full cell of LIBs with the CNMC anode exhibited high specific capacities and Coulombic efficiendes, even at a high current. More importantly, we for the first time overcame the limitation of MWCNTs as anode materials for fast-charging]discharging LIBs （both half cells and full cells） by employing CuNWs, and the resulting anode can be applied to flexible LIBs. This innovative anode structure can lead to the development of ultrafast chargeable LIBs for electric vehides.

关键词： three-dimensional (3D)composite,all-nanowire electrode,fast chargeable batter3 fuN-cell Li-ion batteries(L1Bs),flexible battery